• Title/Summary/Keyword: mixture experimental design

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Enhanced Durability Performance of Polymer Modified Cement Composites for Concrete Repair Under Combined Aging Conditions (복합열화 환경을 받는 콘크리트 시설물을 위한 보수용 폴리머 시멘트 복합체의 내구성능 향상에 관한 연구)

  • Won, Jong-Pil;Park, Chan-Gi
    • Journal of The Korean Society of Agricultural Engineers
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    • v.47 no.6
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    • pp.27-34
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    • 2005
  • The purpose of this study is to improve the durability performance of polymer modified cement composites for repair of concrete under combined aging conditions. The experimental procedure was divided into three parts. First, the replacement level of mineral admixtures in polymer modified cement composites were determined in an experimental study based on a Box Behnken design. Second, the flow value, compressive strength and chloride permeability test of sixteen types of mixtures were conducted. Test results show that the polymer modified cement composites were effected on the improvement of the compressive strength and permeability performance. Third, the effects on the replacement level of silica fume mixture was evaluated by the compressive strength, chloride permeability, chemical resistance and repeated freezing and thawing cycles test. They demonstrated that the polymer modified cement composites using mixture of silica fume, fly ash, and blast furnace slag improved the durability performance.

An Optimum Design of Secondary Battery Using Design of Experiments with Mixture (혼합물실험계획법을 이용한 2차전지의 최적설계)

  • Kim, Seong-Jun;Park, Jong-In
    • Proceedings of the Korean Operations and Management Science Society Conference
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    • 2005.05a
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    • pp.983-989
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    • 2005
  • Secondary batteries with high performance are essential in widespread use of modern portable devices such as cellular phones and laptop computers. High energy density, long cycle life, and safety are some of important requirements for secondary battery. To achieve such characteristics, a mixing proportion of electrolyte solution ingredients in the battery should be carefully chosen. In this paper, using statistical design of mixture experiments (DOME), we attempt to find an optimum condition of designing the secondary battery. DOME has a distinct feature in that the experimental region is represented by simplex, rather than hypercube, because the sum of blend proportions should be unity. Several designs based upon this point have been proposed for mixture experiments. Among them, an extreme vertices design is employed in this paper because there are a couple of blend constraints to be considered. In order to investigate how the mixing proportion interacts with other manufacturing factors, a fractional factorial design is also included across the extreme vertices design. As a result, we find that the blend proportion of solution ingredients has a significant effect on battery performances. By simultaneously optimizing two battery capacities, this paper proposes an optimum blend proportion according to process factor settings.

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Using Design of Mixture Experiments to Select the Ratio of a Three-Component Electrode for Optimal Generation of Hydroxyl Radicals (혼합물 실험계획법을 이용한 OH라디칼 최적 생성을 위한 삼성분 전극의 비율 선정)

  • Park, Young-Seek
    • Journal of Environmental Science International
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    • v.29 no.8
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    • pp.793-800
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    • 2020
  • The conventional development of multi-component electrodes is based on the researcher's experience and is based on trial and error. Therefore, there is a need for a scientific method to reduce the time and economic losses thereof and systematize the mixing of electrode components. In this study, we use design of mixture experiments (DOME)- in particular a simplex lattice design with Design Expert program- to attempt to find an optimum mixing ratio for a three-component electrode for the high RNO degradation; RNO is an indictor of OH radical formation. The experiment included 12 experimental points with 2 center replicates for 3 different independent variables (with the molar ratio of Ru, Ti, Ir). As the Prob > F value of the 'Quadratic' model is 0.0026, the secondary model was found to be suitable. Applying the molar ratio of the electrode components to the corrected response model results is an RNO removal efficiency (%) = 59.89 × [Ru] + 9.78 × [Ti] + 67.03 × [Ir] + 66.38 × [Ru] × [Ir] + 132.86 × [Ti] × [Ir]. The R2 value of the equation is 0.9374 after the error term is excluded. The optimized formulation of the ternary electrode for an high RNO degradation was acquired when the molar ratio of Ru 0.100, Ti 0.200, Ir 0.700 (desirability d value, 1).

Determination of the Optimal Mixture Ratio for Extrudates of Job's-tear and Wheat Flour by Mixture Design Analysis (혼합실험계획법에 의한 율무와 밀가루의 압출성형 최적 배합 조건 설정)

  • Cho, Seok-Cheol;Kang, Byung-Sun
    • Korean Journal of Food Science and Technology
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    • v.45 no.4
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    • pp.473-477
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    • 2013
  • The aim of this study was to identify the optimal ingredient-mixing ratio of Job's-tear and wheat flour subjected to extrusion. A modified distance-based mixture design analysis was chosen for the experimental design. The results showed that the bending failure force, the a-value, and the water absorbtion index (WAI) value had no correlation with the mixture ratio of Job's-tear and wheat flour. However, the diameter of the extrudates, the L- and b-values, and the water solubility index (WSI) value were all found to be correlated to the mixture ratio. While the first three values were determined using a linear model, the WSI value was determined using a quadratic model. The diameter and color had an inverse correlation to the mixture ratio: the higher the ratio of Job's-tear to wheat flour, the lower the diameter and darker the color. The L- and b-values were found to change in accordance with the mixture ratio of Job's-tear to wheat flour. The lowest WSI value was obtained at a 40:60 ratio of Job's-tear to wheat.

Convergence Study on the Optimization for Suppression of Starch Hydrolysis using Rutin, Quercetin and Dietary Fiber Mixture Design (루틴, 퀘르세틴, 식이섬유 혼합물 설계를 이용한 전분소화 지연 효과의 최적화에 대한 융합 연구)

  • Oh, Imkyung;Bae, In Young
    • Journal of the Korea Convergence Society
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    • v.11 no.5
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    • pp.35-41
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    • 2020
  • This study was conducted to develop the efficient system for starch hydrolysis suppression using rutin, quercetin and dietary fiber through the statistical mixture design. The three components were replaced with wheat flour at the level of 10% and the mixed gel with three components was characterized by in vitro starch digestion. The mixture design was applied by simplex-centroid experimental model. The quadratic model (R2=0.86) was well fitted and the obtained regression equation indicated that the significant positive effects was observed in the quercetin and fiber mixture. Based on the statistical results, the best mixing ratio of quercetin and fiber was 72: 28 that led to the lowest predicted glycemic index (pGI). Their interactions on the pGI of starch digestibility were clearly visualized in the 3D surface plot. These results suggested that the mixture of quercetin and fiber interact strongly with wheat flour, consequently retarding starch hydrolysis by 15%.

Experimental Study for Determination of Optimum Waste Vinyl Contents in Asphalt Concrete (아스팔트 콘크리트에 적정 폐비닐 첨가량 결정에 관한 실험적 연구)

  • 김광우;김주인;이순제;최선주
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.44 no.5
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    • pp.88-95
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    • 2002
  • This study is a fundamental research for recycling waste vinyl (WV) in asphalt mixture for improving roadway pavement. Mix design was conducted by WV content and optimum asphalt content (OAC) was determined for dense-graded surface course mixture. Marshall stability test, indirect tensile strength (ITS) test and wheel tracking test were carried out to measure the characteristics of WV-added asphalt concretes. From the results of this study, recycling WV in asphalt mixture is possible. However, as WV content increased, melted WV clustering appeared in asphalt mixture. It could be considered that adding too much WV in asphalt mixture is not proper. The proper content of LDPE and HDPE WV was appeared to be 12% and 8%, respectively.

An Experimental Study on Optimal Mixture Ratio of Hardening Agent for Surface Soil Stabilization (연약지반 표층안정처리를 위한 고화재의 최적조합 산정에 관한 실험적 연구)

  • 천병식;김진춘;최현석
    • Proceedings of the Korean Geotechical Society Conference
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    • 2000.11a
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    • pp.17-24
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    • 2000
  • Hardening agent has been the traditional material for surface soil stabilization of soft ground. This study aims at determining optimal mixture ratio of hardening agent in accordance with the required design specifications. Hardening agent is properly mixtured with Fly ash, Gypsum, Slag and Cement for the ettringite hydrates which is effective for early stabilization of unconsolidated soil. The treated soil is the clay which are widely found here and there in Korea. In this study, preliminary tests were performed to get optimal mixture ratio of stabilizer ingredient, and marine clay in Jin-Hae was used to get physical and chemical properties. Laboratory tests of 50 stabilized soil were peformed to get optimal mixture ratio for 16 stabilizer material of 6 type, and stabilizer mixing was determined.

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A Case Study of Applying Mixture Experimental Design to Enhance Flame Retardancy of Wood-Plastic Composites (합성목재의 난연성 확보를 위한 혼합물 실험계획 사례)

  • Seo, Ho-Jin;Kwon, Minseo;Lee, Gun-Myung;Ju, Hyejin;Byun, Jai-Hyun
    • Journal of Korean Society for Quality Management
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    • v.50 no.1
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    • pp.169-181
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    • 2022
  • Purpose: This paper addresses a case study of developing a flame retardant wood-plastic composites (WPC) by adding tannic acid to the existing synthetic wood. The optimal mixing ratios of six components are explored to minimize the burning time using two mixture designs. Methods: In the preliminary experiment, six components are considered to find important components and their ranges. Seven D-optimal mixture design points are generated. Two points are removed for the balance of plastic components to be maintained, and the remaining five points are augmented with two basic compositions. Four components are selected to be considered in the main experiment. In the main experiment, pellets are extruded at the eight mixture design points. In-house testing of burning time is executed three times. Specimens made of pellets from two promising flame retardant compositions are sent to the accredited laboratories and tested. Results: The test results are as follows: 1) The best composition (Wood flour, Tannic acid, PE, Lubricant) = (25, 41, 10, 2) (wt%) shows the burning time of 1 second, which is 9-fold improvement compared to the the burning time of 9 seconds from the existing composition (58, 0, 10, 2) (wt%). 2) The second best composition (41, 25, 10, 2) (wt%) results in the burning time of 2 seconds. This composition is inferior to the best composition in terms of the flame retardancy, but more economical since it needs less tannic acid which is 100-fold expensive than the wood flour. Conclusion: Flame retardant compositions are found by adding tannic acid to the existing WPC employing optimal mixture designs. This case study will be helpful to practitioners who try to develop new products with additional physical properties with as small number of experimental trials as possible. Future research direction includes exploring conditions which satisfy both performance level and cost limitation simultaneously.

A Study on Composite Blades of 1 MW Class HAWT Considering Fatigue Life (피로수명을 고려한 1 MW급 수평축 풍력터빈 복합재 블레이드 설계에 관한 연구)

  • Kim, Min-Woong;Kong, Chang-Duk;Park, Hyun-Bum
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.40 no.7
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    • pp.564-573
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    • 2012
  • In this work, 1 MW class horizontal axis wind turbine blade configuration is properly sized and analyzed using the newly proposed aerodynamic design procedure and the in-house code developed by authors, and its design results are verified through comparison with experimental results of previously developed wind turbine blade. The structural design of the wind turbine blade is carried out using a composite materials and the netting and rule of mixture deign methods. The structural safety of the designed blade structure is investigated through the various load cases, stress, deformation, buckling and vibration analyses using the commercial FEM code, MSC.NASTRAN. Finally the required fatigue life is investigated using the modified Spera's experimental equation.

Mixutre Optimization of Hwangdo Peach (Prunus persica L. Batsch) Dressing by Mixture Experimental Design (혼합물 실험계획법에 의한 황도복숭아 드레싱 재료혼합비의 최적화)

  • Park, Jung Eun;Kim, Yong-Sik
    • Culinary science and hospitality research
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    • v.23 no.7
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    • pp.20-30
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    • 2017
  • This study was conducted for the optimization of ingredients in salad dressing using Hwangdo peach (Prunus persica L. Batsch). The experiment was designed according to the D-optimal design of mixture design, which included 14 experimental points with 4 replicates for three independent variables (olive oil 40~65%, peach puree 27~50%, vinegar 8~20%). The linear regression models for pH, viscosity and color value and the quadratic regression models for emulsion stability, all sensory evaluation of the products were proven to be valid by the F-test for the overall significance of the regression model at a 5% level. Viscosity and pH of the products increased as olive oil content. Color value, viscosity and pH of the products increased as peach puree content. pH, viscosity, redness, and yellowness of the products decreased as vinegar content. Sensory evaluation result of the products showed that general preference for the products were increasingly affected by the increases in contents then decreased as they exceeded the optimum levels. In consequence, according to result from the first stage of the experiment, the optimum ingredients ratios of the raw materials were set in olive oil 52.43%, peach puree 35.07%, and vinegar 13.91% for ingredients of apricot dressing. These results provided the possibility that peach can be applied to the preparation of a dressing, and thereby present baseline data for the development of new dressings. This is also presumed to meet demands of customers who are always in pursuit of new products.