• Title/Summary/Keyword: micro viscosity

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Preparation and Characterization of Carbon/Phenol Composite by RTM Process (RTM 공정에 의한 탄소/페놀 복합재료의 제조 및 특성 분석)

  • Jin, Da Young;Lee, Hyun Jae;Lim, Sung Chan;Kim, Yun Chul;Yun, Nam Gyun;Lee, Seung Goo
    • Textile Coloration and Finishing
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    • v.28 no.4
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    • pp.239-245
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    • 2016
  • In this study, carbon/phenol composites were prepared from carbon fiber preform and phenol resin by RTM(resin transfer molding) process. And changes in the properties of the composite according to the pre-treatment of phenol resin was mainly studied. RTM process conditions were deduced from viscosity and thermal analysis of phenol resin which were rheometer and thermogravimetric analyzer(TGA). RTM process was performed under various injection and molding temperature. Characterization of the prepared C/P composites were evaluated by various analysis. Morphology of composites was analyzed by Micro-CT(MCT), Mechanical properties of composites were measured through the flexural properties. As results, volatile impurities of phenol resin were effectively removed at resin pre-treatment temperature of $100^{\circ}C$ and composite was sufficiently cured at molding temperature of $180^{\circ}C$.

A Study on Tunnel Entry Design Considering the Booming Noise Resulting from Micro-Pressure Wave (미기압파에 의한 터널 출구 소음 저감을 위한 고속철도 터널 형상 개선에 관한 연구)

  • 목재균;최강윤;유재석
    • Journal of KSNVE
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    • v.7 no.6
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    • pp.959-966
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    • 1997
  • In general, the booming noise intensity at tunnel exit is strongly related to the gradient of the compression wave front created by high speed train entering the tunnel. This paper presents some results in relation with the compression wave front produced when the high speed train enters a tunnel. Four kinds of tunnel entrance shape with real dimensions were studied to investigate the formation of compression wave front inside tunnel by train entering tunnel. Computations were carried out using three-dimensional compressible Euler equation with vanishing viscosity and conductivity of fluid. According to the results, the flow disturbances occured at tunnel entrance were eliminated by tunnel hood with same cross sectional area. The compression wave front is formed completely at 30-40m from tunnel entrance. The maximum pressure gradient of compression wave front is reduced by 29.8% for the inclined tunnel hood and reduced by 21.5% for the tunnel hood with holes at the top face with tunnel without hood. The length of the inclined hood is 15m and the length of the hood with holes is 20m.

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Effects of Viscosity Control by Induction Heating on Micro Cell in Forming Process of Foamed Aluminum (알루미늄 발포재의 성형공정에서 유도가열 법에 의한 점도 제어가 미세 기공에 미치는 영향)

  • Jeon, Yong-Pil;Kang, Chung-Gil
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.6
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    • pp.136-144
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    • 2002
  • Melting method has long been considered difficult to realize because of problems such as the low foamability of molten metal, the varying size of cellular structures and solidification shrinkage. The parameters to solve the problem in electric furnace were stirring temperature, stirring velocity, heating velocity and foaming temperature It is important to consider the effects of induction heating, because it brings about the inner flow by the temperature gradient. Aspect ratio also depends on the induction heating. Mechanical properties are dependent on cell sizes and aspect rations. Therefore, this paper presents the effects of these parameters on the cell sizes. For the sake of this, combined stirring process was used to fabricate aluminum foam materials by the above mentioned parameters. Image analysis was performed to calculate the cell sizes, distributions, and aspect ratioes at the cross section of feared aluminum in the direction of height.

Hemodynamical analysis by viscosity characteristics of artificial blood for μ-PIV experiment of Radio-cephalic arteriovenous fistula(RC-AVF) (μ-PIV기법을 이용한 동정맥루 모사혈관에서의 모사 혈액의 점도특성에 따른 혈류역학적 분석)

  • Song, Ryungeun;Lee, Jinkee
    • Journal of the Korean Society of Visualization
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    • v.14 no.1
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    • pp.33-39
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    • 2016
  • Radio-cephalic arteriovenous fistula(RC-AVF) is the most recommended operation of achieving access for hemodialysis. However, it has high rates of early failure depending on the many haemodynamic conditions. To increase RC-AVF patency rate, many researches were performed by in-vitro experiment via artificial vessel and blood analogue fluid, and there were conflicting opinions about whether the non-Newtonian properties of blood have an influence on the flow in large arteries. To investigate the influence of viscoelasticity of blood within the RC-AVF, we fabricated three dimensional artificial RC-AVF and two kinds of blood analogue fluid. The velocity field of two fluids within the vessel were measured by micro-particle velocimetry(m-PIV) and compared with each other. The velocity profiles of both fluids for systolic phase were matched well while those for diastolic phase did not correspond. Therefore, it is desired to use non-newtonian fluid for in-vitro experiment of RC-AVF.

Optimization of Process Condition for Fe Nano Powder Injection Molding

  • Oh, Joo Won;Lee, Won Sik;Park, Seong Jin
    • Journal of Powder Materials
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    • v.24 no.3
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    • pp.223-228
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    • 2017
  • Nanopowders provide better details for micro features and surface finish in powder injection molding processes. However, the small size of such powders induces processing challenges, such as low solid loading, high feedstock viscosity, difficulty in debinding, and distinctive sintering behavior. Therefore, the optimization of process conditions for nanopowder injection molding is essential, and it should be carefully performed. In this study, the powder injection molding process for Fe nanopowder has been optimized. The feedstock has been formulated using commercially available Fe nanopowder and a wax-based binder system. The optimal solid loading has been determined from the critical solid loading, measured by a torque rheometer. The homogeneously mixed feedstock is injected as a cylindrical green body, and solvent and thermal debinding conditions are determined by observing the weight change of the sample. The influence of the sintering temperature and holding time on the density has also been investigated. Thereafter, the Vickers hardness and grain size of the sintered samples have been measured to optimize the sintering conditions.

Growth and electrical properties of Pb(Zr, Ti)$O_3$ thin films by sol-gel method (솔-젤 법을 이용한 Pb(Zr, Ti)$O_3$ 박막의 성장 및 전기적 특성에 관한 연구)

  • 김봉주;전성진;이재찬;유지범
    • Journal of the Korean Vacuum Society
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    • v.8 no.4A
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    • pp.425-431
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    • 1999
  • $Pb(Zr_{0.52}, Ti_{0.48})O_3$ (PZT) thick films as an actuating material with conducting oxides, $(La_{0.5}Sr_{0.5}) CoO_3$ (LSCO), have been fabricated by sol-gel method for Optical Micro-Electro-Mechanical System (MEMS) devices, in which PZT/LSCO/SiO2 structures were used. In order to improve the adhesion to LSCO solution in order to enhance the wetting behavior of a water-based LSCO precursor solution and further to improve the adhesion between LSCO and $SiO_2$ layers. PZT films were made using 1-3 propanediol based precursor solution which has a high viscosity and a boiling point appropriate for thick film fabrication. In the precursor solution, Ti-propoxied and Zr-propoxied are partially substituted with acetylacetone to achieve the solution stability while maintaining reactivity. Crack free PZT films (0.8~1$\mu\textrm{m}$) have been successfully fabricated at crystallization temperatures above $700^{\circ}C$. Dielectric constants and dielectric losses of the PZT films were 900~1200and 2~5%, respectively. Piezoelectric constant $d_{33}$ of the PZT films constrained by a substrate were 200pm/V at 100kV/cm.

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Toward the computational rheometry of filled polymeric fluids

  • Hwang, Wook-Ryol;Hulsen Martien A.
    • Korea-Australia Rheology Journal
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    • v.18 no.4
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    • pp.171-181
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    • 2006
  • We present a short review for authors' previous work on direct numerical simulations for inertialess hard particle suspensions formulated either with a Newtonian fluid or with viscoelastic polymeric fluids to understand the microstructural evolution and the bulk material behavior. We employ two well-defined bi-periodic domain concepts such that a single cell problem with a small number of particles may represent a large number of repeated structures: one is the sliding bi-periodic frame for simple shear flow and the other is the extensional bi-periodic frame for planar elongational flow. For implicit treatment of hydrodynamic interaction between particle and fluid, we use the finite-element/fictitious-domain method similar to the distributed Lagrangian multiplier (DLM) method together with the rigid ring description. The bi-periodic boundary conditions can be effectively incorportated as constraint equations and implemented by Lagrangian multipliers. The bulk stress can be evaluated by simple boundary integrals of stresslets on the particle boundary in such formulations. Some 2-D example results are presented to show effects of the solid fraction and the particle configuration on the shear and elongational viscosity along with the micro-structural evolution for both particles and fluid. Effects of the fluid elasticity has been also presented.

A study on tunnel entry design considering the booming noise resulting from micro-pressure wave (미기압파에 의한 터널출구소음저감을 위한 고속철도 터널형상개선에 관한 연구)

  • 목재균;최강윤
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 1997.04a
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    • pp.627-635
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    • 1997
  • In general, the booming noise intensity at tunnel exit is strongly related to the gradient of the compression wave front created by high speed train entering the tunnel. This paper presents some results in relation with the compression wave front produced when the high speed train enters a tunnel. Four kinds of tunnel entrance shape with real dimensions were studied to investigate the formation of compression wave front inside tunnel by train entering tunnel. Computations were carried out using three-dimensional compressible Euler equation with vanishing viscosity and conductivity of fluid. According to the reslts, the flow disturbance occured at tunnel entrance were eliminated by tunnel hood with same cross sectional area. The compression wave front is formed completely at 30-40m from tunnel entrance. The maximum pressure gradient of compression wave front is reduced by 29.8% for the inclined tunnel hood and reduced by 21.5% for the tunnel hood with holes at the top face with tunnel without hood. The length of the inclined hood is 15m and the length of the hood with holes is 20m.

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Limit-current type zirconia oxygen sensor with porous diffusion layer (다공성 확산층을 이용한 한계전류형 지르코니아 산소센서)

  • Oh, Young-Jei;Lee, Chil-Hyoung
    • Journal of Sensor Science and Technology
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    • v.17 no.5
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    • pp.329-337
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    • 2008
  • Simple, small and portable oxygen sensors were fabricated by tape casting technique. Yttria stabilized zirconia containing cordierite ceramics (YSZC) were used as a porous diffused layer of oxygen in pumping cell. Yttria stabilized zirconia (YSZ) solid electrolyte, YSZC porous diffusion layer and heater-patterned ceramic sheets were prepared by co- firing method. Limit current characteristics and the linear relationship of current to oxygen concentration were observed. Viscosity variation of the slurries both YSZ and YSZC showed a similar behavior, but micro pores in the fired sheet were increased with increasing of the cordierite amount. Molecular diffusion was dominated due to the formation of large pores in porous diffusion layer. The plateau range of limit current in porous-type oxygen sensor was narrow than the one of aperture-type oxygen sensor. However limit current curve was appeared in porous-type oxygen sensor even at the lower applied voltage. The plateau range of limit-current was widen as increasing the thickness of porous diffusion layer of the YSZ containing cordierite. Measuring temperature of $600{\sim}650^{\circ}C$ was recommended for limit-current oxygen sensor. Porous diffusion layer-type oxygen sensor showed faster response than the aperture-type one and was stable up to 30 days running without any crack at interface between the layers.

Preparation and evaluation of GFP-containing microspheres for oral vaccine delivery system (경구용 백신수송체용 GFP 함유 마이크로스피어의 제조 및 평가)

  • Jiang, Ge;Park, Jong-Pil;Kwak, Son-Hyok;Hwang, Sung-Joo;Maeng, Pil-Jae
    • Journal of Pharmaceutical Investigation
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    • v.30 no.4
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    • pp.253-258
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    • 2000
  • In order to design the oral vaccine delivery system, we prepared the alginate micro spheres containing GFP (green fluorescent protein) as a model drug by spray method. To optimize the preparation conditions of microspheres, we investigated the effects of various parameters including nozzle pressure, nozzle opening angle, and concentrations of sodium alginate and calcium chloride. The prepared microspheres were evaluated by measuring their sizes, loading efficiency, and morphology. The particle size of microspheres was affected by the concentration of sodium alginate and calcium chloride, nozzle pressure, and nozzle opening angle. As the concentration of sodium alginate increased, GFP loading efficiency and particles size of microsphere also increased. However, it was observed to be difficult to spray the sodium alginate solution with concentration greater than 1.5% (w/v), due to high viscosity. The pressure over $3\;kgf/cm^2$ didn't affect the size of particles. As a result, the spraying method enabled us to prepare microspheres for oral vaccine delivery system. In this study, microspheres prepared with 1% (w/v) sodium alginate had greater loading efficiency and better spherical shape.

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