• Title/Summary/Keyword: measuring pH

Search Result 786, Processing Time 0.026 seconds

Studies on the Determination of Rifampicin by Atomic Absorption Spectrophotometry (원자흡광광도법에 의한 리팜피신의 정량에 관한 연구)

  • 이왕규;김박광;유병기
    • YAKHAK HOEJI
    • /
    • v.29 no.4
    • /
    • pp.220-222
    • /
    • 1985
  • Rifampicin reacts with cupric ion to produce rifampicin-Cu(II) chelate (2:1) at pH 6.5, which can be extracted with methylisobutylketone (MIBK). Therefore, rifampicin can be quantitatively, determined by measuring the quantity of Cu(II) in the organic phase by atomic absorption spectrophotometry. Because higher absorbance ratio was obtained in pH 6.0~7.0, buffer solution at pH 6.5 was used in this measurement. Linear relationship was found between absorbance and concentration in the range of 1.0~4.0${\times}10^{-4}M$. This method might be applicable to the determination of rifampicin in the preparations.

  • PDF

Analysis of pH Change and an Automatic pH Control with A New Function:On-Line Estimation of Acetic Acid

  • Jung, Yoon-Keun;Hur, Won
    • Biotechnology and Bioprocess Engineering:BBE
    • /
    • v.2 no.2
    • /
    • pp.69-72
    • /
    • 1997
  • The pH of microbial culture medium was calculated from equations of equilibrium, meterial balances for ionic components and electro-neutrality theory. Ammonium ion consumption and Acetic acid production are found out to be the major contributors for the alteration of the pH as well as the buffer capacity of the medium. By measuring the buffer capacity on-line, levels of acetic acid were estimated by a software sensor using pH signal in a fermentation process of E.coli growing in a minimal medium. The measured values of acetic acid showed good correlation to those of estimated by the software sensor.

  • PDF

On-line Measurement of Buffer Capacity of a Fermentation medium and Estimation of Organic Aicd Production (발효배지의 완충용량의 온라인 측정 및 유기산 생산 추정)

  • Hur, Won;Jung, Yoon-Keun
    • KSBB Journal
    • /
    • v.13 no.4
    • /
    • pp.461-467
    • /
    • 1998
  • A fermentation system was supplemented with a device for the measurement of the durations of alkali pump feeding for automatic pH control and an A/D convertor for precise monitoring of pH value by computer. A software program was developed to measure buffer capacities from the pH signal and the pH control signal during fermentation. By measuring the buffer capacity on-line, levels of acetic acid were estimated by a software sensor using pH signal in a fermentation process of E.coli growing in a minimal medium. The measured values of acetic acid showed correlation to those of estimated by the software sensor. Lacitic acid production was also successfully estimated by the values of buffer capacities measured on-line.

  • PDF

Development of a Micro pH-ISFET Probe for in vivo Measurements of the Ion Concentration in Blood (생체내의 혈중이온농도 예측을 위한 마이크로 pH-ISFET프로브의 개발)

  • Sohn, Byung-Ki;Lee, Jong Hyun;Lee, Kwang Man
    • Journal of the Korean Institute of Telematics and Electronics
    • /
    • v.23 no.1
    • /
    • pp.83-90
    • /
    • 1986
  • A micro pH-ISFET probe, which can be applied to the in vivo measurements of the hydrogen ion concentration in blood, has been developed, and a measuring system equiped with this probe also developed. The pH-ISFET has been fatricated by employing the techniques of integrated circuit fabrication. Two kinds of micro electrode formed around the sensing gate during the wafer process, and the other is a capillary type of Ag/AfCl/sat. KCI reduced in size. This capillary electrode has shown its good performance characteristics so far in the application with ISFET as well as a commercial one. In order to form a micro pH-ISFET probe, this pH-ISFET and well as a commercial one. In order to form a micro pH-ISFET probe, this pH-ISFET and the capillary electrode were built together into a needle tip having 1 mm inner diameter. The chip size of a twin pH-ISFET is 0.8 mmx1.4 mm, the material of the sensing gate membrane is Si3N4, and the sensitivity of the developed probe is about 52mV/pH.

  • PDF

The application of a nondestructive method to measure the acidity of Korean papers (한지의 산성도 측정을 위한 비파괴적 방법의 적용)

  • Lee, Hye-Yun;Chung, Yong-Jae;Lee, Kyu-Sik;Han, Sung-Hee
    • 보존과학연구
    • /
    • s.20
    • /
    • pp.21-47
    • /
    • 1999
  • According to damage of papers by the chemical cause, papers become to acidify. Among the 3 kinds of method measuring the acidity of paper, one was nondestructive method measuring the surface of the paper by flat type electrode and the others were destructive methods measuring directly by cold water extract method and hot water extract method. In case of the cellulolytic cultural properties, the latter methods were not applied because those methods must bedissociated papers. To measure the paper acidity nondestructively, we investigated the correlation of the nondestructive method and the destructive methods. The conclusions are as follows. 1) In the relationship of the cold water extract method and the hot water extract method, It was indicated that the pH measured by the hot water extract method was high quality printing paper 0.08, rough printing paper 0.13, and Korean paper 0.29 higher than that by the cold water extract method.2) In the relationship of the cold water extract method and the surface measurement method, It showed that the pH value measured by the cold water extract method was high quality printing paper 1.86, rough printing paper 0.80,and Korean paper 0.58 higher than value that by the surface measurement.3) In the relationship of the hot water extract method and the surface measurement method, It showed that the pH value measured by the hot ABSTRACT water extract method was high quality printing paper 1.78, rough printing paper 0.66, and Korean paper 0.29 higher than that by the surface measurement. From the above-mentioned results, the pH value measured by the surface measurement was need to high about 1.78∼1.86 in high quality printing paper, 0.66-0.80 in rough printing paper, and 0.29∼0.58 in Korean paper and the surface measurement with flat type electrode was very available to measure the acidity of Korean papers actually.

  • PDF

On-site conservation of a gilt bronze crown (발굴현장 수습 유물 보존처리)

  • Yu, Jae-Eun
    • 보존과학연구
    • /
    • s.20
    • /
    • pp.49-64
    • /
    • 1999
  • According to damage of papers by the chemical cause, papers become to acidify. Among the 3 kinds of method measuring the acidity of paper, one was nondestructive method measuring the surface of the paper by flat type electrode and the others were destructive methods measuring directly by cold water extract method and hot water extract method. In case of the cellulolytic cultural properties, the latter methods were not applied because those methods must bedissociated papers. To measure the paper acidity nondestructively, we investigated the correlation of the nondestructive method and the destructive methods. The conclusions are as follows. 1) In the relationship of the cold water extract method and the hot water extract method, It was indicated that the pH measured by the hot water extract method was high quality printing paper 0.08, rough printing paper 0.13, and Korean paper 0.29 higher than that by the cold water extract method.2) In the relationship of the cold water extract method and the surface measurement method, It showed that the pH value measured by the cold water extract method was high quality printing paper 1.86, rough printing paper 0.80,and Korean paper 0.58 higher than value that by the surface measurement.3) In the relationship of the hot water extract method and the surface measurement method, It showed that the pH value measured by the hot ABSTRACT water extract method was high quality printing paper 1.78, rough printing paper 0.66, and Korean paper 0.29 higher than that by the surface measurement. From the above-mentioned results, the pH value measured by the surface measurement was need to high about 1.78∼1.86 in high quality printing paper, 0.66-0.80 in rough printing paper, and 0.29∼0.58 in Korean paper and the surface measurement with flat type electrode was very available to measure the acidity of Korean papers actually.

  • PDF

Rates and Mechanism of Decomposition of Hydrogen Peroxide by Copper(Ⅱ)-Amines Complexes (구리(Ⅱ)-아민류착물에 의한 과산화수소의 분해반응속도와 메카니즘)

  • Sun-Deuk Kim;Yun-Yeol Shin;Jeong-Eun Park;Chang-Su Kim
    • Journal of the Korean Chemical Society
    • /
    • v.37 no.2
    • /
    • pp.199-205
    • /
    • 1993
  • The decomposition of hydrogen peroxide by copper-amines complexes was studied in the pH range of 7.3∼11.3 by measuring the rate of the decreasing concentration of $H_2O_2$. Decomposition rate of hydrogen peroxide increased with increasing pH, and then decreased with increasing pH successively. The mechanism for this type of reaction involves the formation of peroxo complexes in the rate-determining step preceding deprotonation of hydrogen peroxide and copper-amines complexes.

  • PDF

Feasibility Study on the Development of Fiber-Optic pH Sensor for Endoscope (내시경용 광섬유 pH 측정 센서 개발을 위한 기초 연구)

  • Lee, Bong-Soo;Hong, Ju-Young;Hwang, Young-Muk;Cho, Seung-Hyun
    • Journal of Sensor Science and Technology
    • /
    • v.13 no.3
    • /
    • pp.213-217
    • /
    • 2004
  • The general method to find a H. pylori in the stomach is the rapid urease test but it is only used to decide the infection with H. pylori. In this study, it is tried to develope fiber-optic pH sensor which can be used with gastroscop to quantify H. pylori. To measure the degree of infection with H. pylori, the color change of phenol red according to the degree of pH is measured by optical fibers with different light sources and the optimum distance from a sample to the end of sensor tip is decided by measuring the maximum reflectivity from a sample. Also the sensitivity study is carried out to decide the optimum light source which has sensitive change of reflectivity to the change of pH. It is expected that the fiber-optic pH sensor which measures the degree of infection with H. pylori exactly can be developed.

Rapid Detection of Growth factors of intestinal Lactic Acid Bacteria (장내유산균 증식인자의 신속한 검색)

  • 한명주;임혜영;김동현
    • Journal of Food Hygiene and Safety
    • /
    • v.8 no.2
    • /
    • pp.91-95
    • /
    • 1993
  • The growth of Bifidobacterium and Lactobacillus isolated from human interstinal bacteria were induced by water extract and U-step extract of soybean and carrot and the pH of these bacteria-cultured media were decreased. The increasing growth rates of these bacteria are related to the decrease of the pH of these bacteria-cultured media. When human intestinal flora as starter were inoculated into the medium containing water extract of soybean and carrot. the growth of lactic bacteria were also induced and the pH of the media were decreased. By measuring the pH of the media which were inoculated and cultured intestinal bacteria as a starter, it is possible to determine whether the food are the growth factors of intestinal lactic acid bacteria or not. By this method, the food which decreased pH of the medium were soybean, turnip, carrot. leek, garic, dropwork, wonnwood and onion. 'These foods may induce lactic acid bacteria in human in1estlne.

  • PDF

The development of pH reading system based on vision system (영상 기반 pH 산도 측정 시스템 개발)

  • Moon, Ha-Jung;Lee, Dong-Hoon
    • Journal of IKEEE
    • /
    • v.17 no.4
    • /
    • pp.398-406
    • /
    • 2013
  • Nuclear medicine imaging devices such as PET diagnose disease after injecting radiopharmaceuticals in human body for diagnosis. Radiopharmaceuticals should maintain the proper pH for human body safety. In general, pH paper is used to measure the pH of the radiopharmaceutical. pH of the sample compared with the standard color chart is used for measurement. However, the pH reading difference according to the experience of a rater can be generated. Also, a pH meter for measuring pH has a high sensitivity and contamination of the sensor must be avoided. In this paper, we developed the new hardware device for pH reading method and software was developed with vision algorithm to measure pH easily and simply.