• Title/Summary/Keyword: nano-glass

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Nano-scale adhesion and friction on Si wafer with the tip size using AFM

  • R. Arvind Singh;Yoon, Eui-Sung;Oh, Hyun-Jin;Kong, Ho-Sung
    • KSTLE International Journal
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    • v.5 no.1
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    • pp.1-6
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    • 2004
  • Nano-scale studies on adhesion and friction were conducted in Si-wafer (100) using Atomic Force Microscopy (AFM). Glass (Borosilicate) balls of radii 0.32$\mu\textrm{m}$, 1.25$\mu\textrm{m}$, and 2.5$\mu\textrm{m}$, mounted on cantilever (Contact Mode type NPS) were used as tips. Adhesion and friction between Si-wafer and glass tips were measured at ambient temperature (24${\pm}$1$^{\circ}C$) and humidity (45${\pm}$5%). Friction was measured as a function of applied normal load in the range of 0-160 nN. Results showed that, both adhesion and friction increased with the tip radii. Also, friction increased linearly as a function of applied normal load. The effect of tip size on adhesion and friction was explained as the influence of the capillary force exerted by meniscus and that of the contact area on these parameters respectively. The coefficient of friction was estimated in two different ways, as the slope from the plot of friction force against the applied normal load and as the ratio between the friction force and the applied normal load. Both these estimates showed that the coefficient of friction increased with the tip size. Further, the influence of the adhesion force on the coefficient of friction was also discussed.

Characteristics of Indium Zinc Tin Oxide films grown by RF magnetron sputtering for organic light emitting diodes (RF magnetron sputtering system으로 성장시킨 OLED용 IZTO 박막의 특성연구)

  • Park, Ho-Kyun;Jeong, Soon-Wook;Kim, Han-Ki
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.412-413
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    • 2007
  • We report on the electrical, optical, and structural properties of indium zinc tin oxide (IZTO) anode films grown at room temperature on glass substrate. The IZTO anode films grown by a RF magnetron sputtering were investigated as functions of RF power, working pressure, and process time in pure Ar ambient. To investigate electrical, optical and structural properties of IZTO anode films, 4-point probe, Hall measurement, UV/Vis spectrometer, Field Emission Scanning Electron Microscopy (FE-SEM), and X-ray diffraction (XRD) were performed, respectively. A sheet resistance of $13.88\;{\Omega}/{\square}$, average transmittance above 80 % in visible range were obtained from optimized IZTO anode films grown on glass substrate. These results shown the amorphous structure regardless of RF power and working pressure due to low substrate temperature.

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Experimental and numerical bending deflection of cenosphere filled hybrid (Glass/Cenosphere/Epoxy) composite

  • Pandey, Harsh Kumar;Agrawal, Himanshu;Panda, Subrata Kumar;Hirwani, Chetan Kumar;Katariya, Pankaj V.;Dewangan, Hukum Chand
    • Structural Engineering and Mechanics
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    • v.73 no.6
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    • pp.715-724
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    • 2020
  • The influence on flexural strength of Glass/Epoxy laminated composite curved panels of different geometries (cylindrical, spherical, elliptical, hyperboloid and flat) due to inclusion of nano cenosphere filler examined in this research article. The deflection responses of the hybrid structure are evaluated numerically using the isoparametric finite element technique and modelled mathematically via higher-order displacement structural kinematics. To predict the deflection values, a customised in-house computer code in MATLAB environment is prepared using the higher-order isoparametric formulation. Subsequently, the numerical model validity has been established by comparing with those of available benchmark solution including the convergence characteristics of the finite element solution. Further, a few cenosphere filled hybrid composite are prepared for different volume fractions for the experimental purpose, to review the propose model accuracy. The experimental deflection values are compared with the finite element solutions, where the experimental elastic properties are adopted for the computation. Finally, the effect of different variable design dependent parameter and the percentages of nano cenosphere including the geometrical shapes obtained via a set of numerical experimentation.

Synthesis of nano-crystalline Si films on polymer and glass by ICP-assisted RF magnetron sputtering

  • Shin, Kyung-S.;Choi, Yoon-S.;Choi, In-S.;Han, Jeon-G.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.203-203
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    • 2010
  • Nano-crystalline Si thin films were deposited on polymer and glass by inductively coupled plasma (ICP) - assisted RF magnetron sputtering at low temperature in an argon and hydrogen atmosphere. Internal ICP coil was installed to increase hydrogen atoms dissociated by the induced magnetic field near the inlet of the working gases. The microstructure of deposited films was investigated with XRD, Raman spectroscopy and TEM. The crystalline volume fraction of the deposited films on polymer was about 70% at magnetron RF power of 600W and ICP RF power of 500W. Crystalline volume fraction was decreased slightly with increasing magnetron RF power due to thermal damage by ion bombardment. The diffraction peak consists of two peaks at $28.18^{\circ}$ and $47.10^{\circ}\;2{\theta}$ at magnetron RF power of 600W and ICP RF power of 500W, which correspond to the (111), (220) planes of crystalline Si, respectively. As magnetron power increase, (220) peak disappeared and a dominant diffraction plane was (111). In case of deposited films on glass, the diffraction peak consists of three peaks, which correspond to the (111), (220) and (311). As the substrate temperature increase, dominant diffraction plane was (220) and the thickness of incubation (amorphous) layer was decreased.

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Structure and Properties of Polynorbornene Derivatives: Poly(norbornene dicarboxylic acid dialkyl ester)s and Poly(norbornene dimethyl dicarboxylate)s

  • Shin, Boo-Gyo;Cho, Tai-Yon;Yoon, Do-Y.;Liu, Binyuan
    • Macromolecular Research
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    • v.15 no.2
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    • pp.185-190
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    • 2007
  • Poly(norbornene dimethyl dicarboxylate)s, (PNDMD)s, were prepared by addition polymerization with palladium(II) catalyst from pure exo-monomers, and their structure and properties were compared with those of poly(norbornene dicarboxylic acid dialkyl ester)s, (PNDADA)s. Both polymer series exhibited good solubility in general organic solvents and excellent thermal stability up to $330^{\circ}C$. Wide-angle X-ray scattering (WAXS) study indicated the presence of nano-scale layer-like order in amorphous PNDADAs, while PNDMDs showed random amorphous structure. The glass transition temperatures and dielectric constants of solid polymers were found to decrease as the alkyl side-chain length increases for both polymer series. However, PNDMDs showed lower glass transition temperatures and higher dielectric constants, as compared with those of PNDADAs containing the same alkyl substituents. This difference, caused by the higher side-group mobility of PNDMDs, may be closely related to the nano-scale order in amorphous PNDADAs and its absence in PNDMDs.

Fabrication and Mechanical Properties of Nanoquasicrystalline Phase Reinforced Ti-based Bulk Metallic Glass Matrix Composites (나노 준결정상으로 강화된 Ti계 벌크 비정질기지 복합재의 제조 및 기계적 특성 고찰)

  • Park, Jin-Man;Lim, Ka-Ram;Kim, Tae-Eung;Sohn, Sung-Woo;Kim, Do-Hyang
    • Journal of Korea Foundry Society
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    • v.28 no.6
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    • pp.261-267
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    • 2008
  • In-situ quasicrystalline icosahedral (I) phase reinforced Ti-based bulk metallic glass (BMG) matrix composites have been successfully fabricated by using two distinct thermal histories for BMG forming alloy. The BMG composite containing micron-scale Iphase has been introduced by controlling cooling rate during solidification, whereas nano-scale I-phase reinforced BMG composite has been produced by partial crystallization of BMG. For mechanical properties, micron-scale I-phase distributed BMG composite exhibited lower strength and plasticity compared to the monolithic BMG. On the other hand, nano-scale icosahedral phase embedded BMG composite showed enhanced strength and plasticity. These improved mechanical properties were attributed to the multiplication of shear bands and blocking of the shear band propagation in terms of isolation and homogeneous distribution of nanosize icosahdral phases in the glassy matrix, followed by stabilizing the mechanical and deformation instabilities.

Characteristics of the Nd:YAG laser Spot Welding in $Cu_{54}Ni_{6}Zr_{22}Ti_{18}$ Bulk Metallic Glass Alloy ($Cu_{54}Ni_{6}Zr_{22}Ti_{18}$ 벌크비정질 합금의 Nd:YAG 레이저 점용접 특성)

  • Kim, J.H.;Lee, J.H.;Shin, S.Y.;Bae, J.C.;Lee, C.H.
    • Laser Solutions
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    • v.8 no.2
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    • pp.13-20
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    • 2005
  • Weldability is largely dependent on the phase evolution and the microstructure of the weld. For the weldability of the $Cu_{54}Ni_6Zr_{22}Ti_{18}$ bulk metallic glass, the crystallization affects the sensitivity of the weld to the brittle failure. In order to suppress the irreversible crystallization, Nd:YAG laser welding was chosen. The pulsed Nd:YAG laser was irradiated onto the BMG plate and the effects of the pulse shape [peak power intensity and pulse duration time] on the crystallinity were evaluated.

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A 0.55" PDLC-LCoS Micro-display for Mobile Projectors

  • Do, Yun-Seon;Yang, Kee-Jeong;Sung, Shi-Joon;Kim, Jung-Ho;Lee, Gwang-Jun;Lee, Yong-Hwan;Chung, Hoon-Ju;Roh, Chang-Gu;Choi, Byeong-Dae
    • 한국정보디스플레이학회:학술대회논문집
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    • 2009.10a
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    • pp.1527-1530
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    • 2009
  • A LCoS micro-display using polymer dispersed liquid crystals (PDLCs) for light switching layer was fabricated. The Si backplane of SVGA ($800{\times}600$) with a pixel size of $14{\times}14mm^2$ was prepared by a $0.35{\mu}m$ 18V CMOS process. PDLCs were filled in the gap between backplane and ITO glass by conventional vacuum filling method. The prepared panels were driven by a field sequential color (FSC) scheme at the frequency of 180Hz and were successful in modulating LED lights to show projection images. The preparation and performance of PDLC-LCoS are presented.

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Fluorine-Doping Effect on Structural and Optical Properties of ZnO Nanorods Synthesized by Hydrothermal Method

  • Yoon, Hyunsik;Kim, Ikhyun;Kang, Daeho;Kim, Soaram;Kim, Jong Su;Lee, Sang-Heon;Leem, Jae-Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.204.1-204.1
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    • 2013
  • Fluorine, the radius of which is close to that of oxygen, could be an appropriate anion doping candidate. A lower lattice distortion could be expected for F doping, compared with Al, Ga, and In doping. F-doped ZnO (FZO) and undoped ZnO nanorods were grown onto glass substrate by the hydrothemal method. The doping level in the solution, designated by F/Zn atomic ratio of was varied from 0.0 to 10.0 in 2.0 steps. To investigate the effects of the structure and optical properties of FZO nanorods were investigated using X-ray diffraction, UV-visible spectroscopy and photoluminescence (PL). For the PL spectra, the maximum peak position of NBE moves to higher energy, from 0 to 4 at.%. As the doping concentration increases, the maximum peak position of NBE gradually moves to lover energy, from 4 to 10 at.%.

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The Study of Glass Crystallization Mechanism Using Femtosecond Laser Pulse (극초단파레이저를 활용한 유리의 결정화 메커니즘 고찰)

  • Moon P.Y.;Yoon D.K.;Lee K.T.;Shin S.B.;Cho S.H.;Ryu B.K.
    • Transactions of Materials Processing
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    • v.15 no.3 s.84
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    • pp.213-219
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    • 2006
  • To improve the strength of glass is being studied in order to contribute to weight saving of flat panel displays. Generally, the strength achieved of glass-ceramics is higher as is the fracture toughness by the formation of a heterogeneous phase inside glass. In this study, Ag-doped $45SiO_2-24CaO-24Na_2O-4P_2O_5\;and\;70SiO_2-10CaO-24Na_2O-10TiO_2$ glasses were irradiated to strengthen by crystallization using femto-second laser pulse. XRD, Nano-indenter and SEM etc., irradiation of laser pulse without heat-treated samples was analyzed. Samples irradiated by laser had higher value($4.4{\sim}4.56^*10-3Pa$) of elastic modulus which related with strength of glass than values heat-treated samples and these are $1.2{\sim}1.5$ times higher values than them of mother glass. This process can be applicable to the strengthening of thinner glass plate, and it has an advantage over traditional heat-treatment and ion-exchange method.