• Title/Summary/Keyword: inter-sampling

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NIR - a Tool for Evaluation of Milling Procedure

  • Gergely, Sziveszter;Handzel, Lidia;Zoltan, Andrea;Salgo, Andras
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1125-1125
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    • 2001
  • Micro-scale test methods are producing small-sample size where the conventional physical and chemical tests can not be used (high standard deviation, uncertain sampling conditions, low repeatability). Different small-scale test methods were developed recently for determination of physico-chemical, functional, rheological properties of wheat or wheat dough using miniaturized instruments with sophisticated sample preparation/handling and mechanics (RVA, 2 g mixograph, micro-Z-arm mixer, small-scale noodle maker, micro-baking method etc.). The small-scale methodologies can be used as basic research tools or as technology supported measurements and can be also essential in the early selection for quality traits in breeding programs. The milling as a sample preparation step is essential procedure providing good quality flour or semolina samples from small amount of grain (5-10 g) in a reproducible and reliable way. The aim of present study was to use NIR as quality control tool, and to evaluate the recently developed and manufactured micro-scale lab mill (FQC-2000) produced by Inter-Labor Co. Ltd., Hungary. The milling characteristics of the new instrument were compared to other laboratory mills and the effects of milling action on the chemical composition of fractions were analysed. The fractions were tested with both chemical and near infrared spectroscopic methods. The micro-scale milling resulted significantly different yields, particle size distributions and different fractions from compositional point of view. The near infrared spectra were sensitive enough to distinguish the fractions obtained by different milling procedures. Quantitative NIR calibration equations were developed and tested in order to measure the chemical composition of characteristic milling fractions. Special qualification procedure the PQS (Polar Qualification System) method was used for detecting the differences between fractions obtained by macro and micro-milling procedures. The results and the limitations of PQS method in this application will be discussed.

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The measuring tool development of the stress and coping method of the Korean obese adolescents (한국 비만 청소년의 스트레스와 대처방법에 관한 측정도구 개발연구)

  • 김이순;김영혜
    • Korean Journal of Health Education and Promotion
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    • v.18 no.3
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    • pp.117-131
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    • 2001
  • This study was attempted to develope a highly reliable and valid tool which is useful to assess the Korean obese adolescents' stress and coping method. The data were collected from the total of 600 obese students from middle and high schools in Pusan. The author used a convenience sampling method. The data collection was done from March 2 to July 11, 1999. The analysis of the data was done with SPSS Win(10.0) for descriptive statistics and factor analysis. The preliminary tool was composed of 72 items(stress items: 34, coping method items: 38) with the five point Likert scale. Item analysis and inter consistency were calculated for reliability and validity through pre-test. The preliminary tool was analyzed for reliability and validity. Finally, the tool was of 65 items(stress items: 33, coping method items: 32). The results were as follows: 1. Cronbach Coefficient Alpha for the 33 items of stress was .9485 and the 32 items of coping method was .8534. 2. The factor analysis was done in order to confirm construction and the items were extracted Oblimin rotation and Maximum likelihood extraction method. 3. The factor analysis showed 6 factors in stress and 10 factors in coping method. These 6 factors of stress explained 62.4% and 10 factors of coping method explained 57.4%. 4. Six factor of stress lable were 〈outward appearance〉, 〈boyfriend/ girlfriend〉, 〈occur an outbreak of disease〉, 〈mutual relation of family〉, 〈an obese figure〉, 〈be a burden on exercise〉. 5. Ten factor of coping method lable were 〈be concerned about another affairs〉, 〈recreation activities〉, 〈self-violence〉, 〈relaxation〉, 〈hobby activities〉, 〈avoid a situation〉, 〈communication〉, 〈music〉, 〈negative behavior〉, 〈positive thinking〉. The results of using this scale in a study will contribute to design an appropriate school health management of obese students, and also it will contribute to the development of nursing research.

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Social Work Practitioner's Job Performance - a Multi-Level Analysis - (사회복지 종사자의 직무수행에 관한 다수준 연구)

  • Cho, Sung-Woo;Um, Myung-Yong
    • Korean Journal of Social Welfare
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    • v.61 no.4
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    • pp.137-161
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    • 2009
  • In an effort to identify predictors of job performance, research studies in social work administration has been so far on the individual practitioners' levels of knowledge and skills, which could be used in a workplace. As the theoretical concept of organizational environment was fully introduced into social work administration research, however, studies on practitioners' job performance began to have interest in the team or the organizational level variables as well as individual level variables. Along the course of this tendency, this study attempted to test the effect of individual, team, and organizational level variables on the job performance of human service workers. The individual level variables consisted of knowledge, skills, job satisfaction, personality, and counter-productive work behaviors of workers. The team or the organizational level variables included situational constraint, organizational justice, job characteristics, government-dependency, and inter-organizational cooperation. Multi-level complex survey data collected by cluster sampling method from 314 practitioners in 23 organizations were analyzed using Hierarchial Linear Model. Results showed that both task and contextual performance were affected by individual, team, and organizational level variables in various ways.

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Study for Validation of the Korean Childcare Teacher's Job Satisfaction Scale(K-CTJSS) (한국형 보육교사 직무만족척도(K-CTJSS)의 표준화를 위한 타당화 연구)

  • Cho, Song-Yon;Baik, Eun-Joo;Kim, Hye-Gum;Kwon, Yeon-Hee;Jung, Jee-Nha
    • Journal of Families and Better Life
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    • v.29 no.2
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    • pp.1-12
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    • 2011
  • The purpose of this study was to validate the standardization of the "Korean Childcare Teacher's Job Satisfaction Scale"(K-CTJSS) that the validity and reliability was evaluated by pretest in 2009. K-CTJSS is composed by 40 items with 6 factors and is responded by 6 point Likert scale. Participants consisted of 1,276 childcare teachers in Korea except Gangwon-do and Jeju-do by purposive sampling. Results were as follows: First, exploratory factor analysis resulted in 40 items composed of 6 factors (director's childcare center management system, social recognition, working environment and welfare, workload and time management, relationship with co-workers, relationship with parents). Second, the confirmatory factor analysis supported a 6 factor structure by resulting over appropriate level of goodness of fit. Third, inter-corelation coefficients among 6 factors were significant level(r = .10~.70). Fourth, the reli ability level of 6 factors by Cronbach's ${\alpha}$ were high(.84~.95.). Finally, concurrent validity levels with Childhood Job Satisfaction Survey(Jorde-Bloom, 1989) and the Satisfaction with Life Scale(Diener et al., 1985) were r = .07~.84 and .19~.46, respectively.

Test of the Korean Parent as a Teacher (KPAAT) Inventory - Focusing on the Parents of Preschoolers - (한국형 교사로서의 부모 양육태도 검사도구 검증 - 학령전기 아동의 부모를 대상으로 -)

  • Kim, Young Hee;Kim, Kae Sook;Kim, Shin-Jeong
    • Child Health Nursing Research
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    • v.15 no.3
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    • pp.314-324
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    • 2009
  • Purpose: This study was done to test the reliability and validity of the Korean parent as a teacher (KPAAT) inventory for a group of parents of preschoolers. Methods: For this methodological study with 187parents were recruited from October to December, 2004 using convenience sampling. Self-report questionnaires measured level of child-rearing attitude. Internal consistency reliability was assessed with Cronbach's alpha coefficients. Construct validity of KPAAT inventory was analyzed using item analyses and factor analysis. Statistical analysis was done using SPSS Program Version 14.0. Results: The Cronbach's alpha coefficient for the KPAAT inventory was 0.881. For item analyses, inter-item correlation coefficients were -0.029${\sim}$0.781. Corrected item-total correlation coefficients were 0.012-0.737. Item-to"subscale correlation coefficients ranged from 0.509 to 0.817. Subscale-to-total correlation coefficients were 0.965, 0.711, respectively. Orthogonal varimax rotation of the 85 items in 16 areas of the KPAAT inventory, showed two factors, positive parenting attitude and negative parenting attitude. These two factors explained 48.2% of the total variance. Conclusion: In the original KPAAT inventory six factors were identified through factor analysis, however, in this study only two factors were extracted. Whereas, internal consistency reliability was within an acceptable range, these results suggest additional studies are needed to improve the validity of the KPAAT inventory.

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Accuracy and Reliability of Ground Reaction Force System and Effect of Force Platform Mounting and Environment (지면반력장비의 정밀성, 신뢰도와 장비설치.사용 환경의 영향)

  • Park, Young-Hoon;Youm, Chang-Hong;Sun, Sheng;Seo, Kook-Woong;Kim, Eui-Hwan;Kim, Tae-Whan
    • Korean Journal of Applied Biomechanics
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    • v.17 no.1
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    • pp.1-8
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    • 2007
  • Ground reaction force (GRF) measures are one of the most commonly used in biomechanical study. GRF system is very useful educational tool to explain and demonstrate the Newton's law of universal gravitation and laws of motion as well. However, accuracy, intra- and inter- force platform measures' consistency, reliability, noise, and the effect of platform mounting to GRF measures were not clearly viewed. The aim of this study was to examine the above. GRFs of a plastic dummy and two subjects' quiet upright standing were collected at four university laboratories eight force platforms. The types of platforms, analysis programs, and platform set-up were various. Three 100s-trials were conducted with sampling frequency of 100 Hz. First two trials' vertical component of GRFs, Fz, and CoP sway ranges of mid-60s-portion of 100s trials were analyzed by the paired t-tests and one-way ANOVA. Six of eight platforms' 1st and 2nd trial dummy Fz were statistically different (p<.05) and all platforms ICC were poor (<.28). Fz of the two platforms in every four laboratories were statistically different (p<.05). There were white noises and/or very distinctive noises at specific frequency ranges in all Fz measures. 5 Hz low-pass filtering made clear the Fz differences. CoP ranges of dummy were less than 0.5 cm and the best was 0.02 cm. This CoP range finding agrees with previous results suggests the importance of force platform mounting and A/D card resolution.

Elemental Composition and Source Identification of PM2.5 in Jeju City (제주시 미세먼지(PM2.5)에 함유된 원소의 조성특성 및 오염원)

  • Lee, Ki-Ho;Hu, Chul-Goo
    • Journal of Environmental Science International
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    • v.27 no.7
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    • pp.543-554
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    • 2018
  • From November 2013 to December 2016, ambient fine particulate matter ($PM_{2.5}$) was sampled in the downtown area of Jeju City, South Korea, which has seen rapid urbanization. The atmospheric concentrations of elements were measured in the $PM_{2.5}$ samples. This study focused on Cd, Cr, Cu, Mn, Ni, Pb, As, Sb, Sn, V, and Zn. The concentrations of Al, Na, K, Fe, Ca, Mg, Sr, and La were also obtained for reference. The objectives of this study were to examine the contributions of these elements to $PM_{2.5}$ concentrations in downtown Jeju City, and to investigate the inter-element relationships and the elemental sources by using enrichment factors and principal components analysis (PCA). A composition analysis showed that the 19 elements constituted 6.65 % of the $PM_{2.5}$ mass, and Na, K, Al, Fe, Ca, Mg, and Zn constituted 98 % of the total ion mass. Seasonal trend analysis for the sampling period indicated that the concentrations of the elements increased from November to April. However, no substantial seasonal variations were found in the concentrations of the elements. The composition ratios of some elements (Cu/Zn, Cu/Cd, Cu/Pb, V/Ni, and V/La) were found to be out of range when compared to the literature from other urban areas. The ratios between the elements and the PCA results showed that local contaminant sources in Jeju City rarely influence the composition of $PM_{2.5}$. This suggests that the major sources of $PM_{2.5}$ in Jeju City may include long-range transport of fine particulate matter produced in other areas.

The Effect of Regulation on Recruitment Advertising for Clinical Trial Subjects in Korea (임상시험 대상자 모집 광고에 대한 정부의 규제 효과)

  • Kim, Hyun Jin;Sohn, Hyun Soon
    • Korean Journal of Clinical Pharmacy
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    • v.32 no.3
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    • pp.166-177
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    • 2022
  • Background: Recently clinical trials have expanded extensively in Korea; thus, ensuring the rights of subjects participating in clinical trials is imperative. Accordingly, national regulations on subject recruitment advertisement were enforced from October 25, 2018. In this study, the effect of this regulation was evaluated by analyzing the difference in the provision of information before and after enforcement of the regulation. Methods: Recruitment advertisements for clinical trial subjects 3 years before and after enforcement of the regulation were collated by the significance sampling approach. Print-based (newspapers, buses, and subways) and web-based (clinical trial center websites and online platforms) materials for recruitment in clinical trials of phase 1 to 4 for investigational drugs, medical devices, and oriental medicine were considered. Chi-square tests were conducted for inter-group comparisons. SPSS version 26 was employed for statistical analyses. Results: A total of 137 advertisements were collected comprising 60 pre- and 77 post-regulation enforcement. The overall rate of delivery of critical information in advertisements increased significantly from 47.5% before regulation to 93.2% after regulation enforcement. Particularly, details on expected adverse events augmented significantly (p<0.001). Benefits from participation in clinical trial reduced significantly from 88.3% to 70.1% (p<0.05). As the information provision amplified, the inclusion of professional terms increased. Conclusions: Enforcement of regulations has led to a surge in the amount of information and challenging terms contained in advertisements for recruiting subjects. Therefore, additional efforts are required by subjects to completely understand the information provided in the advertisements.

Spatio-Temporal Variation of Soil Respiration and Its Association with Environmental Factors in Bluepine Forest of Western Bhutan

  • Cheten Thinley;Baghat Suberi;Rekha Chhetri
    • Journal of Forest and Environmental Science
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    • v.39 no.1
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    • pp.13-19
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    • 2023
  • We investigated Soil respiration in Bluepine forest of western Bhutan, in relation to soil temperature, moisture content and soil pH and it was aimed at establishing variability in space and time. The Bluepine forest thrives in the typical shallow dry valleys in the inter-montane Bhutan Himalaya, which is formed by ascending wind from the valley bottom, which carries moisture from the river away to the mountain ridges. Stratified random sampling was applied and the study site was classified into top, mid, low slope and further randomized sample of n=20 from 30 m×30 m from each altitude. The overall soil respiration mean for the forest was found 2248.17 CO2 g yr-1 and it is ~613.58 C g yr-1. The RS from three sites showed a marginal variation amongst sites, lower slope (2,309 m) was 4.64 μ mol m-2 s-1, mid slope (2,631 m) was 6.78 μ mol m-2 s-1 and top slope (3,027 m) was 6.33 μ mol m-2 s-1 and mean of 5.92 μ mol m-2 s-1, SE=0.25 for the forest. Temporal distribution and variations were observed more pronounced than in the space variation. Soil respiration was found highest during March and lowest in September. Soil temperature had almost inverse trend against soil respiration and dropped a low in February and peak in July. The moisture in the soil changed across months with precipitation and pH remained almost consistent across the period. The soil respiration and soil temperature had significant relationship R2=-0.61, p=0.027 and other variables were found insignificant. Similar relationship are reported for dry season in a tropical forest soil respiration. Soil temperature was found to have most pronounced effect on the soil respiration of the forest under study.

Biological soil crusts impress vegetation patches and fertile islands over an arid pediment, Iran

  • Sepehr, Adel;Hosseini, Asma;Naseri, Kamal;Gholamhosseinian, Atoosa
    • Journal of Ecology and Environment
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    • v.46 no.1
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    • pp.31-40
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    • 2022
  • Background: Plant vegetation appears in heterogeneous and patchy forms in arid and semi-arid regions. In these regions, underneath the plant patches and the empty spaces between them are covered by biological soil crusts (moss, lichen, cyanobacteria, and fungi). Biological soil crusts lead to the formation and development of fertile islands in between vegetation patches via nitrogen and carbon fixation and the permeation of runoff water and nutrients in the soil. Results: The present study has investigated the association of biological soil crusts, the development of fertile islands, and the formation of plant patches in part of the Takht-e Soltan protected area, located in Khorasan Razavi Province, Iran. Three sites were randomly selected as the working units and differentiated based on their geomorphological characteristics to the alluvial fan, hillslope, and fluvial terrace landforms. Two-step systematic random sampling was conducted along a 100-meter transect using a 5 m2 plot at a 0-5 cm depth in three repetitions. Fifteen samplings were carried out at each site with a total of 45 samples taken. The results showed that the difference in altitude has a significant relationship with species diversity and decreases with decreasing altitude. Results have revealed that the moisture content of the site, with biocrust has had a considerable increase compared to the other sites, helping to form vegetation patterns and fertile islands. Conclusions: The findings indicated that biological crusts had impacted the allocation of soil parameters. They affect the formation of plant patches by increasing the soil's organic carbon, nitrogen, moisture and nutrient content provide a suitable space for plant growth by increasing the soil fertility in the inter-patch space.