• Title/Summary/Keyword: mixture experimental design

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Robust Designs of the Second Order Response Surface Model in a Mixture (2차 혼합물 반응표면 모형에서의 강건한 실험 설계)

  • Lim, Yong-Bin
    • The Korean Journal of Applied Statistics
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    • v.20 no.2
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    • pp.267-280
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    • 2007
  • Various single-valued design optimality criteria such as D-, G-, and V-optimality are used often in constructing optimal experimental designs for mixture experiments in a constrained region R where lower and upper bound constraints are imposed on the ingredients proportions. Even though they are optimal in the strict sense of particular optimality criterion used, it is known that their performance is unsatisfactory with respect to the prediction capability over a constrained region. (Vining et at., 1993; Khuri et at., 1999) We assume the quadratic polynomial model as the mixture response surface model and are interested in finding efficient designs in the constrained design space for a mixture. In this paper, we make an expanded list of candidate design points by adding interior points to the extreme vertices, edge midpoints, constrained face centroids and the overall centroid. Then, we want to propose a robust design with respect to D-optimality, G-optimality, V-optimality and distance-based U-optimality. Comparing scaled prediction variance quantile plots (SPVQP) of robust designs with that of recommended designs in Khuri et al. (1999) and Vining et al. (1993) in the well-known examples of a four-component fertilizer experiment as well as McLean and Anderson's Railroad Flare Experiment, robust designs turned out to be superior to those recommended designs.

Optimization of the formulation for manufacturing of Bokbunja (Rubus coreanus Miquel)-black mulberry (Morus alba) herbal pill by D-optimal mixture design approach (D-optimal mixture design 이용 복분자-오디 환 제조 배합비 최적화)

  • Moon, Jin-Young;Hwang, Su-Jung;Eun, Jong-Bang
    • Korean Journal of Food Science and Technology
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    • v.53 no.2
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    • pp.174-180
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    • 2021
  • The optimal recipe for manufacturing composite honey-based herbal pills mainly comprising Rubus coreanus powder (RCP), black mulberry powder (BMP), and vitamin C was investigated. Honey-based herbal pills were prepared by mixing these powders, binding them with honey, and then forming a round shape. The experiment was designed based on the D-optimal mixture design, which included 12 experimental points with one replicate for three independent variables as follows: RCP (10~35%), BMP (10~35%), and vitamin C (5~10%). In addition, the dependent variables (total phenolic and flavonoid content and antioxidant activity) were measured and used to optimize the manufacturing conditions. The results showed that high amounts of RCP were correlated with high total flavonoid content, whereas the addition of high amounts of vitamin C resulted in higher antioxidant activity. In conclusion, an optimized formulation for the honey-based herbal pill was found to contain 35% RCP, 10% BMP, and 10% vitamin C.

An Experimental Study about Tractive Performance of Tracked Vehicle on Deep-sea Soft Sediment Based on Design of Experiment Using Orthogonal Array (직교배열표 실험계획법에 의한 심해 연약지반용 무한궤도차량의 견인성능에 대한 실험적 연구)

  • Choi, Jong-Su;Hong, Sup;Kim, Hyung-Woo;Lee, Tae-Hee
    • Ocean and Polar Research
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    • v.26 no.2
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    • pp.333-339
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    • 2004
  • This paper is concerned with an experimental investigation about tractive performance of a tracked vehicle on extremely soft soil. A tracked vehicle model with principal dimensions of $0.9\;m(L)\;{\times}\;0.75\;m(B)\;{\times}\;0.4\;m(H)$ and the weight of 167 kg was constructed with a pair of driving chain links driven by two AC-servo motors. The tracks are configured with detachable grousers with variable span. Deep seabed was simulated by means of bentonite-water mixture in a soil bin of $6.0\;m(L)\;{\times}\;3.7\;m(B)\;{\times}\;0.7\;m(H)$. Slip of vehicle and driving torque of motor were measured with respect to experimental variables; grouser span, grouser chevron angle, driving speed, drawbar-pull weight, position of center-of-gravity and weight. $L_8$ orthogonal array is adopted for DOE (Design Of Experiment). The effects of experiment variables on traction performance are evaluated.

Influence of Molding Conditions on Environmental Stress Cracking Resistance of Injection Molded Part (사출성형품의 공정 조건에 따른 내환경응력균열 특성에 관한 연구)

  • Choi, D.S.;Kim, H.S.
    • Transactions of Materials Processing
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    • v.20 no.2
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    • pp.173-178
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    • 2011
  • Environmental Stress Cracking(ESC) is one of the most common causes of unexpected brittle failure of thermoplastic polymers. The exposure of polymers to liquid chemicals tends to accelerate the crazing process, initiating crazes at stresses that are much lower than the stress causing crazing in air. In this study, ESC of acrylonitirile butadiene styrene(ABS) was investigated as a function of the molding conditions such as injection velocity, packing pressure, and melt temperature. A constant strain was applied to the injection molded specimens through a 1.26% strain jig and a mixture of toluene and isopropyl alcohol was used as the liquid chemical. In order to examine the effects of the molding conditions on ESC, an experimental design method was adopted and it was found that the injection velocity was the dominant factor. In addition, predictions from numerical analyses were compared with the experimental results. It was found that the residual stress in the injection molded part was associated with the environmental stress cracking resistance (ESCR).

Control of Shrinkage Cracking of Cement Composites with Different Length Mixture of PVA Fibers (서로 다른 길이의 PVA 섬유 혼합에 따른 시멘트 복합체의 균열제어 특성)

  • Won, Jong-Pil;Kim, Myung-Kyun;Park, Chan-Gi;Kim, Wan-Young;Park, Kyoung-Hoon;Jang, Chang-Il
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.405-408
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    • 2006
  • The purpose of this study was to determine the optimum length distribution of hybrid PVA(Poly vinyl alcohol) fiber. To produce blended PVA fiber length, first the length distribution of PVA fiber in the cement composites were identified in an experimental study based on simplex lattice design. Among the different length distributions investigated, fiber length was found to have statistically significant effect on plastic shrinkage cracking of cement composites. Subsequently, Complex analysis techniques were used to devise an experimental program that helped determine the optimum combinations of the selected fiber length distribution based on plastic shrinkage crack. The optimum blended PVA length ratio was 0.0146% 4mm fiber, 0.0060% 6-mm fiber, 0.0285% 8-mm fiber, and 0.0209% 12-mm fiber.

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Optimization of Makgeolli Manufacture Using Several Sweet Potatoes (다양한 고구마를 이용하여 제조한 막걸리의 최적화)

  • Cheon, Ji-Eun;Baik, Moo-Yeol;Choi, Sung-Won;Kim, Chang-Nam;Kim, Byung-Yong
    • The Korean Journal of Food And Nutrition
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    • v.26 no.1
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    • pp.29-34
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    • 2013
  • The objective of this study was to manufacture three kinds of domestic sweet potato Makgeolli using a mixture design and an optimization technique. The effects of four different manufacture methods, such as simultaneous saccharification and fermentation (SSF) with or without malt and separate hydrolysis and fermentation (SHF) with or without malt were determined. The SSF methods of Makgeolli produced higher alcohol content than that of SHF methods. The sensory score was not influenced by different making methods. Fourteen experimental points were selected, and rice (10~50%), sweet potato (10~50%) and water (40~60%) were chosen as independent variables. The measured responses were sensory preference, total polyphenol content, and DPPH radical scavenging activities. The ratio of the optimum sweet potato Makgeolli mixture formulation was developed as 15.11 (rice): 44.89 (sweet potato): 40 (water) using the optimization technique. The desirability of the optimum mixture formulation was 0.839. Yellow sweet potato Makgeolli using the optimum mixture formulation produced higher soluble sugar content compared to others. Regular sweet potato Makgeolli produced higher pH. The purple sweet potato Makgeolli's total polyphenol content and DPPH radical scavenging activity were measured to be the highest at $771.91{\pm}1.42mg\;GAE/{\ell}$, $131.55{\pm}4.03%$.

A Comparative Study of Dry Matter Yield and Nutritive Value of Tall type and Turf type Mixtures (상번초 및 잔디형 혼파초지의 건물수량과 사료가치 비교 연구)

  • Lee, Hyung-Suk;Lee, In-Duk
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.26 no.4
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    • pp.221-226
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    • 2006
  • This study was conducted to investigate the effect of tall type mixtures and turf type mixtures on dry matter yield, botanical composition and quality. The experimental design includes two mixture types : Tall type mixtures; orchardgrass (Potomac) 50+tall fescue (Fawn) 20+ Kentucky bluegrass (Kenblue) 10+red clover (Kenland) 20%) and turf type mixtures; Kentucky bluegrass(Newport) 60%+tall fescue (reboil Jr.) 20+perennial ryegrass (palmer II) 20%. The DM yield was higher obtained in tall type mixture than that of turf type mixture (p<0.05). In the chemical composition, Turf type mixture was higher in crude protein (CP) and dry matter digestibility (DMD), but lower in fibrous compound as NDF, ADF, cellulose and lignin than those of tall type mixture (p<0.05). The crude protein dry matter (CPDM) and digestible dry matter (DDM) yield was higher in tall type mixture than turf type mixture (p<0.05). In this experiment, nutritive value of turf type mixture was higher than that of tall type mixture, but CPDM and DDM yield of turf type mixture were lower than that of turf type mixture due to low dry matter yield. On the other hand, turf type mixture was obtained high feed value, and maintaining the various botanical composition on the 13 th cutting frequency condition. therefore, turf type mixture had a utilization possibility under grazing livestock as sheep and milk goats.

Optimization of Ingredient Mixing Ratio for Preparation of Steamed Foam Cake with Barley (Hordeum vulgare L.) Sproutling Powder (어린보릿가루 첨가 거품형 찜케이크의 재료 혼합비율의 최적화)

  • Seo, Min-Ja;Jung, Su-Ji;Jang, Myung-Sook
    • Korean journal of food and cookery science
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    • v.22 no.6 s.96
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    • pp.815-824
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    • 2006
  • This study was performed to determine the optimum ratio of each ingredient in the steamed foam cake with barley (Hordeum vulgare L.) sproutling powder. The experiment was designed according to the D-optimal design of mixture design, which showed 14 experimental points including 4 replicates for three independent variables (sugar 112${\sim}$139%, barley sproutling powder 1${\sim}$8%, and oil 5${\sim}$25%). The compositional and functional properties of test were measured, and these values were applied to the mathematical models. A canonical form and trace plot showed the influence of each ingredient on the mixture final product. The results of F-test, volume, color values (L, a, b), textural properties (hardness, gumminess, chewiness) and sensory characteristics (softness) decided a linear model, while the sensory characteristics (color, smell, taste, overall acceptance) decided a quadratic model. The volume of steamed foam cake was increased by sugar addition, and a negative effect was exerted by barley sproutling powder and oil. L and a of color values increased but the b value decreased with increasing sugar and oil content, whereas barley sproutling powder tended to decrease all color values. The addition of barley sproutling powder also had a positive effect on the textural properties (hardness, gumminess, chewiness). Sensory characteristics (color, smell, softness, taste, overall acceptance) could suffer counter results with the excessive addition of sugar, barley sproutling powder, and oil. The optimum formulations by numerical and graphical methods were similar: sugar, barley sproutling powder, and oil were 130.4%, 4.0%, and 10.7% by numerical method, compared to 130.4%, 4.0%, and 10.7% by graphical method, respectively.

Analysis of Powder Packing for Alumina Using Design of Experiment with Mixture and Vibration (혼합물실험계획법과 가진을 이용한 알루미나 파우더의 충진율 분석)

  • Jeon, Sangjun;Kim, Youngshin;Yang, Daejong
    • Composites Research
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    • v.34 no.5
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    • pp.330-336
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    • 2021
  • Alumina powder is one of the widely used materials for industry, but there is a problem that the strength of the product changes depending on the powder packing state. To solve the above problem, previous studies have been conducted to increase the particle packing efficiency, but most of the existing studies analyzed the packing characteristics of millimeter-scale particles, so the physical properties are different from those of the micrometer scale. It is difficult to apply to the micrometer scale. In this paper, a three-step experiment was performed using a statistical method to increase packing using micrometer-scale alumina powder. First, a size combination with high packing and a mixing ratio were selected using the mixture test design method, and an appropriate excitation frequency was selected by analyzing the height change according to the frequency change in the vibration test apparatus. Finally, an alumina powder packing experiment was performed based on the experimental results mentioned above. As a result, it was confirmed that the maximum height variation was 42% higher than the maximum value of the 155 measurements performed when selecting the packing size combination. It is thought that this study will serve as basic data for processing and packing research using fine powder.

An Experimental Study on the Mix Properties of Concrete Pavement Incorporating Fly-Ash (플라이애쉬를 혼입한 콘크리트포장의 배합특성에 관한 실험적 연구)

  • Lee, Joo-Hyung;Choi, Seong-Yung;Yun, Kyong-Ku;Jung, Young-Hwa
    • Journal of Industrial Technology
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    • v.17
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    • pp.313-322
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    • 1997
  • As the weight of trucks increases, the need for concrete pavement also increases. Therefore, the addition of fly-ash may improve the properties of pavement concrete as well as recycle fly-ash. A full factorial experiment was performed using the primary variables, such as water-cement ratio, fly-ash substitution ratio, and maximum size of coarse aggregate, as a preliminary study for optimum mixture design for pavement concrete. The results of preliminary study indicates that the addition of fly-ash is the most important factor determining concrete strength, followed by the maximum size of coarse aggregate and water-cement ratio. It, also, shows the relative importance of fly-ash substitution ratio, compared to the water-cement ratio, and the interaction effects between the primary variables. Optimum mixture designs for pavement concrete incorporating fly-ash, that satisfied the target responses, were proposed in terms of fly-ash substitution ratio, water cement ratio and maximum size of coarse aggregate.

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