• Korean Journal of Materials Research
• /
• v.29 no.3
• /
• pp.137-142
• /
• 2019

The microstructure, phase, and mechanical properties of three aged porcelain insulators which were manufactured in different years (1973, 1995 and 2008) and which were used in the field for different amounts of time, were investigated. With X-ray 3D computed tomography (CT), defects with ~mm size can be detected without destroying the aged insulators. Defects of small specimens, which are cut from the aged insulators and polished, are analyzed with optical and scanning electron microscopy (OM and SEM), and defects of um size are detected by OM and SEM. The number and size of defects in all the aged insulators are similar. Porcelain insulators manufactured in 1973 contain more $SiO_2$ (quartz and cristobalite) than those manufactured in 2008. Those manufactured in 2008 contain more $Al_2O_3$ than those manufactured earlier. The Vickers hardness of the insulator manufactured in 1973 has the lowest value. The formation of the cristobalite ($SiO_2$) in the insulator manufactured in 1973 which can come from the phase transformation of quartz can cause stress in the insulator by formation of microcracks, which can lead to the low hardness of the insulator.

• Journal of Powder Materials
• /
• v.28 no.5
• /
• pp.403-409
• /
• 2021

In this study, Ti-Mo-EB composites are prepared by ball milling and spark plasma sintering (SPS) to obtain a low elastic modulus and high strength and to evaluate the microstructure and mechanical properties as a function of the process conditions. As the milling time and sintering temperature increased, Mo, as a β-Ti stabilizing element, diffused, and the microstructure of β-Ti increased. In addition, the size of the observed phase was small, so the modulus and hardness of α-Ti and β-Ti were measured using nanoindentation equipment. In both phases, as the milling time and sintering temperature increased, the modulus of elasticity decreased, and the hardness increased. After 12 h of milling, the specimen sintered at 1000℃ showed the lowest values of modulus of elasticity of 117.52 and 101.46 GPa for α-Ti and β-Ti, respectively, confirming that the values are lower compared to the that in previously reported studies.

• Journal of the Korean institute of surface engineering
• /
• v.34 no.5
• /
• pp.421-428
• /
• 2001

New WC-CrN superlattice film was deposited on Si substrate (500$\mu\textrm{m}$) using cathodic arc ion plating system. The microstructure and mechanical properties of the film depend on the superlattice period (λ). In the X-ray diffraction analysis (XRD), preferred orientation of microstructure was changed according to various superlattice periods(λ). During the Transmission Electron Microscope analysis (TEM), microstructure and superlattice period (λ) of the WC - CrN superlattice film was confirmed. Hardness and adhesion of the deposited film was evaluated by nanoindentation test and scratch test, respectively. As a result of nanoindentation test, the hardness of WC - CrN superlattice film was gained about 40GPa at superlattice period (λ) with 7nm. Also residual stress with various superlattice period (λ) was measured on Si wafer (100$\mu\textrm{m}$) by conventional beam-bending technique. The residual stress of the film was reduced to a value of 0.2 GPa by introducing Ti - WC buffer layers periodically with a thickness ratio ($t_{buffer}$/$t_{buffer+superlattice}$ ). To the end, for the evaluation of oxidation resistance at the elevated temperature, CrN single layer and WC - CrN superlattice films with various superlattice periods on SKD61 substrate was measured and compared with the oxidation resistance.

• Transactions of Materials Processing
• /
• v.32 no.2
• /
• pp.67-73
• /
• 2023

To overcome a climate change, manufacturing complex-shaped electric mobility parts becomes one of the important issues for enhancing a performance of motor with reducing their weight. Therefore, development of laser-based additive manufacturing shed on light due to their flexible manufacturing capacity that can be suitable to solve the poor formability of Fe-Si alloys for electric mobility parts. Although there are several studies existed to optimize the performance of additively manufactured Fe-Si alloys, the post-annealing effect was not well investigated yet though this is important to control the texture and mechanical properties of additively manufactured parts. In the present work, annealing effect on the mechanical property and microstructure of additively manufactured Fe-4.5Si alloy was investigated. Because of the ordered phase initiation after annealing, the hardness of additively manufactured Fe-4.5Si alloy increased up to 1173 K while a hardness drop occurs at the 1273 K condition due to the micro-crack initiation. The response surface methodology result represents the 1173 K-5 h sample is an optimal condition to maximize the mechanical property of additively manufactured alloy without micro-cracks.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2007.05a
• /
• pp.389-393
• /
• 2007

The most demanded bimetals in home appliances are manufactured by mainly cladding process and these are mainly consist of Cu alloy and Ni alloy. But it is very difficult to clad these alloys, because the brittle ${Cu_3}{O_4}$ oxide film formed easily on Cu alloy surface during cladding process. Clad rolling and heat treatment processes were applied for the development of bimetals by using the Ni alloy and the 3 types of Cu alloys. Optical microstructure was observed and micro-hardness, specific resistance, deflection were measured from the manufactured new bimetals specimens.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2009.10a
• /
• pp.173-176
• /
• 2009

A great emphasis has been placed on the design of heat treatment process to achieve desired microstructure and mechanical property of final product. In this study, finite element analysis was carried out to predict temperature, microstructure and hardness of eutectoid steel after water quenching. Convective heat transfer coefficients were determined by inverse analysis using surface temperatures measured with three different installation methods of thermocouples. Finally, the effect of convective heat transfer coefficients on the prediction of temperature history and hardness was analyzed by comparing experimental and simulation results.

• Transactions of the Korean Society of Machine Tool Engineers
• /
• v.15 no.1
• /
• pp.102-107
• /
• 2006

This study investigates the properties as the difference friction welding area on SM25C steel rod. The tensile and bending strength and of welded joints, the hardness distribution of welds, the microstructure of welds and the tensile fracture surfaces were mainly investigated through this experiment. The fixed friction welding conditions were revolution 2000rpm, friction pressure 70Mpa, friction time 1.5sec, upset pressure 100Mpa, upset time 2.0sec, upset length 2.8mm and changeable friction welding parameter was friction welding area.

• Laser Solutions
• /
• v.7 no.2
• /
• pp.27-38
• /
• 2004

Laser remelting of surface of cobalt-based hardfacing alloy can eliminate impurities and cracks and improve the wear resistance. In this present study, Stellite ${\sharp}6\;and\;{\sharp}21$ harfacing alloys were remelted by a 3kW CO2 laser. Hardness distribution and microstructures in the laser remelted zone was investigated. Our results showed that in proper laser parameters laser remelted surface of hardfacing alloy had more refined microstructure and more increased micro-hardness than the base material.

• Journal of Welding and Joining
• /
• v.23 no.1
• /
• pp.77-85
• /
• 2005

The structures and mechanical properties of friction stirred welds of oxygen free copper(OFC) sheet were investigated. Defect-free welds were obtained in a relatively wide range of the welding conditions from 1000 to 2000 rpm, and welding speed from 500 to 2000 mm/min. The microstructure of the stirred zone(SZ) showed recrystallized grains, and the gram size varied largely with the welding conditions. The SZ hardness values including those of all the optimum welding conditions were slightly lower than that of the base metal, and increased with decreasing heat input. The tensile strength of the all-SZ increased with increasing the hardness values. The Hall-Fetch relationship was confirmed between the yield strength of the all-52 and the recrystallized grain size of the SZ.

• Journal of the Korean Society for Precision Engineering
• /
• v.21 no.12
• /
• pp.29-36
• /
• 2004

In this paper, a new replication technique for a real 3D microstructure was introduced, in which a master Pattern WES made of photo-curable epoxy using a microstereolithography technology, and then it was transferred onto an epoxy-copper particle composite. A helical gear was selected as one of the real 3D microstructure for this study, and it was replicated from a pure epoxy to an epoxy composite. In addition, the transferability of the microreplication process was evaluated, and the properties of :he epoxy composite were compared to that of the pure epoxy, including hardness, wear-resistance and thermal conductivity.