• 제목/요약/키워드: mechanical and thermal properties

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폴리유산/폴리부틸렌숙시네이트 블랜드의 가공 및 기계적, 열적, 형태학적 특성 (Processing and Mechanical, Thermal and Morphological Properties of Poly(lactic acid)/Poly(butylene succinate) Blends)

  • 김대근;조동환
    • 접착 및 계면
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    • 제15권1호
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    • pp.14-21
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    • 2014
  • 본 연구에서는 이축압출기와 사출기를 사용하여 폴리유산(PLA)와 폴리부틸렌숙시네이트(PBS) 수지의 함량비를 달리하여 PLA/PBS 블랜드를 제조하고, 그들의 기계적, 열적 특성 및 모폴로지를 조사하였다. PLA/PBS 블랜드의 굴곡강도, 굴곡탄성률, 인장강도 및 인장탄성률과 같은 기계적 특성, 그리고 용융거동, 동역학적 열특성 및 열안정성과 같은 열적 특성이 PLA와 PBS 함량비에 크게 의존하였다. 그러나 PLA/PBS 블랜드의 열변형온도는 PLA 또는 PBS 함량 변화에 크게 영향을 받지 않았다. 또한 PLA/PBS 블랜드의 파단면은 PBS 함량이 증가함에 따라 brittle 양상으로부터 ductile 양상으로 변화되었다.

고온 및 냉각조건에 따른 콘크리트의 역학적특성에 관한 실험적 연구 (An Experimental Study on the Mechanical Properties of Concrete with High Temperatures and Cooling Conditions)

  • 김규용;강연우;이태규;최경철;윤민호
    • 한국건축시공학회지
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    • 제12권3호
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    • pp.323-331
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    • 2012
  • 1970년대부터 고온을 받은 콘크리트의 압축강도, 탄성계수, 열응력 등 콘크리트에 영향을 미칠 수 있는 내적, 외적 인자들의 역학적 특성은 조사되어 왔다. 특히, 골재의 열적 특성이나 냉각 방법은 잔존 역학적 특성을 평가하는데 가장 중요하다. 본 연구에서는, 골재 종류와 냉각 방식에 따른 콘크리트의 역학적 특성에 대해 평가했다. 본 연구에서는 열적특성이 다른 일반 골재와 경량골재를 사용했다. 또한, ${\O}100{\times}200mm$ 원주형 공시체를 사용하여 목표 온도, 서냉 및 급냉조건 후에 역학적 특성을 평가하였다. 결과적으로, 보통 골재를 사용한 콘크리트는 경량골재를 사용한 콘크리트보다 냉각조건이 미치는 영향이 큰 것으로 나타났다. 그리고 냉각 속도가 빠르지 않을수록 콘크리트의 잔존 역학적 특성이 크게 나타났다.

방사선 경화 비닐에스터 수지의 기계적 특성 연구 (Mechanical Properties of Radiation-Curing Vinyl Ester Resin)

  • 신범식;전준표;김현빈;강필현
    • 방사선산업학회지
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    • 제4권1호
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    • pp.19-23
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    • 2010
  • Vinyl ester (VE) resins, introduced in the late 1960s, have made large strides in reinforced plastics applications as adhesive and matrix materials on their appropriate mechanical performance characteristics in the glassy state. Generally, VE resins are a group of dimethacrylate resins based on bisphenol A type epoxy resin. They exhibit easy handling properties as well as good resistance to most chemical agents due to their mechanical and thermal properties. In this study, the effects of curing methods of vinyl ester resins on gel contents, flexural strength and dynamic mechanical properties were investigated. Thermal curing (room temperature, $80^{\circ}C$) and electron beam curing were used to crosslink a VE resin/styrene complex (65/35 wt%) with methyl ethyl ketone peroxide (MEKPO) as a catalyst and an 8 wt% cobalt naphthenate in styrene solution as a accelerator. For the samples, gel contents as well as flexural strength and dynamic mechanical properties were characterized and compared by soxhlet apparatus, universal testing machine (UTM) and dynamic mechanical analysis (DMA). As a result, the electron-cured VE resin was confirmed as a better condition than those for gel contents, flexural strength and dynamic mechanical properties, respectively.

Thermal effects on the mechanical properties of cement mortars reinforced with aramid, glass, basalt and polypropylene fibers

  • Mazloom, Moosa;Mirzamohammadi, Sajjad
    • Advances in materials Research
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    • 제8권2호
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    • pp.137-154
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    • 2019
  • In this study, thermal effects on the mechanical properties of cement mortars with some types of fibers is investigated. The replaced fibers were made of polypropylene (PP), aramid, glass and basalt. In other words, the main goal of this paper is to study the effects of different fibers on the mechanical properties of cement mortars after subjecting to normal and sub-elevated temperatures. The experimental tests used for investigating these effects were compressive, splitting tensile, and four-point bending tests at 20, 100 and $300^{\circ}C$, respectively. Moreover, the microstructures of the specimens in different temperatures were investigated using scanning electron microscope (SEM). Based on the experimental results, the negative effects of sub-elevated temperatures on four-point bending tests were much more than the others. Moreover, using the fibers with higher melting points could not improve the qualities of the samples in sub-elevated temperatures.

Effects of Nano-silica/Nano-alumina on Mechanical and Physical Properties of Polyurethane Composites and Coatings

  • Swain, Sarojini;Sharma, Ram Avatar;Bhattacharya, Subhendu;Chaudhary, Lokesh
    • Transactions on Electrical and Electronic Materials
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    • 제14권1호
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    • pp.1-8
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    • 2013
  • The present approach shows the use of nano-silica/nano-alumina in polyurethane (PU) matrix, which lead to significant improvements in the mechanical and thermal properties of the nano-composite. It is observed that with incorporation of 1% of nano-alumina into the PU matrix, there is an improvement in the tensile strength of around 50%, and for nano-silica the improvement is around 41%, at the same concentration. The morphological data shows that above 3% of the nano particles there are agglomerations in the nanocomposite. Again with the absorption of moisture, there is a decrease in the thermal and mechanical properties of the PU resin, but in this research work it is observed that with the incorporation of the nano particles, in the presence of absorbed moisture there is an improvement in mechanical and thermal properties of the composite, over that of the PU matrix.

다중벽 탄소나노튜브와 마이크로미터 크기 실리카 입자로 강화된 에폭시 복합재료의 열 안정성에 관한 연구 (Investigation of Thermal Stability of Epoxy Composite Reinforced with Multi-Walled Carbon Nanotubes and Micrometer-Sized Silica Particles)

  • 오륜;유병일;안지호;이교우
    • Composites Research
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    • 제29권5호
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    • pp.306-314
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    • 2016
  • 본 연구에서는 에폭시 복합재료의 기계적 물성을 향상시킴과 동시에 상대적 단점으로 지적될 수 있는 열안정성과 치수 안정성의 문제를 개선하고자 에폭시 복합재료를 다중벽 탄소나노튜브와 마이크로미터 크기의 실리카 입자로 강화하였다. 두 충전제는 별도의 개질 없이 전단혼합과 초음파기기만을 이용하는 물리적 방법으로 에폭시 수지 내에 분산시켰다. 두 충전제 함량에 따른 시편의 특성은 인장강도, 열팽창계수, 열전도도 측정을 통해 평가하였으며, 시편의 열 안정성을 보다 넓은 범위에서 고찰하기 위해 열팽창계수를 측정한 결과와 미시역학 모델을 이용해 계산한 결과를 비교하였다. 탄소나노튜브 함량 0.6 wt%에 실리카 함량 50 wt%로 강화된 하이브리드 복합재료 시편의 인장강도는 에폭시 복합재료 시편 대비 약 11%의 증가를 보여 가장 좋은 기계적 물성을 나타내었다. 열적 물성을 살펴보면 두 충전제의 함량에 따라 그 결과가 달라지는데, 특히 에폭시 수지 내에 실리카 함량이 증가할수록 열팽창계수는 약 36%까지 감소하였고, 이로 인해 시편의 열 변형이 줄어들면서 열 안정성도 개선되었다. 또한 실리카 함량 50 wt%로 강화된 에폭시 복합재료 시편의 열전도도는 약 72% 정도 증가하였다. 두 충전제로 강화된 하이브리드 복합재료 시편에서는 보다 향상된 기계적, 열적 물성을 확보할 수 있었다.

Beryllium oxide utilized in nuclear reactors: Part I: Application history, thermal properties, mechanical properties, corrosion behavior and fabrication methods

  • Ming-dong Hou;Xiang-wen Zhou;Bing Liu
    • Nuclear Engineering and Technology
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    • 제54권12호
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    • pp.4393-4411
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    • 2022
  • In recent years, beryllium oxide has been widely utilized in multiple compact nuclear reactors as the neutron moderator, the neutron reflector or the matrix material with dispersed nuclear fuels due to its prominent properties. In the past 70 years, beryllium oxide has been studied extensively, but rarely been systematically organized. This article provides a systematic review of the application history, thermal properties, mechanical properties, corrosion behavior and fabrication methods of beryllium oxide. Data from previous literature are extracted and sorted out, and all of these original data are attached as the supplementary material, so that subsequent researchers can utilize this paper as a database for beryllium oxide research in reactor design or simulation analysis, etc. In addition, this review article also attempts to point out the insufficiency of research on beryllium oxide, and the possible key research areas about beryllium oxide in the future.

Evaluation of Thermal Durability of Thermal Barrier Coating and Change in Mechanical Behavior

  • Lee, Dong Heon;Kang, Nam Kyu;Lee, Kee Sung;Moon, Heung Soo;Kim, Hyung Tae;Kim, Chul
    • 한국세라믹학회지
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    • 제54권4호
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    • pp.314-322
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    • 2017
  • This study investigates changes in the mechanical behavior, such as changes in indentation load-displacement curve, wear resistance and contact fatigue resistance of thermal barrier coatings (TBCs) by thermal cycling test and thermal shock test. Relatively dense and porous TBCs on nickel-based bondcoat/superalloy are prepared; the highest temperature applied during thermal durability test is $1350^{\circ}C$. The results indicate that the porous TBCs have relatively longer lifetime during thermal cycling and thermal shock tests, while denser TBCs have relatively higher wear and contact fatigue resistance. The mechanical behavior is influenced by sintering of the TBCs by exposure to high temperature during tests.

EMNC_60과 EMNC_65에 대한 열적, 기계적, 전기적 특성 연구 (Thermal, Mechanical, and Electrical Properties for EMNC_60 and EMNC_65)

  • 박재준
    • 한국전기전자재료학회논문지
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    • 제25권11호
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    • pp.895-901
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    • 2012
  • In order to application for high voltage heavy electric equipments, epoxy/microsilica 60 wt%/nano layered silicate composites (EMNC_60) and epoxy/microsilica 65 wt%/nano layered silicate composites (EMNC_65) respectively was synthesized by our electric field dispersion method and the result was obtained completely dispersion state. Thermal properties such as glass transition temperature (Tg) and thermal expansion coefficient, and DMA characteristics were studied, and mechanical properties such as tensile and flexural tests were performed. AC electrical insulation strength was also tested. The study on thermal property, EMNC_65 was better than EMNC_60 and mechanical, electrical properties much improved EMNC_60 compared with EMNC_65.

나노층상실리케이트가 충진된 에폭시-나노콤포지트의 열적특성 연구 (Thermal Characteristics of Epoxy-Nanocomposites filled Several Types Nano Layered Silicate Particles)

  • 박재준
    • 한국전기전자재료학회논문지
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    • 제21권8호
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    • pp.749-754
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    • 2008
  • A large number of studies on the various characteristics of epoxy-layered silicate nanocomposites, such as electric and mechanical, morphology have been conducted and contributed to improve their characteristics. However, studies on the effects of its thermal conductivities in the thermal properties are not enough, even though there are some excellent evaluations for its insulation performances. Thermal properties will cause thermal degradation and significantly affect the reliability of these epoxy-layered silicate nanocomposites. In the results of the analysis of epoxy-layered silicate nanocomposites $T_g$ for various types of organoclays (10A, 15A, 20A, 30B, and 93A), it showed an excellent thermal property of 10A. Also, it represented low values in storage modulus and mechanical Tan (Delta) at a high temperature section 140$^{\circ}C$ and excellent thermal properties due to its movement to the high temperature section in the case of the property of 10A in the measurement of DMA elastics and mechanical losses. In the results of the measurement of thermal conductivities, power ultrasonic applications represented a significant increase in thermal conductivities in the case of the applications of power ultrasonic and planetary centrifugal mixers. Based on these results, it is necessary to perform related studies because it can be applied as useful materials for future power facilities applications in mold and impregnate insulation.