• Journal of Welding and Joining
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• 제26권3호
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• pp.37-44
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• 2008

Charpy V-Notch test is commonly used to evaluate fracture toughness. However, since the region to be evaluated is limited to bulk material due to the specimen size required, individual evaluation of micro-structures on weldment is very difficult. In this study, ASP(Advanced Small Punch) test was carried out to evaluate material degradation and fracture toughness on the B.M, W.M and each micro-structures of HAZ for X20CrMoV121 and 2.25Cr1Mo steels with artificial aging time. In addition, to evaluate fracture toughness and material degradation of B.M and W.M of X20CrMoV121 steels with aging times, CVN (Charpy V-notch) test was performed. And then the correlation between ASP and CVN test on X20CrMoV121 steels was obtained. Furthermore, through this correlation, material degradation property of each micro-region of the HAZ in weldment, which was impossible to be evaluated by the CVN test, can be estimated and determined.

• 한국세라믹학회지
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• 제34권3호
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• pp.257-264
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• 1997

MPB조성영역에 MnO2를 첨가한 압전체를 제조하여 분극처리후에 반복압축응력을 부여함에 따른 압전열화 현상을 조사하고 분극처리 전후의 굽힘강도의 변화 및 파괴특성을 연구하였다. MnO2를 0.25wt.% 첨가한 시편에서 가장 적은 열화현상이 일어났다. 굽힘강도는 분극처리 후 하중방향에 평행한 방향으로 분극처리한 시편이 분극처리 전보다 높은 강도를 나타내었고, 수직한 방향으로 분극처리한 시편은 낮은 값을 나타내었다. 이는 분극처리시 발생하는 전계방향으로 압축잔류응력, 직각방향으로 인장잔류응력 때문인 것으로 사료된다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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• pp.456-459
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• 2003

Polychloroprene(CR) is well known as elastomer commonly utilized in the electrical. It is mainly used for cable jacket and insulator. The irradiation degradation property of polymer materials is very important to prevent unexpected accidents in the Nuclear Power Plant(NPP). The irradiation degradation is caused by the oxidation of polymer materials, and this oxidation is occurred by oxygen radical produced from air. In this study, we evaluate the oxidation properties of CR. CR is irradiated for 200, 400, 600, 1000 kGy radiation dose. The oxidation properties of irradiated CR are investigated by differential scanning calorimetry, dynamic mechanical properties and FT-IR/ATR. Glass transition temperature(Tg), decomposition onset temperature(DOT), loss modulus and mechanical tan $\delta$ values are compared together. The irradiation limit of CR in the NPP, is known for 500 kGy, and this is exactly matched with investigated results.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2010년도 추계학술대회 초록집
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• pp.76.1-76.1
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• 2010

Recently, many efforts to solve the durability problem of PEM fuel cell are carried on constantly. However, despite this attention, durability researches of gas diffusion layer (GDL) are not much reported yet. Generally, GDL of PEM fuel cell experiences three external attacks, which are dissolution of water, erosion of gas flow, corrosion of electric potential. In this study, among these degradation factors, carbon corrosion of electric potential was focused and investigated with accelerated carbon corrosion test. Through the test, it is confirmed that carbon corrosion occurred at GDL, and corroded GDL decreased a performance of operating fuel cell. The property changes of GDL were measured with various methods such as air permeability meter, pore distribution analyzer, thermo gravimetric analyzer, and tensile stress test to discover the effects of carbon corrosion. Carbon corrosion caused not only loss of weight and thickness, but also degradation of mechanical strength of GDL. In addition, to analysis the reason of GDL property changes, a surface and a cross section of GDL were observed with scanning electron microscope. After 100 hours test, the GDL showed serious damage in center of layer.

• 한국염색가공학회지
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• 제29권3호
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• pp.155-161
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• 2017

In CPB(Cold-Pad-Batch) dyeing, the rubber of the padder roll is influenced by the heat, chemical and mechanical influences and thus aging of the padder roll rubber occurs. This study presents an accelerated thermal aging test of the CPB padder roll rubber with strong alkali conditions. Using Arrhenius formula of the various property values for the various aging temperatures($80^{\circ}C$, $90^{\circ}C$, $100^{\circ}C$) of the padder roll, the accelerated life predictions could be calculated. The threshold value of the property was set at different values. The hardness was set at the point where 5% degradation occurs based on the actual use conditions, and the tensile strength was set at the point where 50% degradation occurs based on the general life prediction standards. From the results of the different physical properties at differing temperatures, the Arrhenius plot could be obtained. Through the usage of the Arrhenius Equation, significant duration expectation could be predicted, and the chemical aging behavior of the CPB padder roll could be found at the arbitrary and actual temperatures.

• 청정기술
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• 제19권4호
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• pp.401-409
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• 2013

폐플라스틱에 의한 환경오염 증가로 생분해성 고분자에 대한 관심이 커지고 있다. 본 연구에서는 생분해성 고분자인 폴리 L-락타이드(polylactic acid, PLA)와 폴리 L-락타이드(polylactic acid, PLA)/폴리 부틸렌 숙신산(polybutylene succinate, PBS)(90/10)수지를 기지재료로 하고 유기 크로사이트(cloisite ) 20을 나노 클레이(clay) 20으로 사용하여 이축압출기에서 Clay-20 함량별 로 압출시켜 나노복합체를 제조하였다. 사출성형기로 사출성형시편을 제조하여 나노복합체의 열적, 기계적, 형태학적 및 라만 분광학 특성을 시차열량분석기(differential scanning calorimeter, DSC), 인장시험기, 주사전자현미경(scanning electron microcopy, SEM), 라만-현미경 분광광도계로 조사하였고, 또한 가수분해특성을 조사하였다. 시차열량분석기와 주사전자현미경 시험 결과에서 PLA/Clay-20과 PLA/PBS/Clay-20 나노복합체의 결정화도가 Clay-20 함량이 증가함에 따라 증가하였고, Clay-20과 PLA 및 PLA/PBS 수지가 서로 상용성이 있는 것으로 확인되었다. 또한 Clay-20 함량이 증가함에 따라 두 나노복합체의 인장강도는 감소하지만 신도, 충격강도, 인장탄성률 및 굴곡탄성률이 증가하였다. 특히 Clay-20이 5 wt% 첨가된 PLA/Clay-20과 PLA/PBS/Clay-20 나노복합체의 충격강도는 순수 PLA와 PLA/PBS (90/10) 보다 2배 이상으로 증가하였다. Clay-20 3 wt% 첨가된 PLA/Clay-20 나노복합체의 가수분해속도는 순수 PLA 가수분해속도보다 두 배 정도 빨랐다. 이는 유기화 처리된 Clay-20 나노입자 표면의 친수성으로 계면에서 가수분해가 쉽게 일어나기 때문인 것으로 판단된다. 본 연구에서 적당량의 Clay-20 첨가로 PLA의 기계적특성 개선과 생분해 특성 조절 가능성을 확인하였다.

• 한국초전도ㆍ저온공학회논문지
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• 제4권1호
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• pp.45-59
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• 2002

Evaluation of the mechanical properties of Bi-2223/Ag HTS tapes was carried out by the tension and bending tests. Most of the Bi-2223/Ag tapes retained critical current up to 10 kgf/mm$_2$ axial tension stress, and 0.2% tension strain at room temperature. Applied tension strain exceeding 0.3% in superconducting tapes at 77 K leaded to rapid degradation of the critical current. It was observed that the more filaments, the better axial tension property at 77 K, self-field The influence of bending strain on critical current degradation was revealed to be less sensitive for Bi-2223/Ag HTS tapes with a more number of filaments and higher silver ratio.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2016년도 추계 학술논문 발표대회
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• pp.146-147
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• 2016

Concrete has been recognized as a material which is resistant to high temperatures, but chemicophysical property of concrete is changed by the high temperature. So, mechanical properties of concrete may be reduced. So, concrete at high temperature is evaluated mechanical properties for safety inspection. However, research of ultrasonic method is not much. Therefore, the purpose of this study is to NDT(non-destructive test) of 30, 70, 110MPa concrete exposed high temperature using ultrasonic pulse velocity.

• 한국전기전자재료학회논문지
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• 제17권11호
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• pp.1205-1211
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• 2004

This study has investigated radiation degradation of chloroprene rubber in the presence of some fire retardant. Ammonium polyphosphate, aluminium trihydroxide, magnesium hydroxide, calcium carbonate and antimony trioxide were selected as flame retardant. Samples were irradiated using a Co$^{60}$ ${\gamma}$ -ray and ray up to 2000 kGy at a dose rate of 5 kGy/hr in the presence of air atmosphere at room temperature. After irradiation, samples were assessed fire retardancy with electrical properties and mechanical properties. Some considerations concerning the effects of the fire retardants added to chloroprene rubber on the radiation and thermal stability of chloroprene rubber are presented. From fire retardancy with electrical and mechanical property measurements, it was found that addition of magnesium hydroxide resulted in maximum fire retardant effect.

• Corrosion Science and Technology
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• 제7권3호
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• pp.145-151
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• 2008

Material degradation such as high temperature oxidation of metallic material is a severe problem in energy generation systems or manufacturing industries. The metallic materials are oxidized to form oxide films in high temperature environments. The oxide films act as diffusion barriers of oxygen and metal ions and thereafter decrease oxidation rates of metals. The metal oxidation is, however, accelerated by mechanical fracture and spalling of the oxide films caused by thermal stresses by repetition of temperature change, vibration and by the impact of solid particles. It is therefore very important to investigate mechanical properties and adhesion of oxide films in high temperature environments, as well as the properties in a room temperature environment. The oxidation tests were conducted for Ni and Ni-Co alloy under high temperature corrosive environments. The hardness distributions against the indentation depth from the top surface were examined at room temperature. Dynamic indentation tests were performed on Ni oxide films formed on Ni surfaces at room and high temperature to observe fractures or cracks generated around impact craters. As a result, it was found that the mechanical property as hardness of the oxide films were different between Ni and Ni-Co alloy, and between room and high temperatures, and that the adhesion of Ni oxide films was relatively stronger than that of Co oxide films.