• Corrosion Science and Technology
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• v.6 no.1
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• pp.24-28
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• 2007

Alumina coated SiC whiskers were prepared by homogeneous precipitation of aluminum sulfate. The Si3N4 composites reinforced with coated SiC whiskers were fabricated by hot-pressing at $1800^{\circ}C$ for 2 h under an $N_{2}$ atmosphere of 0.1 MPa to examine the effects of coated whiskers on the mechanical properties of SiC whisker reinforced $Si_{3}N_{4}$ composite. By the addition of alumina coated SiC whiskers instead of as received ones, the fracture toughness of composite was about 6.7 $MPam^{1/2}$ which was slightly lower than as received SiC whisker reinforced composite. This result seems to be caused by the fact that the crack deflection and whisker pull-out were decreased. Thus, alumina coated SiC whiskers were considered to form relatively strong interface bond with $Si_{3}N_{4}$ matrix.

• Transactions on Electrical and Electronic Materials
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• v.7 no.4
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• pp.204-209
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• 2006

Photo Resist (PR) ashing process was carried out with the atmospheric pressure- dielectric barrier discharge (ADBD) using $SF_6/N_2/O_2$. Ashing rate (AR) was sensitive to the mixing ratio of the oxygen and nitrogen of the blower type of ADBD asher. The maximum AR of 5000 A/min was achieved at 2% of oxygen in the $N_2$ plasma. With increasing the oxygen concentration to more than 2% in the $N_2$ plasma, the discharge becomes weak due to the high electron affinity of oxygen, resulting in the decrease of AR. When adding 0.5% of SF6 to $O_2/N_2$ mixed plasma, the PR AR increased drastically to 9000 A/min and the ashed surface of PR was smoother compared to the processed surface without $SF_6$. Carbon Fluorinated polymer may passivate the PR surface. It was also observed that the glass surface was not damaged by the fluorine.

• The Journal of Korean Academy of Prosthodontics
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• v.45 no.6
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• pp.769-779
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• 2007

Statement of problem. When TiN coating is applied to the abutment screw, occurrence of greater preload and prevention of the screw loosening could be expected due to decrease of frictional resistance. However, the proper thickness of TiN coating on abutment screw has not been yet reported. Purpose. The purpose of this study is to find out the appropriate TiN coating thickness by evaluating the detorque force and the surface change of titanium abutment screw with various TiN coating thickness. Material and methods. 1. Material Thirty five non-coated abutment screws were prepared for TiN coating. TiN coatings were prepared by Arc ion plating method. Depending on the coating deposition time(CDT), experimental groups were divided into 6 groups(CDT 30min, 60min, 90min, 120min, 150min, 180min) and those of 1 group was not coated as a control group. Each group was made up of 5 abutment screws. 2. Methods FE-SEM(Field Emission Scanning Electron Microscoper) and EDX(Energy Dispersive X-ray Spectroscopy) were used to observe the surface of the abutment screw. Electric scales was used to measure the weight of the abutment screw after the repeated closing and opening of 10 trials. Detorque force was measured with digital torque gauge, at each trial. Results. 1. As the coating deposition time increased, the surface became more consistent and smooth. 2. As for the abutment screws that were TiN coated for more than 60 minutes, no surface change was found after the repeated closing and opening. 3. The TiN coated abutment screws showed less weight change than the non-coated abutment screws. 4. The TiN coated abutment screws showed higher mean detorque force than the noncoated abutment screws. 5. The abutment screw coated for 60 minutes showed the highest mean detorque force. Conclusion. The coating layer of proper thickness is demanded to obtain consistent and smooth coating surface, resistance to wear, and increased detorque force of the abutment screw. In conclusion, the coating deposition time of 60 minutes indicated improved mechanical property, when TiN coating was conducted on titanium abutment screw.

• 제어로봇시스템학회:학술대회논문집
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• 1996.10a
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• pp.95-98
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• 1996

Universal Learning Network(U.L.N.), which can model and control the large scale complicated systems naturally, consists of nonlinearly operated nodes and multi-branches that may have arbitrary time delays including zero or minus ones. Therefore, U.L.N. can be applied to many kinds of systems which are difficult to be expressed by ordinary first order difference equations with one sampling time delay. It has been already reported that learning algorithm of parameter variables in U.L.N. by forward and backward propagation is useful for modeling, managing and controlling of the large scale complicated systems such as industrial plants, economic, social and life phenomena. But, in the previous learning algorithm of U.L.N., time delays between the nodes were fixed, in other words, criterion function of U.L.N. was improved by adjusting only parameter variables. In this paper, a new learning algorithm is proposed, where not only parameter variables but also time delays between the nodes can be adjusted. Because time delays are integral numbers, adjustment of time delays can be carried out by a kind of random search procedure which executes intensified and diversified search in a single framework.

• The Journal of Engineering Geology
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• v.5 no.2
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• pp.129-138
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• 1995

To elucidate the effects of flow rate on the hydraulic fracturing property of andesite, the hydraulic fracturing tests were conducted under three flow rates. As the tests are conducted with 1ml/min, 2ml/min and 3 ml/min under the constant axial load of 40 kN, the breakdown pressures of andesite seem to be constant as 163kg/cm$^2$. The hydraulic fracturing tests were carried out under the temperatures of five stages to elucidate the effects of temperature variation on hydraulic fracturing property of granite. As the tests are carried out under the constant flow rate of 1.7ml/min, with the axial load of 40kN, the breakdown pressures of granite are 168kg/cm$^2$ at room temperature, and 124kg/cm$^2$ at 20$0^{\circ}C$. The breakdown pressure decreases about 25% than that of room temperature with increasing the temperature. Under the controlled flow rates, the initiation pressures of the microcracks of granite are well coincided with the breakdown pressures and these results are also confirmed by the levels of acoustic emission.

• Bulletin of the Korean Chemical Society
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• v.33 no.2
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• pp.459-463
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• 2012

N-hydroxyphthalimide (NHPI) and copper chloride ($CuCl_2$) were first utilized for aerobic oxidation of ${\alpha}$-isophorone (${\alpha}$-IP) to ketoisophorone (KIP) and the effects of co-catalysts, temperature, reaction time, solvent, amount of $CuCl_2$ and pressure of oxygen were investigated extensively. NHPI/$CuCl_2$ turned out to be highly efficient to this oxidation with up to 91.3% conversion and 81.0% selectivity under mild conditions. And various hydrocarbons including benzylic compounds, cycloalkene and its derivatives were also oxidized smoothly under optimized conditions. Moreover, the possible reaction mechanism was proposed and verified by FT-IR spectra.

• Korean Journal of Materials Research
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• v.11 no.10
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• pp.863-868
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• 2001

The present study was carried out to investigate the effect of MA processing variables on the microstructural properties of composite powders and the coefficient of thermal expansion of pulse electric current sintered AlN-Cu powder compacts. The AlN-Cu powders had a size of less than 15 $\mu\textrm{m}$ with 25 nm size of copper crystallite after MA 32 hours. The finely distributed AlN-Cu powder compacts were completely achieved after PECS. The residual oxygen was considerably removed after hydrogen reduction treatment. The residual carbon was completely removed to 97%. The CTE of AlN-Cu powder compacts showed a good consistency with Kingery-Tuner model when the volume fraction of copper was less than 60%. When it was more than 60%, the CTE had a good agreement with Series model.

• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.421-422
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• 2013

Recently, ZnO has received attentionbecause of its applications in optoelectronics and spintronics. In order to investigate deep level defects in ZnO, we used N-doped ZnO with various of the N-doping concentration. which are reference samples (undoped ZnO), 27%, 49%, and 88%-doped ZnO. Photoinduced current transient spectroscopy (PICTS) measurement was carried out to find deep level traps in high resistive ZnO:N. In reference ZnO sample, a deep trap was found to located at 0.31 (as denoted as the CO trap) eV below conduction band edge. And the CN1 and CN2 traps were located at 0.09, at 0.17 eV below conduction band edge, respectively. In the case of both annealed samples at 200 and $300^{\circ}C$, the defect density of the CO trap increases and then decreases with an increase of N-doping concentration. On the other hands, the density of CN traps has little change according to an increase of N-doping concentration in the annealed sample at $300^{\circ}C$. According to the result of PICTS measurement for different N-doping concentration, we suggest that the CO trap could be controled by N-doping and the CN traps be stabilized by thermal annealing at $300^{\circ}C$.

• Bulletin of the Korean Mathematical Society
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• v.57 no.5
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• pp.1095-1113
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• 2020

In this paper, we investigate the transcendental meromorphic solutions for the nonlinear differential equations $f^nf^{(k)}+Q_{d_*}(z,f)=R(z)e^{{\alpha}(z)}$ and fⁿf^(k) + Q_d(z, f) = p₁(z)e^α₁(z) + p₂(z)e^α₂(z), where $Q_{d_*}(z,f)$ and Q_d(z, f) are differential polynomials in f with small functions as coefficients, of degree d_* (≤ n - 1) and d (≤ n - 2) respectively, R, p₁, p₂ are non-vanishing small functions of f, and α, α₁, α₂ are nonconstant entire functions. In particular, we give out the conditions for ensuring the existence of these kinds of meromorphic solutions and their possible forms of the above equations.

• Proceedings of the KIEE Conference
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• 1990.07a
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• pp.177-179
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• 1990

Recently, it is reported that the behaviour of PECVD under high electric field and current condition has a major effect on MNS device degradation. In this paper, we evaluated the breakdown and TDDB characteristics of Laser assisted PECVD SiN films which is introduced new deposited method. And also, long term insulator breakdown reliability is described by examing time dependent dielectric breakdown under positive voltage. Failure tines against electric field are examined and acceleration factors are obtained for each case. From these data, breakdown wearout limitation for Laser Assisted PECVD SiN film can be characterized.