• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 추계학술대회
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• pp.1172-1177
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• 2004

The evolution of incipient soot particles has been examined by high resolution electron microscopy (HRTEM) and elemental analyzer in ethylene-air inverse diffusion flames. Laser Induced Incandescence(LII) and laser scattering methods were introduced for examining the change of soot volume fraction and morphological properties in combustion generated soot qualitatively. Soot particles, collected by thermophoretic sampling were analyzed by using HRTEM to examine the nano structure of precursor particles. HRTEM micrographs apparently reveal a transformation of condensed phase of semitransparent tar-like material into precursor particles with relatively distinct boundary and crystalline which looks like regular layer structures. During this evolution histories C/H analysis was also performed to estimate the chemical evolution of precursor particles. The changes of C/H ratio of soot particles with respect to residence time can be divided into two parts: one is a very slowly increasing regime where tar-like materials are transformed into precursor particles (inception process) the other is an increasing region with constant rate where surface growth affects the increase of C/H ratio dominantly (surface growth region). These results provide a clear picture of a transition to mature soot from precursor materials.

• 한국연소학회지
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• 제9권2호
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• pp.38-44
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• 2004

The evolution of incipient soot particles has been examined by high resolution electron microscopy (HRTEM) and elemental analyzer in ethylene-air inverse diffusion flames. Laser Induced Incandescence(LII) and laser scattering methods were introduced for examining the soot volume fraction and morphological properties in combustion generated soot qualitatively. Soot particles, collected by thermophoretic sampling, were analyzed by using HRTEM to examine the nano structure of precursor particles. HRTEM micrographs apparently reveal a transformation of condensed phase of semitransparent tar-like material into precursor particles with relatively distinct boundary and crystalline which looks like regular layer structures. During this evolution histories, C/H analysis was also performed to estimate the chemical evolution of precursor particles. The changes of C/H ratio of soot particles with respect to residence time can be divided into two parts: one is a very slowly increasing regime where tar-like materials are transformed into precursor particles (inception process) the other is an increasing region with constant rate where surface growth affects the increase of C/H ratio dominantly (surface growth process). These results provide a clear picture of a transition to mature soot from precursor materials.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1993년도 제18회 학술대회 초록집
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• pp.77-84
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• 1993

Systems with journal bearings generally operate in large scale and under severe loading conditions such as steam generator turbines and internal combustion engines, in contrast to the machineries using rolling element bearings. Failure of the bearings in these machineries can result in the system breakdown. To avoid the time consuming repair and considerable economic loss, the detection of incipient failure in journal bearings becomes very important. In this experimental approach, acoustic emission monitoring is employed to the detection of incipient failure caused by intervention of foreign particles most probable in the journal bearing systems. It has been known that the intervention of foreign materials, insufficient lubrication and misassembly etc. are principal factors to cause bearing failure and distress. The experiment was conducted under such designed conditions as inserting alumina particles to the lubrication layer in the simulated journal bearing system. The results showed that acoustic emission could be an effective tool to detect the incipient failure in journal bearings.

• 한국가시화정보학회지
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• 제2권1호
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• pp.12-17
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• 2004

The physical characteristics of soot near the soot inception point were investigated with various measurements. In-situ measurements of particle size and volume fraction were introduced based on time resolved laser-induced incandescence (TIRE-LII) and laser-induced ion mobility (LIIM). The one has more convenience and accuracy than conventional LII technique and the other works best for particle sizes of a few nanometers at high concentrations in a uniform concentration field. A complementary ex-situ measurement of particle size is nano differential mobility analyzer (Nano-DMA), which recently developed for measuring particle sizes between 2nm and 100nm and provides high-resolution size information for early soot. Particles will be also collected on transmission electron microscope (TEM) grids using rapid thermophoretic sampling and analyzed for morphology. These measurements will allow fresh and original insight into the characterizing soot inception process. The measured physical properties of incipient soot will clarify the controlling growth mechanism combined with chemical ones, and the dominant mechanism for soot modeling can be deduced from the information.

• Geomechanics and Engineering
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• 제13권6호
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• pp.947-961
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• 2017

An innovative spiral variable-section capillary model is established for piping critical hydraulic gradient of cohesion-less soils causing water/mud inrush in tunnels. The relationship between the actual winding seepage channel and grain-size distribution, porosity, and permeability is established in the model. Soils are classified into coarse particles and fine particles according to the grain-size distribution. The piping critical hydraulic gradient is obtained by analyzing starting modes of fine particles and solving corresponding moment equilibrium equations. Gravities, drag forces, uplift forces and frictions are analyzed in moment equilibrium equations. The influence of drag force and uplift force on incipient motion is generally expounded based on the mechanical analysis. Two cases are studied with the innovative capillary model. The critical hydraulic gradient of each kind of sandy gravels with a bimodal grain-size-distribution is obtained in case one, and results have a good agreement with previous experimental observations. The relationships between the content of fine particles and the critical hydraulic gradient of seepage failure are analyzed in case two, and the changing tendency of the critical hydraulic gradient is accordant with results of experiments.

• 한국치위생학회지
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• 제17권5호
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• pp.817-826
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• 2017

Objectives: The aim of this study was to investigate the effects of bamboo salts on remineralization effects on subsurface of artificial carious enamel. Methods: Incipient carious enamel was formed in permanent bovine incisors and then specimens were divided into three groups randomly: 3% bamboo salt (BS), 2% (NaF) and the solution of mixed 3% BS and 2% NaF. For remineralization, specimens of each of the three groups were treated for 24 hrs at $37^{\circ}C$ incubator. After treatment, specimens were analyzed using SEM and VHN. Statistical analysis used was one-way ANOVA. Results: In SEM observation, the BS group showed narrower distances between enamel rods than the cases of incipient subsurface caries enamel. The NaF and BS+NaF groups showed that the enamel rods near the surface were destructed, and innumerable round small particles were deposited near the surface of enamel. The BS+NaF group showed more minerals attachment between enamel rods than the cases of other groups. The differences in subsurface microhardness (${\Delta}VHN$) increased all of three groups in total by $80{\mu}m$. The ${\Delta}VHN$ of the BS+NaF group increased significantly more than NaF and BS groups in depth of $50{\mu}m$, $80{\mu}m$. Conclusions: The 3% bamboo salt with 2% NaF solution was found to increase subsurface hardness of incipient caries enamel. Thus, bamboo salt will be used to contribute to prevention on dental caries.

• 한국수자원학회:학술대회논문집
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• 한국수자원학회 2018년도 학술발표회
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• pp.149-149
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• 2018

Prediction on initial motion of sediment is crucial to evaluate sediment transport and channel stability. The condition of incipient movement of sediment is characterized by bed shear stress, which is generated from force of moving water against the bed of the channel, and by critical shear stress, which depends on force resisting motion of sediment due to the submerged weight of the grains. When the bed shear stress exceeds the critical shear stress, sediment particles begin rolling and sliding at isolated and random locations. In Mountain River, debris flow frequently occurs due to heavy rainfall and can lead some natural stones from mountain slope into the bed river. This phenomenon could add additional forces to sediment transport system in the bed of river and also affect or change direction and magnitude of sediment movement. In this paper, evaluations on incipient motion of uniform coarse gravel under falling spheres impacts using small scale flume channel were conducted. The drag force of falling spheres due to water flow and length movement of falling spheres were investigated. The experiments were carried out in flume channel made by glass wall and steel floor with 12 m long, 0.6 m wide, and 0.6 m deep. The bed slopes were selected with the range from 0.7% to 1.5%. The thickness of granular layer was at least 3 times of diameter of granular particle to meet grain placement condition. The sphere diameters were chosen to be 4cm, 6 cm, 8 cm, 10 cm. The spheres were fallen in to the bed channel for critical condition and under critical condition of motion particle. Based on the experimental results, the Shields curve of particles Reynold number and dimensionless critical shear stress were plotted. The relationship between with drag force and the length movement of spheres were plotted. The pathways of the bed material Under the impact of spheres falling were analyzed.

• 비파괴검사학회지
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• 제14권1호
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• pp.16-22
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• 1994

일반적으로 구름 베어링 시스템에 비해 발전용 터어빈이나 내연기관 엔진과 같은 저어널 베어링을 가진 시스템은 상대적으로 대형 설비이거나 더 가혹한 운전조건에서 가동되는 경우가 많다. 이런 회전기계류에서의 베어링의 파손은 설비의 운전 중단 및 관련 설비의 파손까지도 초래할 수 있게 된다. 따라서 이로 인한 보수에 소비되는 시간 및 경제적인 손실등을 피하기 위해서는 저어널 베어링의 조기파손 감지의,역할은 매우 중요하게 된다. 본 연구에서는 음향방출 기술을 이용하여 베어링에서 발생할 수 있는 파손의 조기검출을 위해 실험실용으로 직접 제작한 저어널 베어링 시스템을 이용하여 여러 형태의 비정상 조건을 만들어 가며 실험을 행하였다. 베어링 손상 및 피로의 주 요인으로서는 윤활유 부족, 윤활층에의 이물질의 혼입, 조립 불량 등이 대표적인 원인으로서 알려져 있으며 이에 근거하여 실험 조건을 윤활유에의 이물질 혼입, 윤활유 부족, 그리고 축과 베어링간의 금속간 접촉등의 인위적인 형태로 구성하여 실험하였다. 그 결과로서 음향방출 기술이 저어널 베어링의 조기파손 감지에 매우 효과적인 도구라는 것을 입증하였다.

• 대한화학회지
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• 제6권1호
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• pp.54-60
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• 1962

The water gas shift conversion catalyst prepared by the American Cyanamide Co. was subjected to fluidization in a 2-in. Pyrex glass tube to obtain the basic fluidization characteristic data. The size of the catalyst charged ranged from 70 to 120 meshes and it was supported on a single layer 300-mesh wire gauze through which the fluidizing medium, the air, was passed. Following are some data and facts found by the authors: (1) The catalyst particles were porous, and their surfaces were trough and irregular. (2) The average effective particle density and the average shape factor of these particles were 152.2 lb/$ft^3$ and 0.865 respectively. (3) As the particle diameter of the catalyst increased, the minimum fluid voidage of the bed decreased slightly. (4) Just before the incipient fluidization, pressure drop suddenly fell and the bed expanded simultaneously. (5) After fluidization set in, the expansion characteristics of the catalyst bed were similar to those of sand and glass beads except intense bubbling in the catalyst bed.

• Korea-Australia Rheology Journal
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• 제20권3호
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• pp.165-173
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• 2008

Multiple particle tracking microrheology is used to characterize the viscoelastic properties of biomaterial and synthetic polymer gels near the liquid-solid transition. Probe particles are dispersed in the gel precursors, and their dynamics are measured as a function of the extent of reaction during gel formation. We interpret the dynamics using the generalized Stokes-Einstein relationship (GSER), using a form of the GSER that emphasizes the relationship between the probe particle mean-squared displacement and the material creep compliance. We show that long-standing concepts in gel bulk rheology are applicable to microrheological data, including time-cure superposition to identify the gel point and critical scaling exponents, and the power-law behavior of incipient network's viscoelastic response. These experiments provide valuable insight into the rheology, structure, and kinetics of gelling materials, and are especially powerful for studying the weak incipient networks of dilute gelators, as well as scarce materials, due to the small sample size requirements and rapid data acquisition.