• Title/Summary/Keyword: metal analysis

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A Study on the Characteristics of Linear Ultrasonic Motor Using Metal-Ceramics Composite Structure (금속-세라믹 복합구조 선형 초음파 모터의 특성 연구)

  • Lee, Jae-Hyung;Choi, Myeong-Il;Jeong, Dong-Seok;Park, Tae-Gone
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.08a
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    • pp.80-83
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    • 2002
  • In this study, a single phase driven piezoelectric motor design is presented for linear motion-metal/ ceramics composite structure. Using ANSYS finite element analysis software, mode shape of free motor was obtained to clarify the working principle of this motor. And characteristics of the motor was measured. The motor is composed of a piezoelectric ceramic, a metal ring which has 4 arms, and a guider. The motor with 25.0[mm] diameter was studied by finite element analysis and experimentation too. As a result, the motor was expressed the best speed in resonance frequency. And according as voltage of the motor increase, the speed increased by ratio.

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Finite Element Analysis of the Unconstrained Cylindrical Bending Process Considering Continuous Contact Treatment (연속 접촉 처리를 고려한 실린더 벤딩 성형 공정의 유한요소해석)

  • Kim T. J.;Yang D. Y.
    • Transactions of Materials Processing
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    • v.14 no.6 s.78
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    • pp.547-552
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    • 2005
  • In general, the sheet metal and die are described by finite elements for the simulation of the metal forming processes. Because the characteristics as continuum of the sheet metal are represented with triangles and rectangles, the errors occur inevitably in finite element analysis. Many contact schemes to describe the deformation modes exactly have been introduced in order to decrease these errors. In this study, a scheme for continuous contact treatment is proposed in order to consider the realistic behavior of contact phenomena during the forming process. The discrete mesh causes stepwise propagation of contact nodes of the sheet even though the contact region of the real forming process is altered very smoothly. It gives rise to convergence problem in case that the process, for example bending process, is sensitive to the contact between the sheet and the tools. The analysis of the unconstrained cylindrical bending process without blank holder is also presented in order to investigate the effect of the proposed algorithm.

Synthesis and Characterization of Polymer and Polymer Complex with Some Transition Metal Ions (몇 개의 전이금속 이온과 고분자와 고분자 Complex의 합성과 특성연구)

  • Badr, S.K.;Mohamed, T.Y.
    • Journal of the Korean Chemical Society
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    • v.54 no.1
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    • pp.43-48
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    • 2010
  • Polyamide derived from azo compound of o-amino phenol coupled with acetyl acetone, maleic anhydride acid and p-phenylene diamine were prepared. The prepared polyamide (PA) was refluxed with metal salts of transition metal ions include, $Co^{+2},\;Cr^{+2},\;Ni^{+2},\;Cu^{+2},\;Zn^{+2},\;Cd^{+2}$ and $Fe^{+3}$ in dimethyl formamide (DMF) in different molar ratios. These complexes were characterized and identified by elemental and thermal analysis, IR, 1H NMR spectra. The data showed that PA ligand coordinates with metal ions in abidentate manner through donating N=N and O-H groups. The metal ions are surrounded by coordinated water molecules and anions to establish the geometrical structure of the complexes. The thermal analysis degradation at different temperatures explained the weight loss of hydrated water and the decompositions of complexes until a constant weight loss of metal oxides is obtained.

Chemical Properties of Mineral Surfaces and Metal Ion Sorption: A Review (광물표면의 화학적 특성과 금속이온 수착의 고찰: A Review)

  • Yoon, Soh-Joung
    • Economic and Environmental Geology
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    • v.45 no.2
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    • pp.205-215
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    • 2012
  • Metal ions, toxic or potentially toxic to biota and human beings, can be immobilized by sorption onto the mineral surfaces in soils and sediments. This article briefly explains theories regarding the chemical properties of mineral surfaces to sorb metal ions and processes of extended X-ray absorption fine structure (EXAFS) analysis for sorption study, and reviews atomic-scale findings on metal sorption on mineral surfaces. The theoretical understanding on the chemistry of mineral surfaces and metal sorption is fundamental to the proper analysis of the atomic-scale spectroscopy to determine the sorption phases. Atomic-scale findings on metal sorption phases discussed here include co-precipitation, ternary complexation, aging effects, and desorption possibilities, as well as outer-sphere complexation, inner-sphere complexation, and surface precipitation.

A Study on the Characteristic Evaluation of Sewage and Industrial Wastewater Treatment Sludges by Physico-chemical Analysis (물리화학적 분석을 통한 하 ${\cdot}$ 폐수처리 슬러지류의 특성평가)

  • Kwon, Gi-Hong
    • Journal of Environmental Health Sciences
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    • v.31 no.1
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    • pp.86-93
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    • 2005
  • Because generally large amount of sludges are generated from the process of sewage and wastewater treatment, the management and controlment of those sludge has become a important issue in many researches. In this dissertation, we conducted the research to see the physico-chemical characteristics of sludges generated from various sources. Moisture of sludges were 81.5% in textile industries, 81.4% in frame metal industries, 80.7% in 1st metal industries. Volatile solid were 22.1% in hide · rubber industries, 21.9% in coke · petroleum industries. Fixed solid were 18.5% and 17.7% in the 1st metal industries and frame metal industries. High heating value by wet base were 1,850 kcal/kg in coke · petroleum industries, 1,220 kcal/kg in hide · rubber industries, but sludges from the 1st metal industries and frame metal industries were impossible to incinerate because most of those sludges were inorganic. The leaching test showed that hazardous materials was detected in nearly every kinds of sludges. Some of sludges from hide · rubber industries and frame metal industries exceeded the leaching criteria and so they were classified as specific wastes. And other sludges generated in sewage treatment plants or other industries was below the leaching criteria.

The Effects of binary metal oxide catalysts for the synthesis of glycerol carbonate (이원계 금속산화물 촉매가 글리세롤카보네이트 합성에 미치는 영향)

  • Baek, Jae-Ho;Moon, Myung-Jun;Lee, Man-Sig
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.1
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    • pp.456-461
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    • 2012
  • The glycerol carbonate was synthesized by glycerol and urea using metal oxide catalysts. The physical properties of the prepared metal oxide catalysts were investigated by X-ray diffraction (XRD), specific surface area analysis (BET), field emission scanning electron microscopy (FE-SEM) and temperature programmed desorption (TPD). In addition, we confirmed the conversion of the glycerol and the yield of the glycerol carbonate according to characteristics of metal oxide catalysts. From XRD and FE-SEM analysis, the crystallite size and crystallinity of metal oxide catalysts decrease with addition of Al. In addition, the Zn-Al mixed metal oxide had higher catalytic activity than the pure ZnO due to decreased side reaction in the synthesis of glycerol carbonate.

Stress distribution of near the interface on high temperature fatigue in ceramic/metal bonded joints (세라믹/금속접합재의 고온피로에 따른 접합계면의 응력분포)

  • 박영철;허선철;윤두표;김광영
    • Journal of Ocean Engineering and Technology
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    • v.10 no.2
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    • pp.106-119
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    • 1996
  • The ceramic has various high mechanical properties such as heat, abrasion, corrosion resistance and high temperature strength compared with metal. It also has low speciffic weight, low thermal expansibillity, low thermal conductivity. However, it could not be used as structural material since it is brittle and difficult for the machining. Therefore, there have been many researches to attempt to join ceramic with metal which is full of ductillity in order to compensate the weakness of ceramic.The problem is that residual stress develops around the joint area while the ceramic/metal joint material is cooled from high joining temperature to room temperature due to remarkable difference of thermal expansion coefficients between ceramic and metal. Especially, the residual stress at both edges of the specimen reduces the strngth of joint to a large amount by forming a singular stress field. In this study, two dimensional finite element method is attempted for the thermal elastic analysis. The joint residual stress of ceramic/metal developed in the cooling process is investigated and the change of joint residual stress resulted from the repetitive heat cycle is also examined. In addition, it is attempted to clarify the joint stress distribution of the case of tensile load and of the case of superposition of residual stress and actual loading stress.

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Axial buckling response of fiber metal laminate circular cylindrical shells

  • Bidgoli, Ali M. Moniri;Heidari-Rarani, Mohammad
    • Structural Engineering and Mechanics
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    • v.57 no.1
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    • pp.45-63
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    • 2016
  • Fiber metal laminates (FMLs) represent a high-performance family of hybrid materials which consist of thin metal sheets bonded together with alternating unidirectional fiber layers. In this study, the buckling behavior of a FML circular cylindrical shell under axial compression is investigated via both analytical and finite element approaches. The governing equations are derived based on the first-order shear deformation theory and solved by the Navier solution method. Also, the buckling load of a FML cylindrical shell is calculated using linear eigenvalue analysis in commercial finite element software, ABAQUS. Due to lack of experimental and analytical data for buckling behavior of FML cylindrical shells in the literature, the proposed model is simplified to the full-composite and full-metal cylindrical shells and buckling loads are compared with the available results. Afterwards, the effects of FML parameters such as metal volume fraction (MVF), composite fiber orientation, stacking sequence of layers and geometric parameters are studied on the buckling loads. Results show that the FML layup has the significant effect on the buckling loads of FML cylindrical shells in comparison to the full-composite and full-metal shells. Results of this paper hopefully provide a useful guideline for engineers to design an efficient and economical structure.

Involvement of Lipopolysaccharide of Bradyrhizobium japonicum in Metal Binding

  • Oh, Eun-Taex;Yun, Hyun-Shik;Heo, Tae-Ryeon;Koh, Sung-Cheol;Oh, Kye-Heon;So, Jae-Seong
    • Journal of Microbiology and Biotechnology
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    • v.12 no.2
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    • pp.296-300
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    • 2002
  • Bacterial cell surface components are the major factors responsible for pathogenesis and bioremediation. In particular, the surface of a Gram-negative bacterium cell has a variety of components compared to that of a Gram-positive cell. In our previous study, we isolated an isogenic mutant of Bradyrhizobium japonicum, which exhibited altered cell surface characteristics, including an increased hydrophobicity. Polyacrylamide gel electrophoretic analysis of the lipopolysaccharide (LPS) in the mutant demonstrated that the O-polysaccharide part was completely absent. Meanwhile, a gel permeation chromatographic analysis of the exopolysaccharide (EPS) in the mutant demonstrated that it was unaltered. Since LPSs are known to have several anion groups that interact with various cation groups and metal ions, the mutant provided an opportunity to examine the direct role of LPS in metal binding by B. japonicum. Using atomic absorption spectrophotometry, it was clearly demonstrated that LPS was involved in metal binding. The binding capacity of the LPS mutant to various metal ions $(Cd^{2+},\;Cu^{2+},\;Pb^{2+},\;and\;Zn^{2+})$ was 50-70% lower than that of the wild-type strain. Also, through an EPS analysis and desorption experiment, it was found that EPS and centrifugal force had no effect on the metal binding. Accordingly, it would appear that LPS molecules on B. japonicum effect the properties, which precipitate more distinctly metal-rich mineral phase.

Comparison of Blood Lead Concentration Using Graphite Furnace Atomic Absorption Spectrometry (GF-AAs) and Inductively Coupled Plasma-mass Spectrometry (ICP-MS) (흑연로 원자 흡광 광도법과 유도 결합 플라즈마 질량 분석법을 이용한 혈중 납 농도 비교)

  • Kang, Min-Kyung;Kwon, Jung-Yeon;Kim, Byoung-Gwon;Lim, Hyoun-Ju;Seo, Jeong-Wook;Kim, Yu-Mi;Hong, Young-Seoub
    • Journal of Environmental Health Sciences
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    • v.45 no.3
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    • pp.258-266
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    • 2019
  • Objectives: In this study, blood lead was analyzed using graphite furnace atomic absorption spectrometry (GF-AAs) and inductively coupled plasma mass spectrometry (ICP-MS). We tried to examine the difference and consistency of the analytical values and the applicability of the analytical method. Methods: We selected 57 people who agreed to participate in this study. After confirming the linearity of the calibration standard curves in GF-AAs and ICP-MS, the concentrations of lead in quality control material and samples were measured, and the degree of agreement was compared. Results: The detection limit of the ICP-MS was lower than that of GF-AAs. The coefficient of variation of reference materials was shown to be stable in the ICP-MS and GF-AAs. When the correspondence between the two equipments was verified by bias of the analysis values, a concordance was shown, and approximately 98% of the ideal reference lines were present within ${\pm}40%$ of the deflection. Conclusion: GF-AAs showed high sensitivity to single heavy metal analysis, but it took much time and showed higher detection limit than ICP-MS. Therefore, it would be considered necessary to switch to ICP-MS analysis method, considering that the level of lead exposure is gradually decreasing.