• Title/Summary/Keyword: matrix analysis

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Tertiary Matrices for the Analysis of Polyethylene Glycols Using MALDI-TOF MS

  • Hong, Jangmi;Kim, Taehee;Kim, Jeongkwon
    • Mass Spectrometry Letters
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    • v.5 no.2
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    • pp.49-51
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    • 2014
  • The effectiveness of tertiary matrices composed of the combination of three common matrices (dihydrobenzoic acid (DHB), ${\alpha}$-cyano-4-hydroxycinnamic acid (CHCA), and sinapinic acid (SA)) was compared with that of single or binary matrices in the analysis of polyethylene glycol (PEG) polymers ranging from 1400 to 10000 Da using matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS). A tertiary matrix of 2,5-DHB+CHCA+SA was the most effective in terms of S/N ratios. CHCA and CHCA+SA produced the highest S/N ratios among the single matrices and the binary matrices, respectively. The improvement observed when using a tertiary matrix in analyses of PEG polymers by MALDI-TOF MS is believed to be due to the uniform morphology of the MALDI sample spots and synergistic effects arising from the mixture of the three matrix materials.

Sample Preparation for Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry

  • Kim, Jeongkwon
    • Mass Spectrometry Letters
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    • v.6 no.2
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    • pp.27-30
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    • 2015
  • This article reviews the fundamentals of sample preparation used in matrix-assisted laser desorption/ionization-mass spectrometry (MALDI-MS). MALDI is a soft ionization method used to generate analyte ions in their intact forms, which are then detected in MS analysis. MALDI-MS boasts fast analysis times and easy-to-use operation. The disadvantages of MALDI-MS include the occurrence of matrix-associated peaks and inhomogeneous distribution of analyte within the matrix. To overcome the disadvantages of MALDI-MS, various efforts have been directed such as using different matrices, novel matrix systems, various additives, and different sample preparation methods. These various efforts will be discussed in detail. This article will benefit those who would like to obtain basic knowledge of MALDI sample preparation and those who would like to use MALDI-MS in their chemical analyses.

On the Structure of A Matrix for Dynamic Stability Analysis of One Machine to the Infinite Bus (발전기-무한모선계통의 동태안정도 해석시 A행렬의 구조)

  • Kwon, Sae-Hyuk;Song, Kil-Yeong
    • Proceedings of the KIEE Conference
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    • 1989.07a
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    • pp.211-215
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    • 1989
  • The structure of A matrix of one machine connected to the infinite bus is described for a full model. The A matrix can be partitioned to submatrices which depend on the initial operating point and do not depend on it. When the dynamic properties for several different operating points are desired, those submatrices can be obtained through simple column operations. Furthermore, the elements of A matrix car be directly calculated from the manufacturer's data. RMS quantities of the state variables for the initial operating point are used. This approach can save the labor for calculating the elements of A matrix for the dynamic stability analysis.

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Numerical Method for the Analysis of Bilinear Systems via Legendre Wavelets (르장드르 웨이블릿을 이용한 쌍일차 시스템 수치 해석)

  • Kim, Beomsoo
    • Journal of Institute of Control, Robotics and Systems
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    • v.19 no.9
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    • pp.827-833
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    • 2013
  • In this paper, an efficient computational method is presented for state space analysis of bilinear systems via Legendre wavelets. The differential matrix equation is converted to a generalized Sylvester matrix equation by using Legendre wavelets as a basis. First, an explicit expression for the inverse of the integral operational matrix of the Legendre wavelets is presented. Then using it, we propose a preorder traversal algorithm to solve the generalized Sylvester matrix equation, which greatly reduces the computation time. Finally the efficiency of the proposed method is discussed using numerical examples.

Design of an Intelligent Polymer-Matrix-Composite Using Shape Memory Alloy (형상기억합금을 이용한 지능형 고분자 복합재료의 설계)

  • Jeong, Tae-Heon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.10
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    • pp.1609-1618
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    • 1997
  • Thermo-mechanical behaviors of polymer matrix composite(PMC) with continuous TiNi fiber are studied using theoretical analysis with 1-D analytical model and numerical analysis with 2-D multi-fiber finite element(FE) model. It is found that both compressive stress in matrix and tensile stress in TiNi fiber are the source of strengthening mechanisms and thermo-mechanical coupling. Thermal expansion of continuous TiNi fiber reinforced PMC has been compared with various mechanical behaviors as a function of fiber volume fraction, degree of pre-strain and modulus ratio between TiNi fiber and polymer matrix. Based on the concept of so-called shape memory composite(SMC) with a permanent shape memory effect, the critical modulus ratio is determined to obtain a smart composite with no or minimum thermal deformation. The critical modulus ratio should be a major factor for design and manufacturing of SMC.

A Micromechanical Analysis on the Elastic Behavior in Discontinuous Metal Matrix Composites (불연속 금속복합체에서의 탄성거동에 관한 미세구조역학적 해석)

    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.6 no.3
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    • pp.58-64
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    • 1997
  • A micromechanics model to describe the elastic behavior of fiber or whisker reinforced metal matrix composites was developed and the stress concentrations between reinforcements were investigated using the modified shear lag model with the comparison of finite element analysis (FEA). The rationale is based on the replacement of the matrix between fiber ends with the fictitious fiber to maintain the compatibility of displacement and traction. It was found that the new model gives a good agreement with FEA results in the small fiber aspect ratio regime as well as that in the large fiber aspect ratio regime. By the calculation of the present model, stress concentration factor in the matrix and the composite elastic modulus were predicted accurately. Some important factors affecting stress concentrations, such as fiber volume fraction, fiber aspect ratio, end gap size, and modulus ratio, were also discussed.

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Elastic-Plastic Stress Distributions Behavior in the Interface of SiC/Ti-15-3 MMC under Transverse Loading(II) (횡하중을 받는 SiC/Ti-15-3 MMC 복합재 계면영역에서의 탄소성 응력장분포거동(II))

  • Kang Ji-Woong;Kwon Oh-Heon
    • Journal of the Korean Society of Safety
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    • v.20 no.2 s.70
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    • pp.26-31
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    • 2005
  • The strong continuous fiber reinforced metal matrix composites (MMCs) are recently used in aerospace and transportation applications as an advanced material due to its high strength and light weight. Unidirectional fiber-metal matrix composites have superior mechanical properties along the longitudinal direction. However, the applicability of continuous fiber reinforced MMCs is somewhat limited due to their relatively poor transverse properties. Therefore, the transverse properties of MMCs are significantly influenced by the properties of the fiber/matrix interface. In order to be able to utilize these MMCs effectively and with safety, it must be determined their elastic plastic behaviors at the interface. In this study, the interfacial stress states of transversely loaded unidirectional fiber reinforced metal matrix composites investigated by using elastic-plastic finite element analysis. Different fiber volume fractions $(5-60\%)$ were studied numerically. The interlace was treated as three thin layer (with different properties) with a finite thickness between the fiber and the matrix. The fiber is modeled as transversely isotropic linear-elastic, and the matrix as isotropic elastic-plastic material. Using proposed model, the effects of the interface region and fiber arrangement in MMCs on the distributions of stress and strain are evaluated. The stress distributions of a thin multi layer interface have much less changes compared with conventional perfect interface. The analyses were based on a two-dimensional generalized plane strain model of a cross-section of an unidirectional composite by the ANSYS finite element analysis code.

Development of an Informetric Analysis System KnowledgeMatrix (계량정보분석시스템 KnowledgeMatrix 개발)

  • Lee, Bangrae;Yeo, Woon Dong;Lee, June Young;Lee, Chang-Hoan;Kwon, Oh-Jin;Moon, Yeong-ho
    • Proceedings of the Korea Contents Association Conference
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    • 2007.11a
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    • pp.167-171
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    • 2007
  • Application areas of Knowledge Discovery in Database (KDD) have been expanded into many R&D management processes including technology trends analysis, forecasting and evaluation etc. Established research field such as informetrics (or scientometrics) has recently fully utilized techniques or methods of KDD. Various systems have been developed to support works of analyzing large-scale R&D related databases such as patent DB or bibliographic DB by a few researchers or institutions. But extant systems have some problems for korean users to use. Their prices is not cheap, korean language process not available, and user's demands not reflected. To solve these problems, Korea Institute of Science and Technology Information (KISTI) developed stand-alone type information analysis system named as KnowledgeMatrix. KnowledgeMatrix system offer various functions to analyze retrieved data set from databases. Knowledge Matrix main operation unit is composed of user-defined lists and matrix generation, cluster analysis, visualization, data pre-processing. KnowledgeMatrix show better performances and offer more various functions than extant systems.

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Stability Analysis of Induction Motor Rotor by Unbalanced Electromagnetic Forces (불평형 전자기력에 의한 유도전동기 회전자의 안정성해석)

  • 양보석;손병구
    • Journal of KSNVE
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    • v.8 no.6
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    • pp.1086-1092
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    • 1998
  • This paper presents a general analytical method for analyzing the instability of unbalanced electromagnetic forces produced in induction motors with an eccentric rotor. The equations to be solved are a set of second order differential equations which give matrices with periodic coefficients that are a function of time due to the unbalanced electromagnetic force. The method is based on an extension of the Floquet theory. A transfer matrix over one period of the motion is obtained. and the stability of the system can be determined with the eigenvalues of the matrix. The analysis results of instability zone were coincided upon comparing that of transfer matrix method with that of rotating frame. Two examples are given. including an industrial application. The results show that the method proposed is satisfactory.

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Design and Characterization of a Reactor for Matrix Type SFCLs Using Electromagnetic Field Analysis (전자장 해석을 통한 매트릭스형 한류기용 리액터 설계 및 특성해석)

  • Chung, Dong-Chul;Yun, Chang-Hun;Choi, Hyo-Sang
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.58 no.2
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    • pp.227-230
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    • 2009
  • In this paper, we performed the optimum design of reactors for matrix-type superconducting-fault current limiters (SFCLs), using electromagnetic analysis tools. We decided a optimun position within a reactor for superconducting elements of current-limiting parts and trigger parts from the calculation of magnetic flux internsity for reactor structures. Also we decided effective distance length between two reactors through the analysis of the distribution of magnetic field, according to distance lengths between them. We designed and characterized matrix-type SFCLs, based on our optimum design of a reactor. We confirmed uniform distribution of a fault current, resulted from the improvement of simultaneous quench characteristics within our matrix-type SFCL.