• Proceedings of the KSR Conference
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• 2005.11a
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• pp.344-349
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• 2005

Cast steels have been mainly in rod type couplers which connect railway vehicles. These components, as important members, are exposed to repeat to repeated stresses and impact loading during stop and departure service for a long tie. The coupler suffers fatigue crack initiations and demage that cause need to repair weldment due to these loading conditions. Therefore, the heat affected zone of cast steel couple in rod type were evaluated in view of metallurgical weld characteristics after repair welding at laboratory. The specimens with two different welding techniques were evaluated after several welding conditions and post-heat treatments. Micro-vickers hardness and tensile tests and microstructural observations were conducted on heat affected zone of the weldment according to repair weld and post-heat treatment.

• Journal of Surface Science and Engineering
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• v.35 no.2
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• pp.122-128
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• 2002

This study was conducted to synthesize the diamond like carbon films by plasma enhanced chemical vapor deposition (PECVD). The effects of gas composition on growth and mechanical properties of the films were investigated. A little amount of hydrogen or oxygen were added to base gas mixture of methane and argon. Methane dissociation and diamond like carbon nucleation were enhanced by installing negatively bias grid near substrate. The deposited films were indentified as hard diamond like carbon films by micro-Raman spectroscopy. The surface and fractured cross section of the films which were observed by scanning electron microscopy showed that film growth is very slow as about 0.3$\mu\textrm{m}$/hour, and relatively uniform with hydrogen addition. Vickers hardness of tungsten carbide (WC) cutting tool increased from about 1000 to 1600~1800 by deposition of DLC film, that of commercial TiN coated tool was about 1270. In cutting test of aluminum 6061 alloy, DLC coated cutting tool showed 1/3 or lower crater and flank wear than TiN coated or non-coated WC cutting tools.

• Proceedings of the KIEE Conference
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• 2003.07c
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• pp.1469-1471
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• 2003

The effect of heat treatment on torsion characteristics of high nitrogen steel wire has been studied by using torsion test, micro vickers hardness and scanning electron microscopy. After heat treatment at $600{\sim}700^{\circ}C$, torsion cycle was increased with increasing temperature. Especially, in case of high nitrogen steel wire heat treated at $650^{\circ}C$, torsion cycle was sharply increased. It is estimated that the cold-worked high nitrogen steel wire started to recrystallize around at $640^{\circ}C$ in air atmosphere.

• Journal of Welding and Joining
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• v.18 no.2
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• pp.184-184
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• 2000

In this study, the lap welding between austenitic stainless steel and carbon steel was carried out using arc spot welding process and weldability of welded specimens was estimated. From the tensile-shear strength test, micro Vickers hardness test, and microstructure observation, specimen of 6.5mm(hole of upper plate) showed the best results in terms of tensile-shear strength and nugget shape. And there was an unmixed zone in fusion boundary between the carbon steel base metal and bulk weld metal. This zone had very thin width with the hard microstructure. The shape of weld nugget in arc spot welding of dissimilar metal welds was predicted by searching thermal history of a weld joint through a three-dimensional finite element model. From the numerical analysis, predicted the shape of weld nugget showed good agreement with the experiment(Received August 24, 1999)

• Journal of Surface Science and Engineering
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• v.26 no.4
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• pp.183-191
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• 1993

Diffusion coating(metalliding) of aluminium on steel from molten fluorides(29.2wt.% LiF-11.7wt.% NaF-59.1wt.% KF, FLINAK) was studied. The electrolytic cell consists of a steel cathode and a consumable aluminium anode. Effects of manganese on the aluminium deposition were also investigated. The quality of the deposit was analyzed by SEM, OM, EPMA, EDXA, and also examined by means of Micro-Vickers hardness and corrosion tests. Deposit layer was identified as an aluminium-rich iron alloy caused by diffusion process. The optimum condition for the metalliding was found to be the current density, 50 to $150mA/\textrm{cm}^2$, the bath tem-perature, $57.5^{\circ}C$, and the amount of AlF3, 10wt.%. Addition of manganese fluoride (up to 5wt.%) as a co-de-posit element improved significantly the quality of the deposit layer.

• Journal of Surface Science and Engineering
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• v.25 no.3
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• pp.133-143
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• 1992

Titanium nitride(TiN) films have been prepared by HCD plasma enhanced reactive ion plating. Density and temperature of the plasma generated by the HCD were investigated. It was shown that parameters such as the substrate bias voltage(0 350V) and N2 flow rate(10 180SCCM) influenced the growth, the growth, the microstructure and the color tone of the film mostly. In order to study the interface region, surface analysis by AES combined with sputter depth profiling was performed. Microhardness of the coated TiN films were measured by micro Vickers hardness tester. Also, the effect of coating parameters on composition, coating surface and fracture morphology, grain size and growth rate were examined.

• Corrosion Science and Technology
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• v.17 no.3
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• pp.129-137
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• 2018

The resistance to corrosion of additive manufactured (3D printing) Ti-6Al-4V alloys was investigated using micro-electrochemical tests. In terms of corrosion resistance, the acicular martensitic ${\alpha}^{\prime}$ phase in such additive manufactured Ti-6Al-4V was the focus of attention, and its behavior was distinct from that of conventional subtractive manufactured Ti-6Al-4V. To order to identify ${\alpha}^{\prime}$ phase, XRD tests were performed and micro Vickers hardness was measured for different grains (bright and dark grains) in the additive manufactured Ti-6Al-4V alloy. Micro-electrochemical tests were performed to measure corrosion resistance of bright and dark grains in the additive manufactured Ti-6Al-4V alloy with specially designed electrochemical micro-droplet cell. Critical pitting temperature (CPT) measurement was performed to evaluate the resistance to pitting corrosion of additive manufactured Ti-6Al-4V alloys with different volumes of ${\alpha}^{\prime}$ phase and subtractive manufactured Ti-6Al-4V alloy. The dark grains of the laminated Ti-6Al-4V alloy distributed broader than the bright grains measured with low microhardness. The dark grains of the Ti-6Al-4V alloy, which was rich in martensite ${\alpha}^{\prime}$, had lower general corrosion and pitting resistance than bright grains. As the fraction of martensite ${\alpha}^{\prime}$ phase increased, the resistance to the pitting corrosion decreased.

• Korean Journal of Materials Research
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• v.23 no.9
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• pp.531-536
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• 2013

This paper investigates the effect of prolonged high temperature exposure on concentric laminated $Al_2O_3-ZrO_2$ composites. An ultrafine scale microstructure with a cellular 7 layer concentric lamination with unidirectional alignment was fabricated by a multi-pass extrusion method. Each laminate in the microstructure was $2-3{\mu}m$ thick. An alternate lamina was composed of 75%$Al_2O_3$-(25%m-$ZrO_2$) and t-$ZrO_2$ ceramics. The composite was sintered at $1500^{\circ}C$ and subjected to $1450^{\circ}C$ temperature for 24 hours to 72 hours. We investigated the effect of long time high temperature exposure on the generation of residual stress and grain growth and their effect on the overall stability of the composites. The residual stress development and its subsequent effect on the microstructure with the edge cracking behavior mechanism were investigated. The residual stress in the concentric laminated microstructure causes extensive micro cracks in the t-$ZrO_2$ layer, despite the very thin laminate thickness. The material properties like Vickers hardness and fracture toughness were measured and evaluated along with the microstructure of the composites with prolonged high temperature exposure.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.19 no.3
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• pp.29-35
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• 2020

This paper studies the main parameters of tube-to-bar dissimilar material and shape friction welding for piping materials. The weldability of joint parts was investigated with respect to tensile tests, micro-Vickers hardness, the bond of area, and optical microstructure. The specimens are tested as-welded. Optimal welding conditions are n = 2000 rpm, HP = 50 MPa, UP = 100 MPa, HT = 5 sec, and UT = 10 sec when the metal loss (Mo) is 11 mm. Moreover, the same two materials for friction welding are strongly mixed with a well-combined structure of micro-particles without any molten material, particle growth, or defects. Therefore, the expected result of dissimilar material friction welding includes a reduction of cost and material in the welding process.

• Journal of the Korean Institute of Gas
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• v.14 no.6
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• pp.38-43
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• 2010

According to the lack of resources and the stringency of environmental regulations, a study of the high strength thin plate sheet steels for automobile have been become an important issue for automobile industry. However, the problem of hydrogen embrittlement of high strength sheet steels was concerned with the degradation of mechanical properties. Therefore, we studied the hydrogen behavior of surface layers of 590MPa DP sheet steels on development using by relationship the microstructure of subsurface and the distribution of micro hardnesses. Hydrogen was charged into the specimens using by the cathodic electrolytic method. The behavors of under surface layers were investigated by the observation of microstructures and the micro vickers hardness test with the amount of hydrogen charging with hydrogen charging conditions.