• Title/Summary/Keyword: mineral powder

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Preparation of Nano-sized Pt Powders by Solution-phase Reduction (액상환원법(液相還元法)에 의한 백금(白金) 나노분말(粉末) 제조(製造))

  • Kim, Chul-Joo;Yoon, Ho-Sung;Cho, Sung-Wook;Sohn, Jung-Soo
    • Resources Recycling
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    • v.16 no.5
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    • pp.36-40
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    • 2007
  • Platinum plays an important role in many applications because of its extraordinary physical and chemical properties. All these applications require the use of platinum in the finely divided state. Therefore the preparation of platinum nanoparticles by reducing platinum-surfactant salt with reducing agent in the solution was investigated in this study. The net interaction between C14TABr and $H_2[PtCl_6]$ in aqueous solution results in the formation of $[C14TA]_2[PtCl_6]$. The concentration of C14TABr and the concentration of $H_2[PtCl_6]$ has to be above cmc and 0.32 mM, respectively in order to obtain complex-micelle aggregation for mono dispersed Pt particles. Pt particle size increases with increasing $H_2[PtCl_6]$ and C14TABr concentration. And the shape of Pt particles was well controlled with increasing surfactant concentration.

Adsorption Behaviors of Nickel Ion on the Manganese Dioxide Powder (이산화망간 미립자(微粒子)의 니켈이온 흡착(吸着) 거동(擧動))

  • Baek, Mi-Hwa;Kim, Min-Kyung;Kim, Dong-Su;Sohn, Jeong-Soo
    • Resources Recycling
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    • v.17 no.1
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    • pp.59-65
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    • 2008
  • The adsorption features of nickel ion in wastewater on manganese dioxide from spent batteries were investigated for its usage as an adsorbent. The aquatic behavior of nickel ion was characterized by MINTEQ program and the considered influential variables on the adsorption of nickel ion were its initial concentration, reaction temperature, the amount of adsorbent, and pH. The adsorption ratio of nickel ion decreased with increasing its initial concentration and thermodynamic estimation has been carried out based on the adsorption characteristics of nickel ion depending on temperature. In addition, the adsorption of nickel ion was shown to be promoted according to the amount of manganese dioxide and a lot of nickel ions were adsorbed as the solution pH was raised.

Vapor phase synthesis of silicon nitride powder using DC plasma torch (DC 플라즈마 토치를 이용한 질화규소 분말의 기상합성)

  • Hwang, Y.;Sohn, Y.U.;Chung, H.S.;Choi, S.K.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.4
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    • pp.370-377
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    • 1994
  • DC plasma torch which is a non-transferred type was constructed and silicon nitride powders were produced. Ar gas is used as a plasma gas and gas reactants with the carrier gas are introduced beneath the plasma ignition part. Two slits are attached and a reactive quenching gas is introduced through them. Using $SiCl_4 and NH_3$ as starting materials, silicon nitride powders were produced. As-produced powders were amorphous and crystalline silicon nitrides were obtained by heating at $1420^{\circ}C$ for two hours under nitrogen atmosphere. Silicon nitride phase was identified in the XRD patterns and IR spectrum, and the image of the powders before and after heating was observed from the TEM analysis.

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An Assessment of Utilization of the Pungchon Limestone in Paper Industry (풍촌층 석회석의 제지 산업에서의 응용성 평가)

  • Lee, Na-Kyong;Noh, Jin-Hwan
    • Journal of the Mineralogical Society of Korea
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    • v.20 no.4
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    • pp.339-349
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    • 2007
  • For various types of the Pungchon limestone, diverse mineral characters of the limestone including their size and morphology are investigated by using of ELS and SEM to examine the possibility of application as fillers to paper industry. Also, the measurement of zeta potential and the evaluation of coagulation properties in calcite suspension was made for fine powders of the limestone to examine the applicability and efficiency in wet-papermaking process. Fine powder of the Pungchon lime-stone, largely controlled by original mineral characters of ore in mineralogical aspects, exhibits some-what different trend in particle morphology according to ore types, and thereby, the size distribution, zeta potential and coagulation properties also become different. The examined whiteness, brightness, opacity and sheet strength in hand sheet also show remarkable differences according to ore types. These are seemed to be basically due to the results of combined effects of whiteness, site distribution, refractive index, and morphology of the limestone powder on the properties of hand sheet. Considering the investigated results, all types of the Pungchon limestone appear to be sufficiently applicable to paper industry. Especially, the mega-crystalline calcite type is evaluated to be overall suitable for the purpose of paper industry due to the higher values in whiteness and brightness. In addition the fine powder of micro-crystalline calcite type is assessed particularly to have a good quality in sheet strength by virtue of irregular particle shape.

CaO Optimal Classification Conditions for the Use of Waste Concrete Fine Powder as a Substitute for Limestone in Clinker Raw Materials (폐콘크리트 미분말을 클링커 원료의 석회석 대체재로 사용하기 위한 CaO 최적 분급 조건)

  • Ha-Seog Kim;Sang-Chul Shin
    • Land and Housing Review
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    • v.15 no.1
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    • pp.147-156
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    • 2024
  • This study aims to reduce CO2 generated during the manufacturing process by using limestone (CaCO3), a carbonate mineral used in the production of cement clinker, as a decarbonated raw material that does not contain CO2. Among various industrial by-products, we attempted to use cement paste attached to waste concrete. In general, limestone for cement must have a CaCO3 content of at least 80% (CaO, 44% or more) to ensure the quality of cement clinker. However, the CaO content of waste concrete fine powder is about 20% on average, so in order to use it as a cement clinker raw material, the CaO content must be increased to more than 35%. Therefore, by using the difference in hardness of the mineral composition of waste concrete fine powder to selectively crush CaO type minerals with relatively low hardness, classify and sieve, the CaO content can be increased by more than 35%. Accordingly, in this study, we experimentally and statistically reviewed and analyzed the optimal conditions for efficiently separating CaO and SiO2 and other components by selectively pulverizing minerals containing relatively low CaO through a grinding process. As a result of the optimal grinding conditions experiment, it was found that the optimal conditions were a grinding time of less than 5 minutes, a type of material to be crushed of 30 mm, and an amount of material to be crushed of 1.0 or more. However, it is judged that it is necessary to review pulverized materials of mixed particle sizes rather than pulverized products of single particle size.

Experimental Study on Durability Properties of High Performance Concrete on Using Hydraulic Mineral Admixtures for Bridge Deck Overlay (수경성 광물질 혼합재를 사용한 교면 덧씌우기용 고성능 콘크리트의 내구성능에 관한 실험적 연구)

  • Kim, Ki-Hyung;Son, Hyung-Ho;Jung, Ho-Jin;Lee, Jae-Nam
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.2
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    • pp.74-80
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    • 2011
  • In this study, it is evaluated on the properties of mechanical performance, autogenous shrinkage and chloride resistance for application of high performance concrete for bridge deck overlay used slag powder and fly ash as a representative by-product of industrialization. According to test results, it is evaluated that the durability of concrete is improved the properties of chloride resistance, autogenous shrinkage and alkali aggregate reaction by using hydraulic mineral admixtures. It is considered to have a green construction and an economic feasibility on recycling of by-product as a improved concrete for durability and efficiency in materials and constructions.

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Analysis of the General and Mineral Compositions of Kamut Powder and Effect of Kamut(Triticum turanicum Jakubz) Powder and Its Effect on Blood Parameters in Mice Fed a High-Fat Diet Supplement (카무트 분말가루의 영양성분 분석 및 고지방식이 섭취 시 카무트 분말가루의 첨가가 흰쥐 체내에서 혈중 대사 인자에 미치는 영향)

  • Shin, Kyung-Ok
    • The Korean Journal of Food And Nutrition
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    • v.30 no.6
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    • pp.1157-1163
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    • 2017
  • This study, analyzed the general and minerals composition of kamut and investigated its effect on blood components in mice fed a high fat diet. The content of each general component of kamut was as follows: $11.02{\pm}0.75%$ water, $13.16{\pm}1.28%$ crude protein, $1.85{\pm}0.19%$ crude fat, and $1.97{\pm}0.13%$ ash. The leptin level was the highest in the HF group($30.00{\pm}0.00ng/mL$) when compared to the control group. There was a significant decrease of $23.65{\pm}5.54ng/mL$ in the HFK group when compared to the HF group (p<0.05). The blood LDL-cholesterol concentration was the lowest in the control group at $10.00{\pm}2.00mg/dL$. The level was highest in the HF group at $28.00{\pm}0.00mg/dL$ when compared with the other groups (p<0.05). The aspartate transaminase (AST) level was significantly higher in the HFK group ($179.33{\pm}173.88U/L$) than in the control ($61.00{\pm}12.73U/L$) and HF groups ($132.00{\pm}0.00U/L$). According to the results of this study, the consumption of kamut lowers the blood LDL-cholesterol level more than the consumption of wheat flour. Additionally, kamut contains antioxidant substances such as selenium and zinc, which are thought to contribute to vascular health and thus aid in maintaining good health. Therefore, it is necessary to develop a variety of health foods using kamut; it should be used as a functional food for the maintenance of good health.

Studies on the Application of the Spent Alkaline Manganese Batteries Powder as an Adsorbent for Nickel Ion (폐(廢)알칼리망간전지(電池) 분말(粉末)의 니켈 이온 흡착제(吸着劑)로서의 활용(活用)에 관한 연구(硏究))

  • Baek, Mi-Hwa;Kim, Dong-Su;Sohn, Jeong-Soo
    • Resources Recycling
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    • v.17 no.2
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    • pp.63-69
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    • 2008
  • The adsorption features of $Ni^{2+}$ onto spent alkaline manganese batteries powder have been investigated with the adsorbent dose, initial concentration of adsorbate and temperature as the experimental variables. The adsorption reaction of $Ni^{2+}$ ion followed the pseudo-second order rate model, and the adsorption rate constants($k_2$) decreased with increasing initial concentration of nickel ion. The equilibrium adsorption data were fitted to the Langmuir and Freundlich models. The Freundlich model represents the equilibrium data better than the Langmuir model in this initial adsorbate concentration range. As the temperature increased, the adsorbed amount of nickel ion at equilibrium was also increased, which indicated that the adsorption reaction was endothermic. Based on the experimental results obtained along with temperatures, thermodynamic parameters such as ${\Delta}H^{\circ},\;{\Delta}G^{\circ},\;and\;{\Delta}S^{\circ}$ were calculated.

Effect of Substrates on Growth and Yield of Hydroponically Grown Cucumber in Bag Culture (자루재배에서 배지의 종류가 오이의 생육 및 수량에 미치는 영향)

  • 이응호;이재욱;권지선;남윤일;조일환;권영삼
    • Journal of Bio-Environment Control
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    • v.5 no.1
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    • pp.15-22
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    • 1996
  • Cucumbers(Cucumis sativus L. CV. SHARP 1) were cultivated by bag culture for 5 months to investigate the effect of substrates on growth, yield, and mineral contents. The substrates used in the experiment were vermiculite + perlite +peatmoss(1:1:1=V:V:V), perlite+peatmoss(1:1=V:V), perlite+carbonized chaff(7:3=V:V), rockwool, sawdust, and chaff+chaff powder under 10 mesh (7:3=V:V). The rate of moisture content was highest at chaff powder under 10 mesh as 42.5% and was lowest at perlite+carbonized chaff as 31%. Plant height, No. of leaves, fresh and dry weight were increased in vermiculite+perlite+peatmoss(1:1:1=V:V:V). Marketable fruits and yield also showed same aspect with growth. All kinds of mineral contents except K in cucumber plants were higher at vermiculite+perlite+peatmoss(1:1:1=V:V:V), but K content was higher at perlite+ carbonized chaff(7:3=V:V) than those other substrates.

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Solution Combustion Synthesis of LaFeO3 Powders and Their Carbon Ignition Property (용액연소합성법을 이용한 LaFeO3 분말 합성 및 탄소 연소 특성)

  • Rang, Da-Sik;Lee, Tae-Kun;Hwang, Yeon;Bae, Kwang-Hyun;Cho, Sung-Baek
    • Korean Journal of Materials Research
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    • v.17 no.7
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    • pp.382-385
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    • 2007
  • [ $LaFeO_3$ ] powders were prepared as the oxidation catalyst materials to reduce the emission of particulate matters from diesel engine and their catalytic effects on the oxidation of carbon were investigated. Solution combustion method was employed for the powder synthesis, which uses highly exothermic and selfsustaining reactions. In this study $LaFeO_3$ powders were synthesized at $400^{\circ}C$ as varying the ratio ($\Phi$) of fuel (citric acid) and oxidizer (metal nitrate), and their phase and carbon ignition property were examined. As $\Phi$ decreases, the crystallinity of synthesized $LaFeO_3$ powders enhanced. By calcining at $700^{\circ}C$, all the powders synthesized at various $\Phi$ fully crystallized. The calcined $LaFeO_3$ powders showed carbon ignition temperature as low as $501{\sim}530^{\circ}C$, which implied the decrease of the ignition temperature by $120{\sim}150^{\circ}C$.