• Advances in nano research
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• v.1 no.4
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• pp.183-192
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• 2013

One-dimensional multiferroic nanostructured composites have drawn increasing interest as they show tremendous potential for multifunctional devices and applications. Herein, we report the synthesis, structural and dielectric characterization of barium titanate ($BaTiO_3$)-bismuth ferrite ($BiFeO_3$) composite fibers that were obtained using a novel sol-gel based electrospinning technique. The microstructure of the fibers was investigated using scanning electron microscopy and transmission electron microscopy. The fibers had an average diameter of 120 nm and were composed of nanoparticles. X-ray diffraction (XRD) study of the composite fibers demonstrated that the fibers are composed of perovskite cubic $BaTiO_3$-$BiFeO_3$ crystallites. The magnetic hysteresis loops of the resultant fibers demonstrated that the fibers were ferromagnetic with magnetic coercivity of 1500 Oe and saturation magnetization of 1.55 emu/g at room temperature (300 K). Additionally, the dielectric response of the composite fibers was characterized as a function of frequency. Their dielectric permittivity was found to be 140 and their dielectric loss was low in the frequency range from 1000 Hz to $10^7$ Hz.

• Advances in nano research
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• v.9 no.3
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• pp.193-210
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• 2020

In this research, beside presenting real images of produced Functionally Graded Carbon Nanotube-Reinforced Composites (FG-CNTRCs) and a brief review of the synthesis method of FG-CNTRCs, static and buckling analysis of FG-CNTRC with piezoelectric layers are investigated. It is assumed that the material properties of FG-CNTRC are varied through the thickness direction using four different distributions of Carbon Nanotubes (CNTs). To capture the size effects, nonlocal elasticity theory proposed by A.C. Eringen is also adopted in our model. One of the topics in our paper is using a higher order theory with eight different displacement fields and comparing their results with each other. To solve the governing equations, an analytical method is used to find the deflections and critical buckling loads of FG-CNTRCs. To show the accuracy of present methodology, our results are compared with the results of simply supported rectangular nano plates available in the literature. In this research, the effects of aspect ratio, piezoelectric layer and nonlocal parameter are also studied. It is hoped that this work leads to more accurate models on FG-CNTRC.

• Proceedings of the KIEE Conference
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• 2011.07a
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• pp.2152-2153
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• 2011

According to a sharp increase in demand for electricity supply secure, and $CO_2$ regulation in accordance with global environmental problems and to solve problems, etc. These factor less pollution, higher energy conversion hyoyulin way that the new electrical equipment, nano-composites The rapid degeneration of the unit study utilizing the power that is required is Free. Accordingly, cables, transformers and switchgear (GIS)-capacity of power equipment, such as, high-voltage high-density along with the miniaturization of equipment have made angry the reliability of these devices is becoming a very important issue. Insulation materials used in electrical equipment for high voltage withstand, power equipment, power equipment due to aging and overloading caused by a weakening of the insulation failure and replacement in accordance with the age due to increased costs because of the reliability of electrical equipment should be secured should. Therefore, improved performance and longevity of insulation material is recognized as an important challenge. In this study, power isolation and degeneration of the unit for use in various parts of the molding epoxy resin to improve the insulation performance of the epoxy resin by varying the added amount of nano-SiO2 nanocomposites made epoxy/SiO2 analysis and breakdown properties of the experiment want to improve the electrical properties through the geometry.

• Proceedings of the KIEE Conference
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• 2009.07a
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• pp.1378_1380
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• 2009

절연파괴 강도에대한 특성분석을 위해 와이블 plot을 이용하였다. ENMMC에서 실란처리와 미처리특성에서 실란처리된 결과 형상파라미터가 상대적으로 높은 값을 나타내었다. 이는 절연파괴결과가 균질함을 분명하게 나타낸 결과이다. 또한 스케일파리미터에서도 처리된 결과가 상대적으로 높은 결과를 보이고 있다. 나노입자 충진함량에 대한 효과에서도 체적비로 6.2vol%가 24.87vol%보다 월등하게 높은 형상파리미터와 스케일 파리미터를 나타내었다. 현장에서는 B10의 수명이 누적확률(63.2%)보다 오히려 유효한 평가자료 라고 사료된다. 역시 실란처리 된 결과가 미처리된 것에 비하여 그리고 나노입자 충진함량이 적을수록 높은 결과를 나타내었다. 이로서 중전기기 산업절연재료로서 향후 전망을 크게 할 것으로 본다.

• Journal of the Korean Society for Heat Treatment
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• v.16 no.6
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• pp.311-314
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• 2003

In Mo-Xwt%Cu compound, Physical and thermal properties were systematically evaluated in terms of Cu contents and sintering temperature. Typically Cu contents were varied from 15 to 25wt% and also the Sintering temperatures were changed from $1115^{\circ}C$ to $1350^{\circ}C$. In physical properties, Mo-15~25wt%Cu has the maximum density of 95% while Mo-20wt%Cu has the maximum thermal conductivity of 165.179[${\mu}/m^{\circ}C$] at sintering temperature of $1300^{\circ}C$. Especially, Mo-25wt%Cu has the maximum hardness of 173.4 at sintering temperature of $1150^{\circ}C$ and the maximum thermal expansion of 9.0[W/mK] as the specimen heated in the range of temperature from $50^{\circ}C$ to $400^{\circ}C$. Based on electrical conductivity measurements, the relative density increased within creasing Cu contents and the values were in the range of 100~150[W/mK].

• Korean Journal of Materials Research
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• v.26 no.10
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• pp.521-527
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• 2016

Geopolymers have many advantages over Portland cement, including energy efficiency, reduced greenhouse gas emissions, high strength at early age and improved thermal resistance. Alkali activated geopolymers made from waste materials such as fly ash or blast furnace slag are particularly advantageous because of their environmental sustainability and low cost. However, their durability and functionality remain subjects for further study. Geopolymer materials can be used in various applications such as fire and heat resistant fiber composites, sealants, concretes, ceramics, etc., depending on the chemical composition of the source materials and the activators. In this study, we investigated the thermal properties and microstructure of fly ash and blast furnace slag based geopolymers in order to develop eco-friendly construction materials with excellent energy efficiency, sound insulation properties and good heat resistance. With different curing times, specimens of various compositions were investigated in terms of compressive strength, X-ray diffraction, thermal property and microstructure. In addition, we investigated changes in X-ray diffraction and microstructure for geopolymers exposed to $1,000^{\circ}C$ heat.

• Carbon letters
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• v.6 no.3
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• pp.181-187
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• 2005

Bipolar plates require some specific properties such as electrical conductivity, mechanical strength, chemical stability, and low permeability for the fuel cell application. This study investigated the effects of carbon nanotube (CNT) contents and process conditions of hot press molding on the electrical and physical properties using CNT 3~7 wt% added graphite nano-composites in the curing temperatures range of 140~$200^{\circ}C$ and pressure of 200~300 kg/$cm^2$. Bulk density, hardness and flexural strength increased with increasing CNT contents, curing pressure and temperature. With the 7 wt% CNT added noncomposite, the electrical resistance improved by 30% and the flexural strength increased by 25% as compared to that without CNT at the temperature of $160^{\circ}C$ and pressure of 300 kg/$cm^2$. These properties were close to the DOE reference criteria as bulk resistance of 13 $m{\Omega}cm$ and tensile strength of 515 kg/$cm^2$.

• Transactions of Materials Processing
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• v.26 no.4
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• pp.216-221
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• 2017

Recently, interest in multifunctional energetic structural materials (MESMs) has grown due to their multifunctional potential, especially in military applications. However, there are few studies about extrinsic factors that govern the reactivity of MESMs. In this paper, a shock compaction process was performed on the nano Ni/Al-mixed powder to investigate the effect of particle size on the shock reaction condition. Additionally, heating the statically compacted specimen was also performed to compare the mechanical properties and microstructure between reacted and unreacted material. The results show that the agglomerated structure of nanopowders interrupts the reaction by reducing the elemental boundary. X-ray diffraction analysis shows that the NiAl and $Ni_3Al$ intermetallics are formed on the reacted specimen. The microhardness results show that the $Ni_3Al$ phase has a higher hardness than NiAl, but the portion of $Ni_3Al$ in the reacted specimen is minor. In conclusion, using Ni/Al composites as a reactive material should focus on energetic use.

• Journal of Powder Materials
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• v.8 no.3
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• pp.157-162
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• 2001

An optimum route to fabricate the ferrous alloy dispersed $Al_2O_3$ nanocomposites such as $Al_2O_3$/Fe-Ni and $Al_2O_3$/Fe-Co with sound microstructure and desired properties was investigated. The composites were fabricated by the sintering of powder mixtures of $Al_2O_3$ and nano-sized ferrous alloy, in which the alloy was prepared by solution-chemistry routes using metal nitrates powders and a subsequent hydorgen reduction process. Microstructural observation of reduced powder mixture revealed that the Fe-Ni or Fe-Co alloy particles of about 20 nm in size homogeneously surrounded $Al_2O_3$, forming nanocomposite powder. The sintered $Al_2O_3$/Fe-Ni composite showed the formation of Fe$Al_2O_4$ phase, while the reaction phases were not observed in $Al_2O_3$/Fe-Co composite. Hot-pressed $Al_2O_3$/Fe-Ni composite showed improved mechanical properties and magnetic response. The properties are discussed in terms of microstructural characteristics such as the distribution and size of alloy particles.

• Journal of Powder Materials
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• v.27 no.3
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• pp.203-209
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• 2020

The automotive industry has focused on the development of metallic materials with high specific strength, which can meet both fuel economy and safety goals. Here, a new class of ultrafine-grained high-Mn steels containing nano-scale oxides is developed using powder metallurgy. First, high-energy mechanical milling is performed to dissolve alloying elements in Fe and reduce the grain size to the nanometer regime. Second, the ball-milled powder is consolidated using spark plasma sintering. During spark plasma sintering, nanoscale manganese oxides are generated in Fe-15Mn steels, while other nanoscale oxides (e.g., aluminum, silicon, titanium) are produced in Fe-15Mn-3Al-3Si and Fe-15Mn-3Ti steels. Finally, the phases and resulting hardness of a variety of high-Mn steels are compared. As a result, the sintered pallets exhibit superior hardness when elements with higher oxygen affinity are added; these elements attract oxygen from Mn and form nanoscale oxides that can greatly improve the strength of high-Mn steels.