• Restorative Dentistry and Endodontics
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• 제32권3호
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• pp.208-221
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• 2007

파괴 인성 실험은 상아질-복합레진 계면의 파절 저항성을 평가할 수 있는 임상적으로 신뢰 할 만한 방법이다. 본 연구의 목적은 상아질-레진 계면의 파괴인성과 미세인장결합강도를 측정하여 이 두 실험방법이 상아질-레진 결합을 평가하는 데 가지는 유용성을 비교, 평가하는 것이다 파괴 인성 측정에는 short-rod 시편 형태를 이용하였다. 각 시편에서는 소의 하악절치에서 절단한 치아 절편을 포함시켜 결합면을 얻었다. 미세인장 결합강도 또한 소의 하악절치 순면을 연마하여 상아질을 노출시킨 후 상아질 접착제를 도포하고 레진 블록을 축조하여 측정하였다. 각 시편들은 $37^{\circ}C$ 증류수에 24시간 보관한 후 각 실험방법에 맞게 인장력을 가하여 측정치를 구하였다. 통계분석은 95% 신뢰수준의 ANOVA와 Tukey's test를 이용하였으며, 두 실험방법의 상관관계를 보기 위해 Pearson's 상관계수를 계산하였다. 전자현미경 검사를 통해 미세구조 또한 관찰하여 다음과 같은 결론을 얻었다. 1. 파괴인성은 SE군이 가장 높은 값을 나타냈으며, Adper Single Bond 2 (SB), OptiBond Solo (OB) ONE-STEP PLUS (OS), ScotchBond Multi-purpose (SM)군 순으로 나타났고, Clearfil SE Bond (SE)군은 다른 실험군에 비해 유의하게 높은 값을 나타내었으나 (p <0.05), 다른 실험군 사이에는 유의차가 없었다 (p > 0.05). 2. 미세인장결합강도는 SE군이 가장 높은 값을 나타냈으며, SB, OB, SM, 그리고 OS 순으로 나타났다. SB, OB, SM, SE군 사이에는 통계학적인 유의차가 없었으나 (p > 0.05), OS군의 미세인장결합강도는 다른 4개의 실험군에 비해 낮은 값을 나타내었다 (p < 0.05). 3. FE-SEM관찰에서 피막도가 두껍게 나타난 SM군, SE군과 피막도가 얇은 OS군, OB군, SB군 간에 파괴양상이 다르게 나타났다 즉 전자는 접착층 내 파괴가 일어난 반면, 후자는 resin tag나 레진 침투층 내에서 파절되는 양상을 나타내었다. 4. 파괴 인성과 미세인장결합강도 사이에는 통계학적으로 유의 한 상관 관계가 없었다 ($r^2=0.223$, t=0.927). 이와 같은 결과를 토대로, 상아질 접착제의 임상적 효율성을 평가하고자 할 때는 결합강도 뿐만 아니라. 파괴인성도 함께 고려하여 임상적용의 예견성을 높여야 한다고 결론내릴 수 있다.

• 대한소아치과학회지
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• 제34권2호
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• pp.285-291
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• 2007

상아질-레진 접착강도에 대한 collagenase와 esterase의 영향을 살펴보기 위해, 소구치의 교합면 상아질에 Single Bond 2와 Clearfil SE Bond로 접착을 시행하고 미세 시편을 제작하여 PBS collagenase 용액, esterase 용액에 4주간 보관한 후 미세인장결합강도를 측정, 비교하여 다음과 같은 결론을 얻었다. 1. 모든 보관 용액에서 Single Bond 2의 미세인장결합강도는 Clearfil SE Bond보다 유의하게 낮았다(p<0.05). 2. Single Bond 2의 미세인장결합강도는 collagenase군이 PBS군, esterase군보다 낮았다(p>0.05). 3. Clearfil SE Bond의 미세인장결합강도는 esterase군이 PBS군에 비해 낮았으나(p>0.05), collagenase군보다는 높았다(p>0.05). Collagenase군은 PBS군에 비해 유의하게 낮은 미세인장결합강도를 보였다(p<0.05).

• 대한소아치과학회지
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• 제33권4호
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• pp.693-698
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• 2006

유구치 1급 와동의 복합레진 수복 시 C-factor가 가장 크게 나타나며 중합수축에 의한 응력도 가장 크게 나타난다. 이 실험에서는 응력이 각 와동벽 위치에 따라 다르게 나타나는 양상을 microtensile bond strength(MTBS)실험을 통해 확인해보았다. 하악 제2유구치 20개를 두 개의 군으로 나누었다. 각각 다른 종류의 복합레진으로 수복하였고 개별 치아에서 각각 치수벽 시편과 축벽 시편을 얻어 총 4개의 군으로 나누었다. MTBS를 측정하였으며 통계적 유의성을 student T-test를 통해 검정하였다. ZP: Filtek Z250- 치수벽, ZA: Filtek Z250- 축벽, SP : Filtek Supreme - 치수벽, SA: Filtek Supreme - 축벽, 다음과 같은 결과를 얻을 수 있었다. 1. ZP군과 ZA군, SP군과 SA군 사이에서는 유의한 차이가 존재하였다(p<.001). 2. ZP군과 SP군, ZA군과 SA군 사이에서는 유의한 차이가 존재하지 않았다(p<.001).

• Restorative Dentistry and Endodontics
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• 제29권3호
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• pp.233-238
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• 2004

The purpose of this study was to evaluate the effect of immediate or delayed composite resin filling on dentinal microtensile bond strength (${\mu}TBS$) after applied the adhesive. The coronal dentin of human third molars was exposed. Single-Bond or One-Step was applied on the dentin surfaces. and composite resin were constructed immediately (group 1) or 5min., 10min., 15min., 20min. and 30min. (groups 2-6) after an adhesive was applied. The specimens were sectioned and made bar-shaped. Each surface area of them was about $1\textrm{mm}^2$. The ${\mu}TBS$ test was performed by EZ test. The results were analysed by One-way ANOVA and Tukey's test at 95% significance level. The results suggested that the ${\mu}TBS$ of Single-Bond to dentin was decreased when the composite resin was constructed 20min. and 30min. after Single-Bond was applied. But the ${\mu}TBS$ of One-Step was not affected by delayed composite resin filling.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2003년도 제120회 추계학술대회 제 5차 한ㆍ일 치과보존학회 공동학술대회
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• pp.609-609
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• 2003

I. Objectives The purpose of this study was to evaluate the effect of adhesive property on microtensile bond strength and to determine the failure mode. II. Materials and Methods Flat occlusal dentin surfaces were prepared using low-speed diamond saw. The dentin was etched with 37% phosphoric acid. The following adhesives were applied to the etched dentin according to manufacturer's directions；Scotchbond Multi-Purpose in group 1, Primer＆Bond NT in group 2, Scotchbond Multi-Purpose followed by Tetric-flow in group 3. After adhesive application, a cylinder of resin-based composite was built up the occlusal surface.(omitted)

• Restorative Dentistry and Endodontics
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• 제37권4호
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• pp.207-214
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• 2012

Objectives: This study evaluated the influence of chlorhexidine (CHX) on the microtensile bonds strength (${\mu}TBS$) of resin core with two adhesive systems to dentin in endodontic cavities. Materials and Methods: Flat dentinal surfaces in 40 molar endodontic cavities were treated with self-etch adhesive system, Contax (DMG) and total-etch adhesive system, Adper Single Bond 2 (3M ESPE) after the following surface treatments: (1) Priming only (Contax), (2) CHX for 15 sec + rinsing + priming (Contax), (3) Etching with priming (Adper Single Bond 2), (4) Etching + CHX for 15 sec + rinsing + priming (Adper Single Bond 2). Resin composite build-ups were made with LuxaCore (DMG) using a bulk method and polymerized for 40 sec. For each condition, half of specimens were submitted to ${\mu}TBS$ after 24 hr storage and half of them were submitted to thermocycling of 10,000 cycles between $5^{\circ}C$ and $55^{\circ}C$ before testing. The data were analyzed using ANOVA and independent t-test at a significance level of 95%. Results: CHX pre-treatment did not affect the bond strength of specimens tested at the immediate testing period, regardless of dentin surface treatments. However, after 10,000 thermocycling, all groups showed reduced bond strength. The amount of reduction was greater in groups without CHX treatments than groups with CHX treatment. These characteristics were the same in both self-etch adhesive system and total-etch adhesive system. Conclusions: 2% CHX application for 15 sec proved to alleviate the decrease of bond strength of dentin bonding systems. No significant difference was shown in ${\mu}TBS$ between total-etching system and self-etching system.

• Restorative Dentistry and Endodontics
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• 제29권5호
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• pp.430-438
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• 2004

This study evaluated the influence of application time of self-etching primers on microtensile bond strength (${\mu}$TBS) to dentin using three self-etching primer adhesive systems. Dentin surfaces were exposed from forty-eight human molars. They were conditioned with three self-etching primers (Clearfil SE Bond [SE], Unifil Bond [UF], Tyrian SPE + One Step Plus [TY]) and different primining times (10s, 20s, 30s and 40s). Composite resins were bonded to dentin surfaces and specimens were made. ${\mu}TBS$ was tested and statistically compared using by one-way ANOVA and Tukey's Test. The results of this study presented that priming time for 10s in SE and UF groups and for 30s and 40s in TY group was highly decreased ${\mu}TBS$ to dentin.

• The Journal of Advanced Prosthodontics
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• 제7권4호
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• pp.317-322
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• 2015

PURPOSE. The aim was to evaluate the effect of curing mode and different dentin surface pretreatment on microtensile bond strength (${\mu}TBS$) of self-adhesive resin cements. MATERIALS AND METHODS. Thirty-six extracted human permanent molars were sectioned horizontally exposing flat dentin surface. The teeth were divided into 12 groups (3 teeth/group) according to the dentin surface pretreatment methods (control, 18% EDTA, 10% Polyacrylic acid) and curing mode (self-curing vs. light-curing) of cement. After pretreatment, composite resin blocks were cemented with the following: (a) G-CEM LinkAce; (b) RelyX U200, followed by either self-curing or light-curing. After storage, the teeth were sectioned and ${\mu}TBS$ test was performed using a microtensile testing machine. The data was statistically analyzed using one-way ANOVA, Student T-test and Scheffe's post-hoc test at P<.05 level. RESULTS. For G-CEM LinkAce cement groups, polyacrylic acid pretreatment showed the highest ${\mu}TBS$ in the self-cured group. In the light-cured group, no significant improvements were observed according to the dentin surface pretreatment. There were no significant differences between curing modes. Both dentin surface pretreatment methods helped to increase the ${\mu}TBS$ of RelyX U200 resin cement significantly and degree of pretreatment effect was similar. No significant differences were found regarding curing modes except control groups. In the comparisons of two self-adhesive resin cements, all groups within the same pretreatment and curing mode were significantly different excluding self-cured control groups. CONCLUSION. Selecting RelyX U200 used in this study and application of dentin surface pretreatment with EDTA and polyacrylic acid might be recommended to enhance the bond strength of cement to dentin.

• Restorative Dentistry and Endodontics
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• 제43권4호
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• pp.40.1-40.10
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• 2018

Objectives: This study evaluated the microtensile bond strength (${\mu}TBS$) of polymer-ceramic and indirect composite resin with 3 classes of resin cements. Materials and Methods: Two computer-aided design/computer-aided manufacturing (CAD/CAM)-fabricated polymer-ceramics (Enamic [ENA; Vita] and Lava Ultimate [LAV; 3M ESPE]) and a laboratory indirect composite resin (Gradia [GRA; GC Corp.]) were equally divided into 6 groups (n = 18) with 3 classes of resin cements: Variolink N (VAR; Vivadent), RelyX U200 (RXU; 3M ESPE), and Panavia F2 (PAN; Kuraray). The ${\mu}TBS$ values were compared between groups by 2-way analysis of variance and the post hoc Tamhane test (${\alpha}=0.05$). Results: Restorative materials and resin cements significantly influenced ${\mu}TBS$ (p < 0.05). In the GRA group, the highest ${\mu}TBS$ was found with RXU ($27.40{\pm}5.39N$) and the lowest with VAR ($13.54{\pm}6.04N$) (p < 0.05). Similar trends were observed in the ENA group. In the LAV group, the highest ${\mu}TBS$ was observed with VAR ($27.45{\pm}5.84N$) and the lowest with PAN ($10.67{\pm}4.37N$) (p < 0.05). PAN had comparable results to those of ENA and GRA, whereas the ${\mu}TBS$ values were significantly lower with LAV (p = 0.001). The highest bond strength of RXU was found with GRA ($27.40{\pm}5.39N$, p = 0.001). PAN showed the lowest ${\mu}TBS$ with LAV ($10.67{\pm}4.37N$; p < 0.001). Conclusions: When applied according to the manufacturers' recommendations, the ${\mu}TBS$ of polymer-ceramic CAD/CAM materials and indirect composites is influenced by the luting cements.

• 대한소아치과학회지
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• 제45권3호
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• pp.299-306
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• 2018

본 연구의 목적은 산부식 시간과 접착제 적용에 따른 유구치 치면열구전색제의 미세인장 결합강도를 평가하여 비교하는 것이다. 40개의 발거된 건전한 하악 유구치를 선정하여 산부식을 시행하지 않은 군과 산부식을 각각 15, 30, 60초 시행한 군으로 분류하였다. 이를 다시 접착제를 적용하지 않은 군과 적용한 군으로 나누었다. 각 군의 치아에 치면열구 전색제를 도포하여 시편을 제작한 후 미세인장 결합강도를 측정하였다. 산부식을 시행한 15, 30, 60초에 따라 미세인장 결합강도는 유의한 차이가 없었다. 전색제를 적용하기 전에 접착제를 적용한 경우가 산부식만 시행한 경우보다 더 높은 결합강도를 보였으며(p < 0.05), 산부식 시간에 따른 유의한 차이는 없었다. 결론적으로, 유구치의 교합면 법랑질에서 산부식 시간이 15초 이상이면 전색제의 미세인장 결합강도는 유의하게 증가하지 않았으며, 치면열구전색제 도포 전에 접착제를 적용하는 것은 결합강도를 증가시켰다.