Nano-scale adhesion and friction on Si wafer with the tip size using AFM

  • R. Arvind Singh (Tribology Research Center, Korea Institute of Science and Technology) ;
  • Yoon, Eui-Sung (Tribology Research Center, Korea Institute of Science and Technology) ;
  • Oh, Hyun-Jin (Tribology Research Center, Korea Institute of Science and Technology) ;
  • Kong, Ho-Sung (Tribology Research Center, Korea Institute of Science and Technology)
  • 발행 : 2004.06.01

초록

Nano-scale studies on adhesion and friction were conducted in Si-wafer (100) using Atomic Force Microscopy (AFM). Glass (Borosilicate) balls of radii 0.32$\mu\textrm{m}$, 1.25$\mu\textrm{m}$, and 2.5$\mu\textrm{m}$, mounted on cantilever (Contact Mode type NPS) were used as tips. Adhesion and friction between Si-wafer and glass tips were measured at ambient temperature (24${\pm}$1$^{\circ}C$) and humidity (45${\pm}$5%). Friction was measured as a function of applied normal load in the range of 0-160 nN. Results showed that, both adhesion and friction increased with the tip radii. Also, friction increased linearly as a function of applied normal load. The effect of tip size on adhesion and friction was explained as the influence of the capillary force exerted by meniscus and that of the contact area on these parameters respectively. The coefficient of friction was estimated in two different ways, as the slope from the plot of friction force against the applied normal load and as the ratio between the friction force and the applied normal load. Both these estimates showed that the coefficient of friction increased with the tip size. Further, the influence of the adhesion force on the coefficient of friction was also discussed.

키워드

참고문헌

  1. Bhushan, B., 'Nanoscale tribophysics and tribomechanics,' Wear 225229, pp. 465-492, 1999
  2. Bhushan, B., 'Tribology on the macro scale to nano scale of microelectromechanical system materials,' Proc Instn Mech Engrs, Vol. 215, Part J, IMech E 2001
  3. Maboudian, Roya and Howe, T. Roger., 'Critical Review: Adhesion in surface micromechanical structures,' J. Vac. Sci. Technol. B 15 (1), Vol. 15, No.1, Jan/Feb 1997
  4. Komvopoulos, K., 'Surface engineering and microtribology for microelectromechanical systems,' Wear 200, pp. 305-327, 1996
  5. Israelachvili, J. N. and Tabor, D., 'The measurement of van der Waals dispersion forces in the range 1.5 to 130 nm,' Proceedings of the Royal Society of London, A 331, pp. 1938, 1972
  6. Ando, Y. and Ino, J., 'Friction and pull-off forces on submicron-size asperities,' Wear Vol. 216, pp. 115-122, 1998 https://doi.org/10.1016/S0043-1648(97)00158-0
  7. Bhushan, B., 'Micro/nanotribology and its applications to magnetic storage devices and MEMS,' Tribology International Vol. 28, No.2, pp. 85-96, 1995 https://doi.org/10.1016/0301-679X(95)92698-5
  8. Bhushan, B, Kulkarni, A. V. and Koinkar, V. N., Langmuir Vol. 11, p. 3189, 1995 https://doi.org/10.1021/la00008a052
  9. Liu, Huiwen, Imad-Uddin Ahmed, S, Scherge, Matthias., 'Microtribological properties of silicon and silicon coated with diamond like carbon, octadecyltrichlorosilane and stearic acid cadmium salt films,' Thin Solid Films, Vol. 381, pp. 135-142, 2001 https://doi.org/10.1016/S0040-6090(00)01546-7
  10. Bhushan, B., Tribology and Mechanics of Magnetic Storage Devices, $2^{nd}$ edn. Springer-Verlag, New York, 1996
  11. Maboudian, Roya, Ashrust, Robert, W. and Carraro, Carlo., 'Tribological challenges in Micromechanical systems,' Tribology Letters Vol. 12, No.2, pp. 95-100, Feb 2002 https://doi.org/10.1023/A:1014044207344
  12. F. P. Bowden and D. Tabor, 'The Friction and Lubrication of Solids', Clarendon Press, Oxford, p-300, 1950
  13. Y. Sugwara, M. Ohta, T. Konishi, S. Morita, M. Suzuki and Y. Enomoto, 'Effects of humidity and tip radius on the adhesive force measured with atomic for microscopy', Wear 168, pp. 13-16, 1993 https://doi.org/10.1016/0043-1648(93)90191-N
  14. Bowden, F. P. and Tabor, D., Friction and Lubrication, Londone, Methuen, 1956
  15. Bhushan, B., Principles and Applications of Tribology, p.200, John Wiley & Sons Inc, 1998
  16. Carpick, R. W., Agrait, N, Ogletree, D. F. and Salmeron, M., J. Vac Sci. Technol. B14, p. 1289, 1996
  17. Enachescu, M, van den Oetelaar, R. J. A, Carpick, R. W., Ogletree, D. F., Flipse, C. F. and Salmeron, M., Phys. Rev. Lett 81, p. 1877, 1988 https://doi.org/10.1103/PhysRevLett.81.1877
  18. Enachescu, M, van den Oetelaar, R. J. A, Carpick, R. W., Ogletree, D. F., Flipse, C. F. and Salmeron, M., 'Observation of proportionality between friction and contact area at the nanometer scale,' Tribology Letters Vol. 7, pp. 73-78, 1999 https://doi.org/10.1023/A:1019173404538
  19. Johnson, K. L., Kendall, K. and Roberts, A. D., 'Surface energy and contact of elastic solid,' Proceedings of the Royal Society of London, A 324, pp. 301-313, 1971
  20. Yoon, Eui-Sung, Yang, Seung Ho, Han, Hung-Gu and Kong, Hosung, 'An experimental study on the adhesion at a nanocontact,', Wear Vol. 254, pp. 974-980, 2003 https://doi.org/10.1016/S0043-1648(03)00302-8
  21. Bhushan, B. and Sundarajan, S., 'MicrolNanoscale friction and wear mechanisms of thin films using Atomic Force and Friction Force Microscopy,' Acta mater. Vol. 46, No. 11, pp.3793-3804, 1998 https://doi.org/10.1016/S1359-6454(98)00062-7
  22. Skinner, J. and Gane, N., ' Sliding friction under negative load,' Journal of Physics D5, pp. 2087-2094, 1972