• Title/Summary/Keyword: microwave

Search Result 4,502, Processing Time 0.031 seconds

Improved Solubility and Characterization of Photovoltaic Properties D/A Copolymers based on Rigid Structure of Phenothiazine-Quinoxaline (Rigid한 Phenothiazine-Quinoxaline D/A 공액 고분자 구조의 용해성 향상 연구 및 유기박막태양전지로의 특성 분석)

  • Seong, Ki-Ho;Yun, Dae-Hee;Park, Yong-Sung
    • Clean Technology
    • /
    • v.20 no.4
    • /
    • pp.415-424
    • /
    • 2014
  • In this study, two kinds of polymer (PPQX-2hdPTZ (P1), POPQX-2hdPTZ (P2)) were synthesised by Suzuki coupling reaction based on phenothiazine derivative as electron-donor and quinoxaline derivative as electron-acceptor. Microwave synthesis workstation was used to shorten the polymerization time and increase the degree of polymerization. The physical, thermal stability, optical and electrochemical properties of the synthesized polymer were confirmed. The thermal stability of two polymers was outstanding as the initial decomposition temperature was $323-328^{\circ}C$. And additional substituted alkoxy chain on P2 showed higher degree of polymerization. An analysis of electrochemical properties, all polymer had similar HOMO energy level values. Device was fabricated by ITO/PEDOT:PSS/active layer/$BaF_2$/Al structure and photovoltaic properties were confirmed. Each device has a different film thickness and the resulting change in PCE was confirmed. As a result the thinner thickness of the film showed a high efficiency ($PCE_{max}:P1=1.0%$, P2 = 1.1%).

Mineral Contents in Soybeans with Different Cooking Methods (조리방법에 따른 콩의 무기질 함량)

  • Kim, So Young;Hwang, Jinbong;Park, Ji Su;Choi, Youngmin;Nam, Jin-sik;Lee, Jong-Hun;Seo, Dongwon
    • The Korean Journal of Community Living Science
    • /
    • v.28 no.4
    • /
    • pp.525-535
    • /
    • 2017
  • The purpose of this study was to compare the of ash and minerals contents in different types of soybeans (Baektae, Seoritae, Heuk Tae and Seomoktae) with different cooking methods. Raw, boiled and pan-fried soybean samples were prepared by the Rural Development Administration. Samples were digested by using a microwave and analyzed using ICP-OES and ICP-MS for determining the ash and minerals contents. Ash content in four raw soybeans ranged from 5.07 to 5.59 g/100g. There was no significant difference in the ash contents in raw and pan-fried soybeans (p>0.05). However, the ash content of boiled soybeans was 9 to 14% lower than that of raw soybeans (p<0.05). The minerals contents of Baektae and Seomoktae were high and the major minerals of various soybeans were K, P, Mg, and Ca, which accounted for ash 60.80-65.61%, 20.73-24.26%, 6.90-8.46% and 5.79-8.60%, respectively. The mineral contents of soybeans were significantly different depending on the type of cultivar (p<0.05), but the tendency was not constant. Because the process of soaking and boiling of soybeans made the soluble minerals elute, the ash and mineral contents were reduced. And process of pan-frying of soybeans make Because process of soaking and boiling of soybeans make soluble minerals elute (Ed- this section is very confused and seems to have 2 sentences combined: please check your intended meaning), the ash and mineral contents were reduced. As the soybeans are cooked by pan-frying, the water in the soybeans is evaporated and the mineral content is concentrated or kept constant. These results can serve as the basic data of mineral content during processing and cooking of soybeans.

Large-strain Soft Sensors Using Elastomers Blended with Exfoliated/Fragmented Graphite Particles (탄성중합체와 박리 후 파쇄된 흑연입자 복합재를 이용한 대변형률 연성 센서)

  • Park, Sungmin;Nam, Gyungmok;Kim, Jonghun;Yoon, Sang-Hee
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.40 no.9
    • /
    • pp.815-820
    • /
    • 2016
  • An elastic polymer (e.g., PDMS) blended with EFG particles is a promising conductive composite for fabricating soft sensors that can detect an object's deformation up to or more than 50%. Here, we develop large-strain, sprayable soft sensors using a mixture of PDMS and EFG particles, which are used as a host elastomer and electrically conductive particles, respectively. A solution for a conductive composite mixture is prepared by the microwave-assisted graphite exfoliation, followed by ultrasonication-induced fragmentation of the exfoliated graphite and ultrasonic blending of PDMS and EFG. Using the prepared solutions for composite and pure PDMS, 1-, 2-, and 3-axis soft sensors are fabricated by airbrush stencil technique where composite mixture and pure PDMS are materials for sensing and insulating layers, respectively. We characterize the soft strain sensors after investigating the effect of PDMS/EFG wt% on mechanical compliance and electrical conductance of the conductive composite.

Polyphenol Contents and Physiological Activity of the Lespedeza bicolor Extracts (싸리 추출물의 폴리페놀 함량과 생리활성)

  • Lee, Yang-Suk;Joo, Eun-Young;Kim, Nam-Woo
    • Food Science and Preservation
    • /
    • v.13 no.5
    • /
    • pp.616-622
    • /
    • 2006
  • This study was intended to analyze the contents of polyphenol compounds and vitamin C, and the inhibitory activities of xanthine oxidase and tyrosinase to measure physiological efface of various extract of Lespedeza bicolor. The vitamin C content was $26.42{\pm}0.08mg/100g$. The content of phenolic compounds included in the flesh L bicolor was $1.14{\pm}0.02mg/g$. The ethanol extract by reflux method and water extracts by the microwave-assisted method showed the highest content as 154.95 mg/g and 145.17 mg/g, respectively. The xanthine oxidase inhibitory tate of water extracts was the highest value of 87.85% at the concentration of 1,000 ug/mL. All kinds of extracts showed the highest inhibitory activity for the xanthine oxidase at the concentration of 1,000 ug/mL and a decreasing pattern of the inhibitory race over the concentration of 1,000 ug/mL. The tyrosinase inhibitory rate was increased with an increment of the extract concentrations, and the activity of ethanol extracts was the highest as 55.22% at the concentration of 3,000 ug/mL.

Temperature Dependence of the Dielectric Properties $xBa(Zn_{1/3}Nb_{2/3})O_3-(1-x)Sr(Zn_{1/3}Nb_{2/3})O_3$ Solid Solution ($xBa(Zn_{1/3}Nb_{2/3})O_3-(1-x)Sr(Zn_{1/3}Nb_{2/3})O_3$ 고용체의 온도 변화에 따른 유전 특성)

  • Shim, Hwa-Sup;Lee, Han-Yeong;Kim, Geun-Young;An Chul
    • Journal of the Korean Institute of Telematics and Electronics
    • /
    • v.27 no.11
    • /
    • pp.77-82
    • /
    • 1990
  • The temperature and the composition dependence of the dielectric properties of the solid solution materials in the system $xBa(Zn_{1/3}Nb_{2/3})O_{3}\[BZN]-(1-x)\Sr(Zn_{1/3}Nb{2/3)O_{3}\[SZN]$ at microwave frequency was studied. The dielectric constant and unloaded Q were $40.5{\pm}0.5,5980{\pm}100$ respectively for BZN at 10 GHz and $36.9{\pm}0.5,2700{\pm}100$ for SZN at 10.2GHz. The temperature coefficient of the resonant frequency was $+27.5ppm/{\circ}C$ for BZN and $-39.1ppm/{\circ}C$ for SZN. The results also showed that 0.3 BZN-0.7 SZN is the most temperature-stable composition among xBZN-(1-x) SZN solid solutions. In this case, the dielectric constant, the unloaded Q and $\tau_{f}$ at 9.8GHz were $41.5{\pm}0.2,2920{\pm}100$ and $-3.5ppm/{\circ}C$, respectively.

  • PDF

A Microwave Push-Push VCO with Enhanced Power Efficiency in GaInP/GaAs HBT Technology (향상된 전력효율을 갖는 GaInP/GaAs HBT 마이크로파 푸쉬-푸쉬 전압조정발진기)

  • Kim, Jong-Sik;Moon, Yeon-Guk;Won, Kwang-Ho;Shin, Hyun-Chol
    • Journal of the Institute of Electronics Engineers of Korea SD
    • /
    • v.44 no.9
    • /
    • pp.71-80
    • /
    • 2007
  • This paper presents a new push-push VCO technique that extracts a second harmonic output signal from a capacitive commonnode in a negativegm oscillator topology. The generation of the $2^{nd}$ harmonics is accounted for by the nonlinear current-voltage characteristic of the emitter-base junction diode causing; 1) significant voltage clipping and 2) different rising and falling time during the switching operation of core transistors. Comparative investigations show the technique is more power efficient in the high-frequency region that a conventional push-push technique using an emitter common node. Prototype 12GHz and 17GHz MMIC VCO were realized in GaInP/GaAs HBT technology. They have shown nominal output power of -4.3dBm and -5dBm, phase noise of -108 dBc/Hz and -110.4 dBc/Hz at 1MHz offset, respectively. The phase noise results are also equivalent to a VCO figure-of-merit of -175.8 dBc/Hz and -184.3 dBc/Hz, while dissipate 25.68mW(10.7mA/2.4V) and 13.14mW(4.38mA/3.0V), respectively.

Correlation Analysis Between Soil Moisture Retrieved from Satellite Images and Ground Network Measurements (위성관측 토양수분과 지상관측망 자료의 상관성 분석)

  • Kim, Gwang-Seob;Kim, Jong-Pil
    • Journal of the Korean Association of Geographic Information Studies
    • /
    • v.14 no.2
    • /
    • pp.69-81
    • /
    • 2011
  • The soil moisture data of the National Aeronautics and Space Administration(NASA) and the Vrije Universiteit Amsterdam(VUA) in collaboration with NASA, retrieved from Advanced Microwave Scanning Radiometer-Earth observing system(AMSR-E) brightness temperature, were collected to evaluate the applicability of the remote sensed soil moisture in South Korea. The averages of the soil moisture by in-situ sensors, by NASA and by VUA-NASA are approximately 0.218, 0.119, and $0.402m^3/m^3$, respectively. This indicates that the soil moisture of NASA was underestimated and that of VUA-NASA was overestimated. The soil moisture products of VUA-NASA showed a better relationship with the in-situ data than that of NASA data. However, there are still limitations of C-band soil moisture measurements. To improve the applicability of satellite soil moisture measurements, bias correction and other post processings are essential using in-situ soil moisture measurements at various surface conditions.

Luminous Characteristics of Transparent Field Emitters Produced by Using Ultra-thin Films of Single Walled Carbon Nanotubes

  • Jang, Eun-Soo;Goak, Jeung-Choon;Lee, Han-Sung;Lee, Seung-Ho;Lee, Nae-Sung
    • Proceedings of the Materials Research Society of Korea Conference
    • /
    • 2009.05a
    • /
    • pp.31.1-31.1
    • /
    • 2009
  • Carbon nanotubes (CNTs) are attractive material because of their superior electrical, mechanical, and chemical properties. Furthermore, their geometric features such as a large aspect ratio and a small radius of curvature at tip make them ideal for low-voltage field emission devices including backlight units of liquid crystal display, lighting lamps, X-ray source, microwave amplifiers, electron microscopes, etc. In field emission devices for display applications, the phosphor anode is positioned against the CNT emitters. In most case, light generated from the phosphor by electron bombardment passes through the anode front plate to reach observers. However, light is produced in a narrow depth of the surface of the phosphor layer because phosphor particles are big as much as several micrometers, which means that it is necessary to transmit through the phosphor layer. Hence, a drop of light intensity is unavoidable during this process. In this study, we fabricated a transparent cathode back plate by depositing an ultra-thin film of single walled CNTs (SWCNTs) on an indium tin oxide (ITO)-coated glass substrate. Two types of phosphor anode plates were employed to our transparent cathode back plate: One is an ITO glass substrate with a phosphor layer and the other is a Cr-coated glass substrate with phosphor layer. For the former case, light was radiated from both the front and the back sides, where luminance on the back was ~30% higher than that on the front in our experiments. For the other case, however, light was emitted only from the cathode back side as the Cr layer on the anode glass rolled as a reflecting mirror, improving the light luminance as much as ~60% compared with that on the front of one. This study seems to be discussed about the morphologies and field emission characteristics of CNT emitters according to the experimental parameters in fabricating the lamps emitting light on the both sides or only on the cathode back side. The experimental procedures are as follows. First, a CNT aqueous solution was prepared by ultrasonically dispersing purified SWCNTs in deionized water with sodium dodecyl sulfate (SDS). A milliliter or even several tens of micro-liters of CNT solution was deposited onto a porous alumina membrane through vacuum filtration. Thereafter, the alumina membrane was solvated with the 3 M NaOH solution and the floating CNT film was easily transferred to an ITO glass substrate. It is required for CNT film to make standing CNTs up to serve as electron emitter through an adhesive roller activation.

  • PDF

Structural and Electrical Properties of Amorphous 2Ti4O12 Thin Films Grown on TiN Substrate (TiN 기판 위에 성장시킨 비정질 BaSm2Ti4O12 박막의 구조 및 전기적 특성 연구)

  • Park, Yong-Jun;Paik, Jong-Hoo;Lee, Young-Jin;Jeong, Young-Hun;Nahm, Sahn
    • Korean Journal of Materials Research
    • /
    • v.18 no.4
    • /
    • pp.169-174
    • /
    • 2008
  • The structural and electrical properties of amorphous $BaSm_2Ti_4O_{12}$ (BSmT) films on a $TiN/SiO_2/Si$ substrate deposited using a RF magnetron sputtering method were investigated. The deposition of BSmT films was carried out at $300^{\circ}C$ in a mixed oxygen and argon ($O_2$ : Ar = 1 : 4) atmosphere with a total pressure of 8.0 mTorr. In particular, a 45 nm-thick amorphous BSmT film exhibited a high capacitance density and low dissipation factor of $7.60\;fF/{\mu}m2$ and 1.3%, respectively, with a dielectric constant of 38 at 100 kHz. Its capacitance showed very little change, even in GHz ranges from 1.0 GHz to 6.0 GHz. The quality factor of the BSmT film was as high as 67 at 6 GHz. The leakage current density of the BSmT film was also very low, at approximately $5.11\;nA/cm^2$ at 2 V; its conduction mechanism was explained by the the Poole-Frenkel emission. The quadratic voltage coefficient of capacitance of the BSmT film was approximately $698\;ppm/V^2$, which is higher than the required value (<$100\;ppm/V^2$) for RF application. This could be reduced by improving the process condition. The temperature coefficient of capacitance of the film was low at nearly $296\;ppm/^{\circ}C$ at 100 kHz. Therefore, amorphous BSmT grown on a TiN substrate is a viable candidate material for a metal-insulator-metal capacitor.

A Study on the Measurement of River Ice Thickness by Using X-band Scatterometer (X-밴드 산란계를 이용한 하천 얼음 두께 측정에 관한 연구)

  • Han, Hyang-Sun;Kim, Bum-Jun;Lee, Hoon-Yol
    • Geophysics and Geophysical Exploration
    • /
    • v.15 no.1
    • /
    • pp.16-22
    • /
    • 2012
  • In this study, we setup a ground-based scatterometer using an antenna of which the center frequency is 9.5 GHz (X-band), and measured radar backscatterings from air/ice and ice/water interfaces to extract ice thickness. Both of air/ice and ice/water interfaces make strong radar backscatterings and so we can clearly identify two peaks in measured data by scatterometer. By using the distance of two peaks and refractive index of ice, we confirmed that it is possible to measure ice thickness. Field survey was performed at the downstream of Jiam River flowing into Chuncheon Lake. We measured radar backscattering from river ice along a survey path and extracted ice thickness. The ice thickness map of the downstream of Jiam River was produced by using kriging which is one of well known interpolation methods. The ice thickness was about 50 cm along the mainstream while ice was thin as 30 ~ 40 cm at a fast-flowing meander. Ice thickness was particularly thinner at some locations than that of surrounding areas even in the mainstream region of constant flow. This was because of impurities in ice or artificially formed refrozen holes after fishing. We expect that this study helps to expand utilization field of X-band SAR and airborne scatterometer system.