• 한국전기전자재료학회논문지
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• 제12권1호
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• pp.56-61
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• 1999

Highly conductive oxide films of BaRuO$_3$ have been grown heteroepitaxially on (100) LaAlO$_3$ single crystalline substrates by using pulsed laser deposition. The films are c-axis oriented with an in-plane epitaxial relationship of <010><100>BaRuO$_3$ // <110>LaAlO$_3$. Atomic force microscopy (AFM) observation shows that they consist of a fine-arranged network of grains and have a mosaic microstructure. Generally temperature-dependent resistivity shows the transition from metallic curve to semiconductor-metallic twofold curve by the deposition conditions for Ru oxide based materials like SrRuO$_3$, CaRuO$_3$, BaRuO$_3$, etc.. This twofold curve comes from the structural similarity of Ru oxide based materials including BaRuO$_3$. We find that the distance of Ru-Ru bonding in the unit cell of BaRuO$_3$ as well as the grain boundary scattering could be the two important causes of these interesting conductive properties.

• Tribology and Lubricants
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• 제11권4호
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• pp.45-52
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• 1995

The wear behavior of alumina short fiber reinforced tin-bronze matrix composites was studied at the room temperature and an elevated temperature. The effect of the composition of specimens and the variation of wear conditions on the wear properties was examined by a pin-on-disc type wear testing machine. The wear mechanism according to the compositon of specimens at various wear conditions was discussed by the observation of the microstructure and the analysis of the composition on the worn surfaces. A thicker oxide layer on worn surfaces led to a lower wear loss because of the lubricating effect of oxide layers between pin and disc. As the testing temperature was raised to 350$^{\circ}$C, the fiber reinforced composites exibited markedly increased wear resistance even at a higher applied load since the reinforcement of composites with alumina fibers was not affected to a large extent by raising temperature. The results obtained by AES and EDS analysis indicated that the oxide layer of the worn surfaces formed at 350$^{\circ}$C was proved as Fe-oxide. This was explained by the faster formation of Fe-oxide than Cu-oxide at 350$^{\circ}$C.

• Tribology and Lubricants
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• 제31권6호
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• pp.287-293
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• 2015

Laser surface texturing (LST), a surface engineering modification, has been considered as one of the new processes used to improve tribological characteristics of materials by creating artificially patterned microstructure on the contact surface of mechanical components. In LST technology, the laser is optimized to obtain or manufacture the dimples with maximum precision. The micro-dimples reduce the coefficients of friction and also improve the wear resistance of materials. This study investigates the effect of dimple density is investigated. For this purpose, a ball-on-disc type tester is used with AISI 52100 bearing steel as the test material. Discs are textured with a 5% and 10% dimple density. Experimental work is performed with normal loads of 5 N, 10 N, and 15 N under a fixed speed of 150 rpm at room temperature. The effect of the textured surface is compared to that of the untextured one. Experimental results show that the textured surface yields lower friction coefficients compared to those of untextured surfaces. Specifically, the 10% dimple density textured surface shows better friction reduction behavior than the 5% dimple density textured sample, and has an 18% improvement in friction reduction compared with the untextured samples. Microscopic observation using a scanning electron microscope (SEM) shows that the major friction mechanisms of the AISI 52100 bearing steel are adhesion, plastic deformation, and ploughing.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 춘계학술대회 논문집
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• pp.321-324
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• 2005

The main purpose of the present study has been placed on investigating the effects of controlled rolling and cooling on the microstructures and mechanical properties of C-Si-Mn-V steels for cold forming. The steels were manufactured in vacuum induction melting(VIM) furnace and casted to 1.1ton Ingots and the ingots were forged to $\Box150$ billet. The forged billets were reheated in walking beam furnace and rolled to coil, the stocks were rolled by Controlled Rolling and Cooling Technology (CRCT), so rolled at low temperature by water spraying applied in rolling stage and acceleratly cooled before coiling. Rolled coils were cold drawed to the degree of $27\%$ of area reduction without heat treatment. Microstructual observation, tensile test, compression test and charpy impact tests were conducted. The mechanical properties of the steels were changed by area reduction of cold drawing and it is founded that there are optimum level of cold drawing to minimize compression stress for these steels. From the result of this study, it is conformed that mechanical properties and microstructure of C-Si-Mn-V steels for cold forming were enhanced by accelerated cooling and founded optimum level of cold drawing.

• 열처리공학회지
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• 제18권4호
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• pp.235-241
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• 2005

Thermal creep properties of the advanced zirconium fuel claddings named by HANA alloys which were developed for high burn-up application were evaluated. The creep test of HANA cladding tubes was carried out by the internal pressurization method in temperature range from 350 to $400^{\circ}C$ and in the hoop stress range from 100 to 150 MPa. Creep tests were lasted up to 800 days, which showed the steady-state secondary creep rate. The creep resistance of HANA fuel claddings was affected by final annealing temperature and various factors, such as alloying element, applied stress and testing temperature. From the results the microstructure observation of the samples before and after creep test by using TEM, the dislocation density was increased in the sample of after creep test. The Sn as an alloying element was more effective in the creep resistance than other elements such as Nb, Fe, Cr and Cu due to solute hardening effect of Sn. In case of HANA fuel claddings, the improved creep resistance was obtained by the control of final heat treatment temperature as well as alloying element.

• 환경생물
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• 제35권4호
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• pp.515-520
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• 2017

Sexual dimorphism of the mouthpart, antenna and mandible of the Cyllorhynchites ursulus in South Korea was studied with linear measurements. The mouthpart and antenna measurements were conducted with a stereoscopic microscope using 122 specimens (72 males and 50 females). Microscopic observation of the mandible were conducted with a Field Emission Scanning Electron Microscope (FE-SEM) using 103 specimens (73 males and 30 females). Results showed that the size difference between males and females was significant in the size of the mouthpart and antenna. On the other hand, we could not detect sexual size dimorphism in the microstructure of the mandible. The bivariate plots made by the result of Principal Component Analysis (PCA) and Discriminant Analysis (DA) showed a size dimorphism in the size of the mouthpart and the antenna between males and females. Based on our study, sexual dimorphism in the mouthpart and antenna exists in C. ursulus from the South Korean population, and this difference seems to be related to the behavioral differences between males and females.

• 한국표면공학회지
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• 제47권5호
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• pp.215-220
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• 2014

Electrodeposition behaviors of Pd-Ni alloys were investigated from the polarization curves in a solution containing ethylenediamine as complexing agent. The microstructure and hardness of electrodeposited Pd-Ni alloys were also characterized. Codeposition of Pd-Ni alloys was successfully performed in the wide current density ranging from 2 to $5000A{\cdot}m^{-2}$ because the deposition potential of Pd became close to that of Ni in the ethylenediamine-contained solution. It was also found from X-ray diffraction patterns that the solid solution between Pd and Ni was formed with variation of the composition of alloys. The measured hardness of Pd-Ni alloys increased with increasing the contents of Ni due to solid solution strengthening and grain refinement. The electrodeposited Pd-Ni alloys also exhibited a crack free smooth surface morphology from the SEM observation.

• 대한금속재료학회지
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• 제46권12호
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• pp.817-822
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• 2008

Metal matrix composite (MMC) materials having low electrical contact resistance based on 316L stainless steel (STS) matrix alloy with $ZrB_2$ particles were fabricated for PEMFC (Polymer Electrolyte Membrane Fuel Cell) separator by powder metallurgy (PM). The effects of the boride particle addition into the matrix alloy on microstructure, surface morphology, and interfacial contact resistance (ICR) between the samples and gas diffusion layer (GDL) were investigated. Both conventional and PM 316L STS samples showed high ICR due to the existence of non-conductive passive film on the alloy surface. The addition of the boride particles, however, remarkably reduced ICR of the samples. SEM observation revealed that the boride particles were protruded out of the matrix surface and particle density existing on the surface increased with increasing the boride content, causing increase of the total contact area between the conductive particles and GDL. ICR of the samples also decreased with increasing the boride content resulted from the increased contact area.

• 대한금속재료학회지
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• 제48권8호
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• pp.717-723
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• 2010

The degradation behavior of fuel cladding is a very import concern in nuclear power generation, because the operation of nuclear plants can be limited by fuel cladding degradation. In order to evaluate the hydride effect on failure of zirconium fuel claddings, a ring tensile test for the circumferential direction was carried out at room temperature for claddings having different hydride characteristics such as density and orientation; microstructural evaluation was also performed for those claddings. The circumferential failure of the claddings was promoted by increasing the hydride concentration in the matrix; however, the failure of the claddings was affected by the hydride orientation rather than by the hydride concentration in the matrix. From fracture surface observation, the cladding failure during the ring tensile test was matched with the hydride orientation.

• 대한금속재료학회지
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• 제50권1호
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• pp.13-22
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• 2012

Forged and flat-bar rolled STD11 tool steel shows anisotropic dimensional change during heat treatment. The dimensional change in the rolling direction is larger than that in the transverse direction. The cause of the anisotropic dimensional change is that the steel is anisotropic in composition, microstructure and other properties. The decrease of anisotropic distortion in tool steel is important for making better precision cold working dies. In this study, the effect of ingot weight and hot rolling reduction ratio on the anisotropic dimensional change of STD11 during heat treatment has been studied. Dimensional change was evaluated by simulating a real heat treatment process, including gas quenching and tempering. Experimental results showed that all the rolled flat-bar products had anisotropic distortion to some degree, but the anisotropic distortion was reduced as hot rolling ratio increased. Ingot weight had a little effect on anisotropic distortion. Microstructural observation showed that the anisotropic dimensional change of STD11 tool steel was closely related to the amount, shape and distribution of coarse carbides.