• Title/Summary/Keyword: micro-degree

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Fabrication of Al Flake Powder for Pigment (안료용 알루미늄 플레이크 분말 제조)

  • 홍성현;김병기
    • Journal of Powder Materials
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    • v.10 no.6
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    • pp.415-421
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    • 2003
  • The study for producing the flake powders by milling of aluminum foil and gas atomized powders was carried out. The effects of lifter bars on the ball motions and milling of aluminum foils were also investigated. The aluminum foils were laminated each other, elongated, fragmented into small foils and finally formed into the flake powders during the dry ball-milling. The spherical atomized-powders were milled to coarse flake powders with high aspect ratio and then changed to fine flake powders with lower aspect ratio. Even though long times were required for making flake powders by milling of foils, the water covering areas of them were higher than those of powders milled using gas-atomized powders, suggesting aluminum foils were more plastically deformed by micro-forging. On the other hand, as the number of lifter bars increased, the necessary rotation speeds of milling jar for cascading mode and cataracting mode decreased drastically. It was possible to achieve same quality of milled flake powder by using the lifter bars under the lower milling speeds. The painting test showed that the appearance of painted surface was good and optimum content range of aluminum paste in car paint to maximize the degree of gloss was 3-5%.

Neuro-fuzzy based prediction of the durability of self-consolidating concrete to various sodium sulfate exposure regimes

  • Bassuoni, M.T.;Nehdi, M.L.
    • Computers and Concrete
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    • v.5 no.6
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    • pp.573-597
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    • 2008
  • Among artificial intelligence-based computational techniques, adaptive neuro-fuzzy inference systems (ANFIS) are particularly suitable for modelling complex systems with known input-output data sets. Such systems can be efficient in modelling non-linear, complex and ambiguous behaviour of cement-based materials undergoing single, dual or multiple damage factors of different forms (chemical, physical and structural). Due to the well-known complexity of sulfate attack on cement-based materials, the current work investigates the use of ANFIS to model the behaviour of a wide range of self-consolidating concrete (SCC) mixture designs under various high-concentration sodium sulfate exposure regimes including full immersion, wetting-drying, partial immersion, freezing-thawing, and cyclic cold-hot conditions with or without sustained flexural loading. Three ANFIS models have been developed to predict the expansion, reduction in elastic dynamic modulus, and starting time of failure of the tested SCC specimens under the various high-concentration sodium sulfate exposure regimes. A fuzzy inference system was also developed to predict the level of aggression of environmental conditions associated with very severe sodium sulfate attack based on temperature, relative humidity and degree of wetting-drying. The results show that predictions of the ANFIS and fuzzy inference systems were rational and accurate, with errors not exceeding 5%. Sensitivity analyses showed that the trends of results given by the models had good agreement with actual experimental results and with thermal, mineralogical and micro-analytical studies.

Preparation of Reproducible and Responsive Scar Model and Histology Analysis

  • Kim, Sang-Cheol;ChoLee, Ae-Ri
    • Journal of Pharmaceutical Investigation
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    • v.40 no.1
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    • pp.45-49
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    • 2010
  • Unlike human, with some exceptions, animals do not heal with excessive scar. The lack of suitable animal model has hindered the development of effective scar therapy. We previously reported that partial thickness rabbit ear wound model resembles human wound heal process. This study was designed to prepare a hypertropic scar wound model which can be employed for testing anti-scar therapy. Four wounds were created down to the bare cartilage on the anterior side of each rabbit ear using 8-mm dermal biopsy punch and histology analysis at post operation day (POD) 5, 28 and 48 were performed. As the outcome of scar formation is largely determined by the early inflammatory response to the wounding and the degree and the duration of occlusion, cephalodin(50 mg/kg) was injected daily and medical occlusive dressings were applied. Five micro wound and scar sections were stained with hematoxylin and eosin for quantification of epidermal regeneration and scar hypertrophy. Sections were also stained using Masson's trichrome and Sirius red to evaluate collagen organization and rete ridge formation. Wound closure process was assessed to 7wks post wounding. Complete removal of the epidermis, dermis and perichondrial layer caused delayed epithelialization, which results in hypertropic scarring. The inability of the wounds to contract and the delay in epithelialization in rabbit ear was likely due to cartilage and it created scar elevation. The results suggest that full thickness surgical punch wound model in rabbit ear could be employed as a reliable and reproducible scar wound model for testing anti-scar therapy.

Optimization of HVOF Spray Parameters for $Cr_3C_2 - 7wt%NiCr$ Coating Powder by Experimental Design Method (실험계획법에 의한 $Cr_3C_2 - 7wt%NiCr$ 용사분말의 HVOF 용사변수 최적화)

  • 김병희;서동수
    • Journal of Welding and Joining
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    • v.15 no.1
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    • pp.125-134
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    • 1997
  • This study was conducted by L9 orthogonal array to obtain optimum spray parameters for This study was conducted by L9 orthogonal array to obtain optimum spray parameters for $Cr_3C_2 - 7wt%$(80wt%Ni-20wt%Cr) coating powder. The factors were hydrogen flow rate, oxygen flow rate, gun-to-work distance, powder feed rate. And evaluation methods for the coating were surface roughness, oxygen concentration, micro-hardness, pore size and distribution, low angle ($30^{\circ}$) erosion rate, and microstructure of coating. The optimum HVOF spray conditions were proved as follows : hydroen flow rate ; 681 SLPM, oxygen flow rate ; 215 SLPM $H^2/O^2 ratio= 3.16), gun-to-work distance ; 22cm, powder feed rate; 25g/min. The hardness (Hv300) was 1147 and the erosion rate ($30^{\circ}$degree) was $3.16\times10^{-4}$g/g. It is believed that the optimized spray conditions can be improved the wear-resistance and anti-erosion characteristics of the coating.

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Precipitation of Eu3+ - Yb3+ Codoped ZnAl2O4 Nanocrystals on Glass Surface by CO2 Laser Irradiation

  • Bae, Chang-hyuck;Lim, Ki-Soo;Babu, P.
    • Current Optics and Photonics
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    • v.2 no.1
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    • pp.79-84
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    • 2018
  • We present a novel and simple method to enable spatially selective $ZnAl_2O_4$ nanocrystal formation on the surface of $B_2O_3$-$Al_2O_3$-ZnO-CaO-$K_2O$ glass by employing localized laser heating. Optimized precipitation of glass-ceramics containing nanocrystals doped with $Eu^{3+}$ and $Yb^{3+}$ ions was performed by controlling $CO_2$ laser power and scan speed. Micro-x-ray diffraction and transmission electron microscopy revealed the mean size and morphology of nanocrystals, and energy dispersive x-ray spectroscopy showed the lateral distribution of elements in the imaged area. Laser power and scan speed controled annealing temperature for crystalization in the range of 1.4-1.8 W and 0.01-0.3 mm/s, and changed the size of nanocrystals and distribution of dopant ions. We also report more than 20 times enhanced downshift visible emission under ultraviolet excitation, and 3 times increased upconversion emission from $Eu^{3+}$ ions assisted by efficient sensitizer $Yb^{3+}$ ions in nanocrystals under 980 nm excitation. The confocal microscope revealed the depth profile of $Eu^{3+}$ ions by showing their emission intensity variation.

A Research on the Analysis Method of School Exterior Space Lacking Natural Surveillance (학교 외부공간의 자연적 감시 취약지역 분석기법에 관한 연구)

  • Kweon, Ji-Hoon
    • The Journal of Sustainable Design and Educational Environment Research
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    • v.11 no.1
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    • pp.23-31
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    • 2012
  • The number of school crime has grown continuously for last ten years and its intensity also has reached to serious condition. The concept of CPTED(Crime Prevention through Environmental Design) needs to be focused for improving school environment regarding this context. The exterior space of school environment is variously exposed to school crimes committed by colleague students and also intruders. From the perspective of school CPTED, Natural surveillance as one of the practical strategies requires the micro-scale analysis which clarifies local visibility at each different school exterior space. Thus, the purpose of this research is to develop the analysis method clarifying visibility condition at exterior space of school environment, which supports finding the condition of natural surveillance. The programmed analysis algorithm generated quantitative results clarifying Degree for static visibility and Clustering Coefficient for user tracking visibility. The result of this study produced the analysis method feasible to clarify weak natural surveillance conditions at school exterior spaces. Also, it is expected that the developed analysis method will be used to improve the layout of school exterior space from the perspective of CPTED.

A Piezoelectric Immunosensor for Early Cervical Cancer Detection

  • Yang, Li;Huang, Xianhe;Sun, Liang
    • Asian Pacific Journal of Cancer Prevention
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    • v.15 no.21
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    • pp.9375-9378
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    • 2014
  • Background: A piezoelectric immunosensor for early cervical cancer detection was developed involving short analyis time and less invasive technique for $p16^{INK4a}$, a protein that has been linked to cervical cancer. Materials and Methods: $5{\mu}L$ of 5.0 mg/mL $p16^{INK4a}$ antibody and then supernatant from different clinical samples from West China Second University Hospital (Sichuan, China) were dripped on the center of the AT-cut crystal through a micro-injector. Absorption of the $p16^{INK4a}$ by antibody caused a shift in the resonant frequency of the immunosensor, and the resonant frequency was correlated to the amount of the $p16^{INK4a}$ in the supernatant. Results: The greater severity of lesion grading, the greater the expression level of $p16^{INK4a}$. Conclusion: Degree of cervical cancer lesion development could be determined by detected amount of $p16^{INK4a}$ in different clinical samples.

A Measuring Method for 3-DOF Displacement by Using Spherical Reflector (구면 반사체를 이용한 3 자유도 변위 측정 기법)

  • Kwon, Ki-Hwan;Moon, Hong-Kie;Cho, Nahm-Gyoo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.12
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    • pp.2687-2694
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    • 2002
  • A precision displacement measuring system is proposed, which can detect the 3-DOF translational motions of precision positioning devices. The optical system, which is composed of two diode-laser sources and two quadratic PSDs, is adapted to detect the position of the spherical reflector usually mounted on the platform of positioning devices. Each of the laser beams from diode-laser sources is reflected at the highly reflective surface of the sphere; hence, the 3-dimensional position of the sphere causes the directional change of the reflected beams, which is detected by the PSDs. In this paper, we define the relationships between the output values of the two PSDs and the 3-DOF translational motions of the sphere. Based on a deduced measurement model, we perform measurement simulation and evaluate the performance of the proposed measurement system: linearity, sensitivity, measuring range, and measurement error. The results show that the proposed measuring method is very useful for the measurement of the precision displacement of 3-DOF micro motions.

Study on Erosion Characteristics of Aged HK40 Steel (열화된 HK40강의 마식특성에 관한 연구)

  • Kim, Am-Kee;Chun, Yong-Du;Lee, Kum-Bae;Kim, Chang-Hoon;Nahm, Seung-Hoon
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.403-408
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    • 2003
  • The erosion behavior of :artificially aged HK40 steel was investigated. Erosion tests were conducted at room temperature, $200^{\circ}C$ and $400^{\circ}C$ using $Al_2O_3$ particles. Erosion rates increased with increment of temperature. The maximum erosion rate increased with the impingement angle of 30 degree. The erosion rate increased, reached the maximum at 1000 hours, and after that, decreased with heat treatment time. The mechanism of erosion seems to be the cutting wear which is very much associated with the strength of material. As results, the erosion rates were rather affected by the tensile strength and the strain hardening coefficient than the hardness and the yield strength. Such changes of material properties would be caused by the change of micro-structure due to the precipitation of carbide and the dissolution of solid element within matrix during the heat treatment.

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Structural Changes during Oxidation Process of Anisotopic Mesophase Carbon fibers(I) - TEM and XRD Study (산화반응에 의한 이방성 메조페이스 탄소섬유의 구조 변화(I) - TEM 및 XRD를 이용한 분석)

  • Roh, J.S.
    • Korean Journal of Materials Research
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    • v.13 no.12
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    • pp.825-830
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    • 2003
  • Structural changes during oxidation of anisotopic mesophase carbon fiber(AMCFs) have been observed with TEM and XRD. It was shown that the AMCFs are three dimensionally stacked structure of turbostratic layers, and are non-homogeneous structure which consist of the highly ordered areas and the random areas. The $d_{ 002}$, Lc, and La of AMCFs which were measured by XRD were 3.44, 146, and $135\AA$, respectively. It was observed that the oxidation initiated at the random areas, because the $d_{002}$ / decreased to the value of 3.41 $\AA$ during initial oxidation stage. It was also observed that the La of the oxidized AMCFs increased up to 182 $\AA$ during the whole oxidation process, and the $d_{002}$ of that increases up to 9.44 $\AA$ when the burn-off is over the degree of 20%. Therefore, it was suggested that the micro-crystalline grew up by heat treatment effects during the fibers were oxidized, In addition, it was shown that there was difference in the measured value of La by XRD and TEM, in case of 39% oxidized fibers for example, the measured La was $ 165\AA$ by XRD and in the range of 180∼220 $\AA$ by TEM.