• Analytical Science and Technology
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• v.7 no.2
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• pp.155-164
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• 1994

A conventional Grimm-type glow discharge source was constructed and applied to radio-frequency(13.56MHz) discharge for metal and ceramic analysis. We investigated the emission spectrum for aluminium and aluminium oxide and the influence of discharge operating paramaters including argon pressure, rf-power and DC-bias voltages at the sample-side electrode. Scanning Electron Microscope(SEM) also was used to investigate the effect of rf-sputtering on the microstructure formation of the aluminium oxide. Linear analytical calibration curves were constructed for Manganese and zinc element in samples of low alloy steel(BAS 401-405) and brass(NIST 1108-1117).

• Steel and Composite Structures
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• v.21 no.3
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• pp.573-588
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• 2016

Carbon Fiber Reinforced Plastic (CFRP) and Titanium Alloy (Ti6Al4V) stack, extensively used in aerospace structural components are assembled by fasteners and the holes are made using drilling process. Drilling of stack in one shot is a complicated process due to dissimilarity in the material properties. It is vital to have optimal machining condition and tool geometry for better hole quality and tool life. In this study the tool wear and hole quality were analysed by experimental analysis using three modified twist drills and online tool condition monitoring using Acoustics Emission (AE) sensor. Helix angle and point angle influence tool performance and cutting force. It was found that a tool geometry (TG1) with high helix angle of $35^{\circ}$ with low point angle $130^{\circ}$ results in reduction in thrust force of 150-500 N range but the TG2 also perform almost similar to TG1, but when compared with the AErms voltage generated during drilling it was found that progressive rise in voltage in TG1 is less with respect to TG2 which can be attributed to tool life. In process wear monitoring was done using crest factor as monitoring index. AErms voltage were measured and correlated with the performance of the drills.

• Journal of the Korean Society for Heat Treatment
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• v.18 no.3
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• pp.172-176
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• 2005

Modern automobiles are built with a steadily increasing variety of materials and semifinished products. The traditional composition of steel sheet and cast iron is being replaced with other materials such as aluminum and magnesium. But low formability of these materials has prevented the application of the automotive components. The formability can be enhanced by conducting the warm hydroforming using induction heating device which can raise the temperature of the specimen very quickly. The specimen applied to the test is A6061, A7075 extruded tubes which belong to the age-hardenable aluminum alloys. But in the case of A6061 age hardening occurs at room temperature or at elevated temperatures before and after the forming process. In this study the effects of the heating condition such as heating time, preset temperature, holding time during die closing and forming time on the hydroformability are analyzed to evaluate the phenomena such as dynamic strain hardening and ageing hardening at high temperatures after the hydroforming process.

• Transactions of Materials Processing
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• v.16 no.4 s.94
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• pp.266-270
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• 2007

Inertia welding is a solid-state welding process in which butt welds in materials are made in bar and in ring form at the joint face, and energy required for welding is obtained from a rotating flywheel. The stored energy is converted to frictional heat at the interface under axial load. The quality of the welded joint depends on many parameters, including axial force, initial revolution speed and energy, amount of upset, working time, and residual stresses in the joint. Inertia welding was conducted to make the large rotor shaft for low speed marine diesel engine, alloy steel for shaft of 140mm. Due to material characteristics, such as, thermal conductivity and high temperature flow stress, on the two sides of the weld interface, modeling is crucial in determining the optimal weld parameters. FE simulation is performed by the commercial code DEFORM-2D. A good agreement between the predicted and actual welded shape is observed. It is expected that modeling will significantly reduce the number of experimental trials needed to determine the weld parameters.

• Analytical Science and Technology
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• v.8 no.4
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• pp.443-448
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• 1995

Three anode configurations of six-jet, cone-jet and cylindrical-jet are tested for their analytical performance under power mode operation. The effect of pressure, power and gas flow rate on atomic absorption signals have been studied. The increase of atomic absorption signal of sample element is observed at a fixed pressure in all configurations as the gas flow rate increase up to 300-600 seem, and as the power dissipated in the glow discharge cell increase. The lower the pressure is in the glow discharge cell at a fixed discharge power and argon flow rate, the greater the absorbance of sample element is. The optimum conditions are taken from these data and a calibration curve of Cu in low-alloy steel sample is obtained. In this calibration curve, six-jet configuration shows the best analytical results varies as the sample element.

• Journal of Ocean Engineering and Technology
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• v.29 no.6
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• pp.481-487
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• 2015

The effects of the heat input and preheat/interpass temperatures on the tensile strength and impact toughness of multipass welded weld metal were investigated and interpreted in terms of the recovery of the alloying elements and microstructure. Increases in both the heat input and preheat/interpass temperatures decreased the tensile strength of the weld metal. A lower recovery of alloying elements, especially Mn and Si, and smaller area fraction of acicular ferrite in the weld metal were observed in higher heat input welding, resulting in a lower tensile strength. In contrast, only a microstructure difference was observed at a higher preheat/interpass temperature. The impact toughness of the weld metal gradually increased with an increase in the heat input because of the lower tensile strength. However, it decreased again when the heat input was larger than 45 kJ/cm because of the much smaller area fraction of acicular ferrite. No effect of the preheat/interpass temperature on the impact toughness was observed. The formation of a weld metal heat-affect zone showed little effect on the impact toughness of the weld metal in this experiment.

• Bulletin of the Korean Chemical Society
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• v.30 no.11
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• pp.2577-2583
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• 2009

Presented are the formation of iron oxide layers on evaporator tubes in an actual fossil power plant operated under all volatile treatment (AVT) condition and an experimental simulation of iron oxide formation in the presence of ferrous and ferric ions. After actual operations for 12781 and 36326 hr in the power plant, two iron oxide layers of magnetite on the evaporator tubes were found: a continuous inner layer and a porous outer layer. The experimental simulation (i.e., artificial corrosion in the presence of ferrous and ferric ions at 100 ppm level for 100 hr) reveals that ferrous ions turn the continuous inner oxide layer on tube metal to cracks and pores, while ferric ions facilitate the production of porous outer oxide layer consisting of large crystallites. Based on a comparison of the oxide layers produced in the experimental simulation with those observed on the actually used tubes, we propose possible routes for oxid layer formation schematically. In addition, the limits of the proposed corrosion routes are discussed in detail.

• Proceedings of the Acoustical Society of Korea Conference
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• autumn
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• pp.231-234
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• 2000

In relation to a non-destructive evaluation of irradiation damage of micro-structure of interstitial, void and dislocation, the changes in the hysteresis loop and Barkhausen noise amplitude and the harmonics frequency due to neutron irradiation were measured and evaluated. The Mn-Mo-Ni low alloy steel of reactor pressure vessel was irradiated to a neutron fluence of $2.3\times10^{19}n/cm^2$ $(E\ge1MeV)$ at $288^{\circ}C.$The saturation magnetization of neutron irradiated metal did not change. Neutron irradiation caused the coercivity to increase, whereas susceptibility to decrease. The amplitude of Barkhausen noise parameters associated with the domain wall motion were decreased by neutron irradiation. The spectrum of Barkhausen noise was analyzed with an applied frequency of 4Hz and 8Hz, and a sampling time of 50 $\mu$ sec and 20 $\mu$ sec. The harmonic frequency of Joule effect shows 4Hz, 8Hz, 12Hz and 16Hz reflected from an unirradiated specimen. On the contrary, the harmonic frequency disappeared for the irradiated specimen. Harmonic frequency of induced voltage of sinusoidal magnetic field And Spectrum of Barkhausen noise on material is determined.

• Advances in materials Research
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• v.7 no.3
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• pp.195-201
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• 2018

High Strength low alloy steels containing various levels of C, Nb and Mn were used and for each of which, a simulated double thermal cycle was applied with the same first peak temperature and different second peak temperatures to produce HAZ microstructure corresponding to multi-pass weld. Effect of double cycle second temperature on the microstructure was observed and compared with single cycle results obtained from previous works, it was found that the percentage of martensite austenite constituent (MA) increases by Nb addition for all steels with the same Mn content and the increase in Mn content at the same Nb content shows an increase in MA area fraction as well. MA area fraction obtained for the double cycle is larger than that obtained for the single cycle for all steels used which imply that MA will have great role in the brittle fracture initiation for double cycle and the inter-pass temperature should be controlled for medium and high-carbon Mn steel to avoid large area fraction of MA. The beneficial effects of Niobium obtained in single pass weld were not observed for the double cycle or multi pass welds.

• Transactions of Materials Processing
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• v.32 no.2
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• pp.92-99
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• 2023

In this study, shear fracture specimens are designed using finite element analyses for the characterization of ductile fracture criteria of metal sheets. Many recently suggested ductile fracture criteria require experimental fracture data at the shear stress states in the model parameter identification. However, it is challenging to maintain shear stress states in tension-based specimens from the initial yield to the final fracture, and the loading path can be different for the different materials even with the same shear specimen geometries. To account for this issue, two different shear fracture specimens for low ductility/high ductility metal sheets are designed using the sensitivity tests conducted by finite element simulations. Priorly mechanical properties including the Hosford-Coulomb fracture criterion of the aluminum alloy 7075-T6 and DP590 steel sheets are used in the simulations. The results show that shear stress states are well-maintained until the fracture at the fracture initiation points by optimizing the notch geometries of the shear fracture specimens.