• 제목/요약/키워드: mixture experimental design

검색결과 300건 처리시간 0.025초

복합열화 환경을 받는 콘크리트 시설물을 위한 보수용 폴리머 시멘트 복합체의 내구성능 향상에 관한 연구 (Enhanced Durability Performance of Polymer Modified Cement Composites for Concrete Repair Under Combined Aging Conditions)

  • 원종필;박찬기
    • 한국농공학회논문집
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    • 제47권6호
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    • pp.27-34
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    • 2005
  • The purpose of this study is to improve the durability performance of polymer modified cement composites for repair of concrete under combined aging conditions. The experimental procedure was divided into three parts. First, the replacement level of mineral admixtures in polymer modified cement composites were determined in an experimental study based on a Box Behnken design. Second, the flow value, compressive strength and chloride permeability test of sixteen types of mixtures were conducted. Test results show that the polymer modified cement composites were effected on the improvement of the compressive strength and permeability performance. Third, the effects on the replacement level of silica fume mixture was evaluated by the compressive strength, chloride permeability, chemical resistance and repeated freezing and thawing cycles test. They demonstrated that the polymer modified cement composites using mixture of silica fume, fly ash, and blast furnace slag improved the durability performance.

혼합물실험계획법을 이용한 2차전지의 최적설계 (An Optimum Design of Secondary Battery Using Design of Experiments with Mixture)

  • 김성준;박종인
    • 한국경영과학회:학술대회논문집
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    • 한국경영과학회/대한산업공학회 2005년도 춘계공동학술대회 발표논문
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    • pp.983-989
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    • 2005
  • Secondary batteries with high performance are essential in widespread use of modern portable devices such as cellular phones and laptop computers. High energy density, long cycle life, and safety are some of important requirements for secondary battery. To achieve such characteristics, a mixing proportion of electrolyte solution ingredients in the battery should be carefully chosen. In this paper, using statistical design of mixture experiments (DOME), we attempt to find an optimum condition of designing the secondary battery. DOME has a distinct feature in that the experimental region is represented by simplex, rather than hypercube, because the sum of blend proportions should be unity. Several designs based upon this point have been proposed for mixture experiments. Among them, an extreme vertices design is employed in this paper because there are a couple of blend constraints to be considered. In order to investigate how the mixing proportion interacts with other manufacturing factors, a fractional factorial design is also included across the extreme vertices design. As a result, we find that the blend proportion of solution ingredients has a significant effect on battery performances. By simultaneously optimizing two battery capacities, this paper proposes an optimum blend proportion according to process factor settings.

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혼합물 실험계획법을 이용한 OH라디칼 최적 생성을 위한 삼성분 전극의 비율 선정 (Using Design of Mixture Experiments to Select the Ratio of a Three-Component Electrode for Optimal Generation of Hydroxyl Radicals)

  • 박영식
    • 한국환경과학회지
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    • 제29권8호
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    • pp.793-800
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    • 2020
  • The conventional development of multi-component electrodes is based on the researcher's experience and is based on trial and error. Therefore, there is a need for a scientific method to reduce the time and economic losses thereof and systematize the mixing of electrode components. In this study, we use design of mixture experiments (DOME)- in particular a simplex lattice design with Design Expert program- to attempt to find an optimum mixing ratio for a three-component electrode for the high RNO degradation; RNO is an indictor of OH radical formation. The experiment included 12 experimental points with 2 center replicates for 3 different independent variables (with the molar ratio of Ru, Ti, Ir). As the Prob > F value of the 'Quadratic' model is 0.0026, the secondary model was found to be suitable. Applying the molar ratio of the electrode components to the corrected response model results is an RNO removal efficiency (%) = 59.89 × [Ru] + 9.78 × [Ti] + 67.03 × [Ir] + 66.38 × [Ru] × [Ir] + 132.86 × [Ti] × [Ir]. The R2 value of the equation is 0.9374 after the error term is excluded. The optimized formulation of the ternary electrode for an high RNO degradation was acquired when the molar ratio of Ru 0.100, Ti 0.200, Ir 0.700 (desirability d value, 1).

혼합실험계획법에 의한 율무와 밀가루의 압출성형 최적 배합 조건 설정 (Determination of the Optimal Mixture Ratio for Extrudates of Job's-tear and Wheat Flour by Mixture Design Analysis)

  • 조석철;강병선
    • 한국식품과학회지
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    • 제45권4호
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    • pp.473-477
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    • 2013
  • 혼합디자인에 의해 설정된 조건하에서 압출성형한 율무와 밀가루의 압출성형물은 율무 첨가에 대해 여러 반응 요인들이 압출성형물의 특성에 영향을 끼치는 것으로 나타났다. 실험조건은 율무 함량 5-75%, 밀가루 25-95%로 결정하였으며, 수분함량은 20.55%로 고정하여 modified distance based mixture design으로 실험설계 및 분석하였다. Bending 파손강도, WAI, a값 등은 유의성이 없는 것으로 나타났으나, 팽화물의 직경, WSI, L값, b값은 율무와 밀가루의 혼합에 의해 유의성이 존재하는 것으로 나타났다. 팽화물의 직경, L값, b값은 선형 모델로 분석할 수 있었으나 WSI는 quadratic 모델로만 설정이 가능한 것으로 나타났다. 율무의 함량이 많아질수록 외관적으로 팽창되어지는 정도가 적어졌으며, 색상도 어두워지는 것으로 나타났다. 율무의 함량이 증가할수록 L값은 77.84에서 72.73, a값은 1.37에서 1.77로, b값은 19.42에서 17.64로 이동되었다. WSI는 율무와 밀가루가 40%:60%로 혼합되어 압출성형되었을 때 가장 낮게 나타났으며, WAI는 율무와 밀가루 혼합 비율에 대해서는 유의성이 없는 것으로 나타났다. 혼합디자인 계획법은 시리얼류 제품 생산에 적합한 조직 형성과 반응량에 유의한 영향을 미치는 요인 등에 대해 적절한 혼합 비율과 가공 조건 등을 제시할 수 있음을 알 수 있었다. Modified distance based mixture design에 의해, 일반 시중 제품과 유사한 조직감을 나타낼 수 있는 율무와 밀가루, 물의 적정 배합 비율은 60.12:19.42:20.46으로 나타났다.

루틴, 퀘르세틴, 식이섬유 혼합물 설계를 이용한 전분소화 지연 효과의 최적화에 대한 융합 연구 (Convergence Study on the Optimization for Suppression of Starch Hydrolysis using Rutin, Quercetin and Dietary Fiber Mixture Design)

  • 오임경;배인영
    • 한국융합학회논문지
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    • 제11권5호
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    • pp.35-41
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    • 2020
  • 본 연구는 루틴, 퀘르세틴, 식이섬유가 전분 소화율에 미치는 영향을 통계적 혼합물 설계방법을 이용하여 확인하고자 하였다. 세 가지 성분들은 모두 농도가 증가함에 따라 전분소화 지연 효과가 나타났으며, 그 중에서도 퀘르세틴과 식이섬유가 함께 섞였을 때 가장 높은 지연 효과를 보였다. 이 혼합물 설계는 simplex-centroid 실험설계법을 이용하였고, 최적 모델은 quadratic 모델에서 나타났다. 이때 얻어진 회귀방정식을 통하여 유의한 상승효과를 확인할 수 있었다. 최적화 통계 방법을 사용하여 혼합비를 분석한 결과 퀘르세틴과 식이섬유가 72: 28 비율에서 전분 소화 지연 효과가 최대로 나타나는 것을 확인하였다. 전분소화에 대한 영향을 3차원 표면 도표로 시각화하여 나타내었으며, 이 결과로 퀘르세틴과 식이섬유의 상호작용으로 인하여 전분 소화를 15% 이상 지연시키는 것을 확인할 수 있었다.

아스팔트 콘크리트에 적정 폐비닐 첨가량 결정에 관한 실험적 연구 (Experimental Study for Determination of Optimum Waste Vinyl Contents in Asphalt Concrete)

  • 김광우;김주인;이순제;최선주
    • 한국농공학회지
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    • 제44권5호
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    • pp.88-95
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    • 2002
  • This study is a fundamental research for recycling waste vinyl (WV) in asphalt mixture for improving roadway pavement. Mix design was conducted by WV content and optimum asphalt content (OAC) was determined for dense-graded surface course mixture. Marshall stability test, indirect tensile strength (ITS) test and wheel tracking test were carried out to measure the characteristics of WV-added asphalt concretes. From the results of this study, recycling WV in asphalt mixture is possible. However, as WV content increased, melted WV clustering appeared in asphalt mixture. It could be considered that adding too much WV in asphalt mixture is not proper. The proper content of LDPE and HDPE WV was appeared to be 12% and 8%, respectively.

연약지반 표층안정처리를 위한 고화재의 최적조합 산정에 관한 실험적 연구 (An Experimental Study on Optimal Mixture Ratio of Hardening Agent for Surface Soil Stabilization)

  • 천병식;김진춘;최현석
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 가을 학술발표회 논문집
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    • pp.17-24
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    • 2000
  • Hardening agent has been the traditional material for surface soil stabilization of soft ground. This study aims at determining optimal mixture ratio of hardening agent in accordance with the required design specifications. Hardening agent is properly mixtured with Fly ash, Gypsum, Slag and Cement for the ettringite hydrates which is effective for early stabilization of unconsolidated soil. The treated soil is the clay which are widely found here and there in Korea. In this study, preliminary tests were performed to get optimal mixture ratio of stabilizer ingredient, and marine clay in Jin-Hae was used to get physical and chemical properties. Laboratory tests of 50 stabilized soil were peformed to get optimal mixture ratio for 16 stabilizer material of 6 type, and stabilizer mixing was determined.

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합성목재의 난연성 확보를 위한 혼합물 실험계획 사례 (A Case Study of Applying Mixture Experimental Design to Enhance Flame Retardancy of Wood-Plastic Composites)

  • 서호진;권민서;이건명;주혜진;변재현
    • 품질경영학회지
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    • 제50권1호
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    • pp.169-181
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    • 2022
  • Purpose: This paper addresses a case study of developing a flame retardant wood-plastic composites (WPC) by adding tannic acid to the existing synthetic wood. The optimal mixing ratios of six components are explored to minimize the burning time using two mixture designs. Methods: In the preliminary experiment, six components are considered to find important components and their ranges. Seven D-optimal mixture design points are generated. Two points are removed for the balance of plastic components to be maintained, and the remaining five points are augmented with two basic compositions. Four components are selected to be considered in the main experiment. In the main experiment, pellets are extruded at the eight mixture design points. In-house testing of burning time is executed three times. Specimens made of pellets from two promising flame retardant compositions are sent to the accredited laboratories and tested. Results: The test results are as follows: 1) The best composition (Wood flour, Tannic acid, PE, Lubricant) = (25, 41, 10, 2) (wt%) shows the burning time of 1 second, which is 9-fold improvement compared to the the burning time of 9 seconds from the existing composition (58, 0, 10, 2) (wt%). 2) The second best composition (41, 25, 10, 2) (wt%) results in the burning time of 2 seconds. This composition is inferior to the best composition in terms of the flame retardancy, but more economical since it needs less tannic acid which is 100-fold expensive than the wood flour. Conclusion: Flame retardant compositions are found by adding tannic acid to the existing WPC employing optimal mixture designs. This case study will be helpful to practitioners who try to develop new products with additional physical properties with as small number of experimental trials as possible. Future research direction includes exploring conditions which satisfy both performance level and cost limitation simultaneously.

피로수명을 고려한 1 MW급 수평축 풍력터빈 복합재 블레이드 설계에 관한 연구 (A Study on Composite Blades of 1 MW Class HAWT Considering Fatigue Life)

  • 김민웅;공창덕;박현범
    • 한국항공우주학회지
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    • 제40권7호
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    • pp.564-573
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    • 2012
  • 새롭게 제안된 공력 설계 절차와 In-house 프로그램을 이용하여 1 MW급 수평축풍력 터빈 블레이드의 형상을 결정하였고, 기존에 개발된 블레이드의 실험 결과와 본 연구에서 제안한 블레이드와의 비교를 통하여 공력 설계에 대한 타당성을 제시하였다. 블레이드의 구조 설계는 Netting Rule과 Rule of Mixture를 적용하여 설계를 진행하였다. 설계된 블레이드의 구조적 안전성은 상업적 유한요소프로그램인 MSC.NASTRAN을 사용하여 다양한 하중에 따라 선형 정적해석, 변형해석, 좌굴해석, 진동모드해석 등을 수행하였다. 최종적으로 Spera가 제시한 실험식을 적용하여 요구된 피로수명에 대해 타당성을 확인하였다.

혼합물 실험계획법에 의한 황도복숭아 드레싱 재료혼합비의 최적화 (Mixutre Optimization of Hwangdo Peach (Prunus persica L. Batsch) Dressing by Mixture Experimental Design)

  • 박정은;김용식
    • 한국조리학회지
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    • 제23권7호
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    • pp.20-30
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    • 2017
  • This study was conducted for the optimization of ingredients in salad dressing using Hwangdo peach (Prunus persica L. Batsch). The experiment was designed according to the D-optimal design of mixture design, which included 14 experimental points with 4 replicates for three independent variables (olive oil 40~65%, peach puree 27~50%, vinegar 8~20%). The linear regression models for pH, viscosity and color value and the quadratic regression models for emulsion stability, all sensory evaluation of the products were proven to be valid by the F-test for the overall significance of the regression model at a 5% level. Viscosity and pH of the products increased as olive oil content. Color value, viscosity and pH of the products increased as peach puree content. pH, viscosity, redness, and yellowness of the products decreased as vinegar content. Sensory evaluation result of the products showed that general preference for the products were increasingly affected by the increases in contents then decreased as they exceeded the optimum levels. In consequence, according to result from the first stage of the experiment, the optimum ingredients ratios of the raw materials were set in olive oil 52.43%, peach puree 35.07%, and vinegar 13.91% for ingredients of apricot dressing. These results provided the possibility that peach can be applied to the preparation of a dressing, and thereby present baseline data for the development of new dressings. This is also presumed to meet demands of customers who are always in pursuit of new products.