• 제목/요약/키워드: mineral powder

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부순모래를 사용한 습식 숏크리트의 광물성 혼화재료 혼입에 따른 내구성 평가 (Durability Assessment for Crushed Sand Wet-mix Shotcrete Mixed with Mineral Admixtures)

  • 이겨레;한승연;남궁경;윤경구
    • 콘크리트학회논문집
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    • 제26권5호
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    • pp.607-614
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    • 2014
  • 본 논문에서는 품질확보를 위하여 혼합골재 입도분포를 적용한 부순모래 숏크리트에 플라이애시, 고로슬래그 미분말, 메타카올린, 실리카퓸을 종류 및 혼입률에 변동을 주어 혼입하여 숏크리트의 기초특성과 내구특성에 미치는 영향을 고찰하였다. 또한 각 혼화재료의 주요 혼입률을 선정하고 실제 숏팅을 실시 하여 숏팅 전 후의 기초특성과 내구특성을 분석하였다. 실내실험 결과 광물성 혼화재료 혼입률이 증가할수록 압축강도가 증가하는 경향을 보였다. 특히 메타카올린을 혼입한 경우 가장 우수한 강도 증진효과를 보였으며, 숏팅 후 압축강도 역시 코어링에 의한 강도감소 현상을 감안하여도 강도 발현이 우수한 혼화재료로 판단된다. 염소이온 침투저항성 시험과 황산저항성 시험 결과 광물성 혼화재료 혼입은 염소이온과 황산에 대한 저항성이 증진되는 경향을 보인다. 화상분석을 통한 공극구조 분석 결과 공기연행제를 사용하지 않아 소요의 간격계수와 비표면적을 얻는데 실패하였으며, 향후 공기연행제의 도입 후 실험이 진행될 필요성을 보이고 있다.

에어로졸 자기조립에 의한 실리카 나노분말의 표면개질 (Surface Modification Silica Nanoparticles by Aerosol Self Assembly)

  • 길대섭;장희동;장한권;조국;김선경;오경준;최진훈
    • 한국재료학회지
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    • 제20권2호
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    • pp.78-81
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    • 2010
  • Surface modification of silica nanoparticles was investigated using an aerosol self assembly. Stearic acid was used as surface treating agent. A two-fluid jet nozzle was employed to generate an aerosol of the colloidal suspension, which contained 20 nm of silica nanoparticles, surface modifier, and ethyl alcohol. Powder properties such as morphology, specific surface area and pore size distribution were analyzed by SEM, BET and BJH methods, respectively. Surface properties of the silica power were analyzed by FT-IR. The OH bond of the $SiO_2$ surface was converted to a C-H bond. It was revealed that the hydrophilic surface changed to a hydrophobic one due to the aerosol self assembly. Morphology of the surface treated powder was nanostructured with lots of pores having an average diameter of around $2\;{\mu}m$. Depending on the stearic acid concentration (0.25 to 1.0 wt%), the pore size distribution of the particles and the degree of hydrophobicity ranged from 1.5 nm to 180 nm and 29.6% to 50.2%, respectively.

혼화재로서 폐유리 미분말을 사용한 콘크리트의 특성 평가 (The Properties of Concrete containing Waste-glass Powder)

  • 최성우;류득현;김준형
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2017년도 춘계 학술논문 발표대회
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    • pp.222-223
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    • 2017
  • In the automotive industry, such as scrap metal and plastic scrap process is being recycled. Although the glass beads are used as road paving or other additives and processing crushing, recycling is known that there are limits. The utilization of waste glass was evaluated as a concrete admixture by using powder characteristics and chemical composition of the glass. As a result of using waste-glass powder as an admixture, it is difficult to expect the pozzolanic effect, but it is found that it can increase the fluidity of concrete and ensure the durability performance in the appropriate amount range.

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건조새우를 이용한 칼슘강화 건강다과 개발 (Development of Calcium Enriched Healthy Snack using Dried Shrimp)

  • 박은빈;유수인;김연재;백진경
    • 한국식품영양학회지
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    • 제35권1호
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    • pp.1-6
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    • 2022
  • In this study, we developed a healthy snack using dried shrimp powder which is rich in calcium to help prevent bone disease. Different types of yanggaeng were prepared with varying ratios of dried shrimp powder; 1%, 3%, 5%, and 7%. Moisture content, color value, texture properties, and mineral concentration were measured. The L, a, and b chromaticity values showed significant differences in the 5% addition group (p<0.001). The texture properties, hardness, and adhesion decreased significantly as the amount of shrimp powder increased (p<0.001), while chewiness and elasticity significantly increased as the amount increased (p<0.001). Calcium and potassium increased significantly as the amount of shrimp powder increased (p<0.001).

고강도콘크리트의 특성에 미치는 고로슬래그 미분말의 분말도 영향에 관한 실험적 연구 (An Experimental Study on the Influence of Fineness of Blast Furnace Slag Powder on the Properties of High Strength Concrete)

  • 김주상;박규연;김재환;이상수;송하영;김을용
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2006년도 추계 학술발표회 논문집
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    • pp.453-456
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    • 2006
  • In this study, the experiment was carried out to investigate and analyze the influence of fineness of blast furnace slag powder on the properties of high strength concrete. The main experimental variables were water/binder ratio 27.5, 31.5, 35.5(%) water content $165kg/m^3$ and mineral admixtures such as blast furnace slag powder. Even in a case where the ratio of blast furnace slag powder is 70%, using a fineness of 8000 grade afforded a higher strength development than using a plain concrete, which indicates the potential of high utilization in the future. Although it has been pointed out that the concrete using blast furnace slag powder has a problem of yielding relatively low rate of strength development in the early age, it is demonstrated that this can be resolved by using a powder with fineness greater than 6000 grade. It is considered necessary that powder fineness should be upgraded for the applications such as high performance concrete to be used in high strength required areas by considering hydration heat control and early strength requirements in the future.

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혼화재 종류 및 치환율에 따른 모르터의 조기강도 특성에 관한 연구 (A study on the Early-Strength Properties of Mortar according to the Kinds and Replacement Ratio of Mineral Admixture)

  • 최세진;이성연;김성수
    • 한국건축시공학회지
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    • 제7권2호통권24호
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    • pp.59-65
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    • 2007
  • Recently, due to the increase of high-rise buildings construction, many researches for making harden of concrete earlier and remove of forms faster are being performed to reduce construction period. In this study, we compared and analysed the early strength properties of mortar according to the kinds and replacement ratio of mineral admixture to select the kinds and replacement ratio of mineral admixture of high early strength concrete. For this purpose, mortar mixtures according to the kinds(FA, MK, ZR, BFS, DM) and replacement ratio(0, 2, 4% by volume of sand) of mineral admixture were selected. From our test data, early-age compressive strength decreased in accordance with the increase of replacement ratio of fly-ash(FA) & blast furnace slag powder(BSF) and, in case of addition admixture, early-age compressive strength of with containing 4% appeared higher compared with containing 2%.

전이금속 도핑이 ZnO 나노분말의 특성 및 메틸렌블루 광촉매 분해 특성에 미치는 영향 (Effects of transition metal-doping on the properties of ZnO nanoparticles and the photocatalytic degradation of methylene blue)

  • 장한권;오경준;장희동;조국;김동진;최진훈
    • 한국입자에어로졸학회지
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    • 제6권1호
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    • pp.29-35
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    • 2010
  • Transition metals such as V, Fe, and Ni were used to synthesize doped zinc oxide nanoparticles from mixed liquid precursors by using the flame spray pyrolysis (FSP). The effects of dopants on the powder properties such as morphology, specific surface area, crystal structure, and light adsorption were analyzed by TEM, BET, XRD, and UV-Vis diffuse reflection spectrum (DRS), respectively. The results showed that hexagonal wurtzite structured ZnO:M (M = V, Fe, Ni) nanoparticles were successfully synthesized by the FSP. The transition metal-doping resulted in the decrease in its particle size and crystallite size. The UV-vis absorption spectra of ZnO:M nanoparticles were also red-shifted. ZnO:V showed the highest MB degradation of 99.4% under the UV irradiation after 3 hrs.

폐실리콘 슬러지로부터 실리콘 분말의 분리 회수 (Separation and Recovery of Silicon Powder from Waste Silcon Sludge)

  • 장희동;장한권;서용재;김병규;홍승휘;장원철
    • 한국자원리싸이클링학회:학술대회논문집
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    • 한국자원리싸이클링학회 2005년도 춘계임시총회 및 제25회 학술발표대회
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    • pp.147-151
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    • 2005
  • 실리콘 잉곳의 절단공정에서 발생하는 폐실리콘 슬러지는 실리콘과 실리콘카바이드 등의 유가자원이 함유되어 있는데, 본 연구에서는 폐실리콘 슬러지 중의 실리콘 분말을 효과적으로 분리, 회수하는 방법에 대해 검토하였다. 폐실리콘 슬러지는 상당량의 절삭유와 소량의 철분말이 포함되어 있는데 절삭유는 유기 용매에 용해시켜 효과적으로 분리하였고, 철분말은 자력선별에 의해 제거하였다. 절삭유와 철성분이 제거된 잔사인 실리콘과 실리콘 카바이드의 혼합 분말로부터 초음파 분산 선별법을 사용하여 실리콘 분말을 효율적으로 분리회수 하였다.

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한국산 천연 광물 부석 파우더 코팅 및 특성에 관한 연구 (A Study of Properties and Coating Natural Mineral Pumice Powder of in Korea)

  • 김인영;노지민;남은희;신문삼
    • 한국응용과학기술학회지
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    • 제36권2호
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    • pp.498-506
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    • 2019
  • 이 연구는 경상북도 봉화지역에서 매장된 천연 광물을 이용하여 화장료용의 분체로써 활용가치를 부여한 코팅 방법에 관한 것이다. 이 광물의 이름은 부석이라고 칭하며, 미립자 파우더를 개발하여 이 파우더의 성능을 평가하고 화장품의 효능적 가치가 있는 가에 대하여 연구한 결과를 보고한다. 이 파우더의 표면에 오일을 코팅하기 위하여 미립자 표면에 알루미늄하이드록사이드를 1차 코팅한 후에 여기에 알킬실란으로 코팅하였다. 또한, 식물성 오일로 코팅하여 파우더의 응집을 막고, 오일상에서의 분산성을 높일 수 있도록 하였다. 첫째; 부석파우더의 입자는 $10{\sim}50{\mu}m$의 입자를 가지고 있었으며, 입자의 표면에 다공성의 구멍이 있었다. 둘째; 이 파우더의 구성성분은 $SiO_2$, $Al_2O_3$, $Fe_2O_3$, MgO, CaO, $K_2O_2$, $Na_2O$, $TiO_2$, $TiO_2$, MnO, $Cr_2O_3$, $V_2O_5$ 등을 함유하였다. 셋째: 이 파우더의 입자는 판상형 구조를 가지며, 다공성으로 적갈색을 가지고 있음을 SEM과 TEM 분석을 통하여 알 수 있었다. 넷째; 이부석 파우더의 원적외선 방사율은 $0.924{\mu}m$이었으며, 방사에너지는 $3.72{\times}10^W/m^2{\cdot}{\mu}m$ 이었다. 또한 음이온 방출량은 128 ION/cc를 방출하는 것으로써, 코팅을 하더라도 변하지 않고 그대로 그 성능이 유지되는 것을 알 수 있었다. 이러한 결과를 바탕으로 화장품의 응용분야로써 비비크림, 쿠션파운데이션, 파우더펙트 등의 색조화장품, 선블록크림, 워시오프 마사지팩 등의 기초 화장료에 폭넓게 응용이 가능할 것으로 기대한다.

X-Ray Diffraction Analysis of Various Calcium Silicate-Based Materials

  • An, So-Youn;Lee, Myung-Jin;Shim, Youn-Soo
    • 치위생과학회지
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    • 제22권3호
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    • pp.191-198
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    • 2022
  • Background: The purpose of this study was to evaluate the composition of the crystal phases of various calcium silicate-based materials (CSMs): ProRoot white MTA (mineral trioxide aggregate) (WMTA), Ortho MTA (OM), Endocem MTA (EM), Retro MTA (RM), Endocem Zr (EN-Z), BiodentineTM (BD), EZ-sealTM (EZ), and OrthoMTA III (OM3). Methods: In a sample holder, 5 g of the powder sample was placed and the top surface of the material was packed flat using a sterilized glass slide. The prepared slides were mounted on an X-ray diffraction (XRD) instrument (D8 Advance; Bruker AXS GmbH, Germany). The X-ray beam 2θ angle range was set at 10~90° and scanned at 1.2° per minute. The Cu X-ray source set to operate at 40 kV and 40 mA in the continuous mode. The peaks in the diffraction pattern of each sample were analyzed using the software Diffrac (version 2.1). Then, the peaks were compared and matched with those of standard materials in the corresponding Powder Diffraction File (PDF-2, JCPDS International Center for Diffraction Data). A powder samples of the materials were analyzed using XRD and the peaks in diffraction pattern were compared to the Powder Diffraction File data. Results: Eight CSMs showed a similar diffraction pattern because their main component was calcium silicate. Eight CSMs showed similar diffraction peaks because calcium silicate was their main component. Two components were observed to have been added as radiopacifiers: bismuth oxide was detected in WMTA, OM, and EM while zirconium oxide was detected in RM, EN-Z, BD, EZ, and OM3. Unusual patterns were detected for the new material, OM3, which had strong peaks at low angles. Conclusion: It was caused by the presence of Brushite, which is believed to have resulted in crystal growth in a particular direction for a specific purpose.