• Title/Summary/Keyword: impregnation method

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Nondestructive Bending Strength Evaluation of Woodceramics Made from Woody Part of Broussonetia Kazinoki Sieb. - Effect of Resin Impregnation Ratio -

  • Byeon, Hee-Seop;Kim, Jae-Min;Won, Kyung-Rok;Oh, Seung-Won
    • Journal of the Korean Wood Science and Technology
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    • v.39 no.5
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    • pp.398-405
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    • 2011
  • Nondestructive evaluation (NDE) technique method using a resonance frequency mode was carried out for woodceramics made by different phenol resin impregnation ratios (40, 50, 60, 70%) for Broussonetia Kazinoki Sieb. Dynamic modulus of elasticity increased with increasing resin impregnation ratios. There was a close relationship between dynamic modulus of elasticity and static bending modulus of elasticity and between dynamic modulus of elasticity and MOR and between static bending modulus of elasticity and MOR. Therefore, the dynamic modulus of elasticity using resonance frequency mode is useful as a nondestructive evaluation method for predicting the MOR of woodceramics made by different impregnation ratios.

DISCHARGE CHARACTERISTICS OF NICKELOXIDE ELECTRODE PREPARED FROM ELECTROCHEMICAL IMPREGNATION

  • Takenoya, K.;Sasaki, Y.;Yamashita, T.
    • Journal of Surface Science and Engineering
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    • v.32 no.3
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    • pp.363-365
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    • 1999
  • The improved method comprises electrochemically deposition of nickel hydroxide into the sintered nickel plaque cathode from nickel aqueous electrolyte at acid pH in a treating zone containing an anode. The electrochemical impregnation was examined under various conditions. Deposition condition of fine active material was obtained from the impregnation of a high temperature and also high current density. This method also could be decreased swelling and buckling of the plaque. A nickel electrode prepared by electrochemical impregnation is useful as the positive in nickel-cadmium cells. The utilization of the active material indicated almost 100% based on a one electron charge.

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Pd-doped $SnO_2$-based oxide semiconductor thick-film gas sensors prepared by three different catalyst-addition processes

  • Lee, Kyu-Chung;Hur, Chang-Wu
    • Journal of information and communication convergence engineering
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    • v.7 no.1
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    • pp.72-77
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    • 2009
  • Three different procedures for adding Pd compounds to $SnO_2$ particles have been investigated. These processes are: (1) coprecipitation; (2) dried powder impregnation; and (3) calcined powder impregnation. The microstructures of $SnO_2$ particles have been analyzed by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). In the coprecipitaion method, the process does not restrain the growth of $SnO_2$ particles and it forms huge agglomerates. In the dried powder impregnation method, the process restrains the growth of $SnO_2$ particles and the surfaces of the agglomerates have many minute pores. In the calcined powder impregnation method, the process restrains the growth of $SnO_2$ particles further and the agglomerates have a lot more minute pores. The sensitivity ($S=R_{air}/R_{gas}$) of the $SnO_2$ gas sensor made by the calcined powder impregnation process shows the highest value (S = 21.5 at 5350 ppm of $C_3H_8$) and the sensor also indicates the lowest operating temperature of around $410^{\circ}C$. It is believed that the best result is caused by the plenty of minute pores at the surface of the microstructure and by the catalyst Pd that is dispersed at the surface rather than the inside of the agglomerate. Schematic models of Pd distribution in and on the three different $SnO_2$ particles are presented.

Preparation and Properties of Disc Type CuO Catalyst Impregnated Ceramic Filters (디스크형 산화구리 촉매담지 세라믹필터의 제조와 물성)

  • Hong Min-Sun;Moon Su-Ho;Lee Jae-Chun;Lee Dong-Sub;Lim Woo Taik
    • Journal of Korean Society for Atmospheric Environment
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    • v.20 no.2
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    • pp.185-193
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    • 2004
  • A catalyst with CuO ceramic filter for simultaneous treatment of dust and HAP was prepared and characterized. Catalytic ceramic filter can not only potentially achieve the substantial savings in energy but provide with effective optimization and integration of process for simultaneous removal of SO$_2$, NO$_{x}$ and particulates from flue gases. Catalytic ceramic filters remove simultaneously particulates on exterior surface of filters and reduce NO to $N_2$ and $H_2O$ by SCR (Selective Catalytic Reduction) process. Preparation of catalyst impregnated ceramic filter with disk shape (Ψ 50) follow the processing of alumino-silicate ceramic filter, support impregnation and catalyst impregnation (copper oxide). Preparation routes of alumino-silicate catalyst carrier suitable for production of catalytic filters practically were studied and developed using the sol-gel and colloidal processing, homogeneous precipitation and impregnation method. Characterization of the catalyst, catalyst carrier catalytic filter materials have been performed the using various techniques such as BET, XRD, TGA, SEM. Combination of the sol-gel and colloidal processing and impregnation method is recommended to prepare catalyst carriers economically for catalytic filter applications.s.

Effect of Phenol Formaldehyde Impregnation on The Physical and Mechanical Properties of Soft-Inner Part of Oil Palm Trunk

  • Hartono, Rudi;Hidayat, Wahyu;Wahyudi, Imam;Febrianto, Fauzi;Dwianto, Wahyu;Jang, Jae-Hyuk;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.6
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    • pp.842-851
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    • 2016
  • The objective of this study was to improve physical and mechanical properties of soft-inner part of oil palm trunk (S-OPT) after impregnation with phenol formaldehyde (PF) resin and densification by close system compression (CSC) method. Effect of different methods of PF resin impregnation (i.e., no vacuum-pressure, vacuum, and vacuum-pressure) was evaluated. The results showed that PF resin impregnation and CSC significantly improved the physical and mechanical properties of S-OPT up to: (1) 176% in density; (2) 309% in modulus of rupture (MOR); (3) 287% modulus of elasticity (MOE); and (4) 191% in the compressive strength. Physical and mechanical properties of S-OPT showed their best performances when PF resin impregnated with vacuum-pressure method as shown by higher weight gain, density, MOR, MOE, compressive strength, and lower recovery of set due to better penetration of PF resin into S-OPT. Combining PF resin impregnation and densification by CSC method could be a good method to improve physical and mechanical properties of S-OPT.

A Study on the Plant Nutrients Impregnation Methods and Soil Covering Effects of Wood Chips (목재칩의 식물영양제 함침방법과 토양 피복효과에 관한 연구)

  • Yu Jin Hong;Dae Woo Choi;Kwon Woong Choi;Suejin Park;Seok Un Jo;Hee Jun Park
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.46 no.spc
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    • pp.31-38
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    • 2023
  • In this study, in order to develop a method to efficiently inject essential nutrients necessary for plant growth into wood chips, which are simply used as soil covering materials in the agriculture, landscaping and horticultural industries, the atmospheric pressure dipping method and the vacuum pressure impregnating method are used to improve the plant nutrients injectability and impregnation amount were comparatively analyzed. Nutrient ingredients and 8 major heavy metal contents of wood chips injected with nutrients were analyzed, and soil covering effects were examined by covering wood chips injected with nutrients on soil. Comparing the dipping method and the vacuum pressure impregnation method, it took about 48 hours or more to inject 1,500 g or more of the nutrient aqueous solution into 1 kg of wood chips in the dipping method, but the vacuum pressure impregnation method could be impregnated in about 5 minutes. Components of the impregnated nutrients were detected in proportion to the diluted concentration. As a result of covering the wood chips developed in this study on soil, they showed weakly acidic pH, and the heat insulation and moisturizing effects during the winter season were evaluated to be superior to those of uncovered soil. In the future, wood chips impregnated with nutrients are expected to contribute to the more efficient use of waste wood resources and the long-term supply of nutrients essential for plant growth, reducing excessive use of chemical fertilizers and reducing costs.

Ultrastructural Study of Drosophila Ocellar Visual System by Osmium Impregnation (오스뮴침착법에 의한 초파리 단안시각계의 미세구조)

  • Yoon, Chun-Sik
    • Applied Microscopy
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    • v.29 no.4
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    • pp.451-457
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    • 1999
  • Ultrastructure of adult Drosophila ocellus was compared with conventional electron microscopic method and osmium impregnation. When osmium impregnation was applied, some organelles of cells were strongly stained. Especially, subrhabdomeric cisternae (SRC) were strongly stained and showed network-iike structure as in compound eye. Other organelles including SSC, ER, nuclear envelope, pigment granules and mitochondria were also strongly stained. These organelles are known as a general calcium ion reservoir. In conclusion, the strong effect of light and shade by osmium impregnation was regarded as a result of strong binding between calcium ion and osmium tetroxide. Thus, we agree to the opinion that osmium impregnation is very useful methods to the comparative morphology of cell organelles.

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Conservation of Waterlogged Wooden Finds Excavated in Wet-Site (저습지 출토 목재유물의 보존과 현황)

  • Yi, Yong Hee
    • Journal of Conservation Science
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    • v.6 no.2 s.8
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    • pp.126-140
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    • 1997
  • There were some cases in the past that waterlogged wooden finds were neglected and damaged severely because adequate methods of conservation processing could not be found. However, since a wooden ship unearthed in Anapji of Kyongju was processed by poly(ethylene glycol) (PEG) impregnation method in 1975, most of waterlogged wooden finds have been processed by diverse scientific methods. Most commonly-used conservation processing methods of waterlogged wooden finds in Korea are PEG impregnation method, alcohol-ether-resin method and vacuum freeze-drying method. New methods developed recently in Europe and Japan such as sucrose method, sugar-alcohol method and higher alcohol method are also being studied here. The most important task in conservation processing of waterlogged wood is to find good impregnation materials suitable to Korean climate and environments and develop their application methods. For efficient conservation processing, it is important to know the natures of finds and impregnation materials and relation between impregnation and drying condition. To achieve it, many experiments and studies are needed.

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Variation of main components according to the number of steaming and drying of Rehmanniae radix preparata

  • Youn, Ui Joung;Gu, Bon-Seok;Kim, Kyung Hee;Ha, Chulgyu;Jung, In Chan
    • Journal of Pharmacopuncture
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    • v.21 no.2
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    • pp.112-119
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    • 2018
  • Contents of compounds in Rehmanniae Radix change depending on the number of steaming and drying and the drying method. In this study, as an impregnation method for dried Rehmanniae Radix, takju impregnation and cheongju impregnation were carried out and steaming and drying were repeated for 9 times. The changes of 5-HMF and catalpol contents were analyzed according to the number of repetition times to investigate which stage of steaming and drying is preferable. Also, total nitrogen, crude fat, ash, and crude fiber were measured to analyze changes in general components. 5-HMF was not detected in dried Rehmanniae Radix. As a result of repetitive steaming and drying, the content of 5-HMF increased only slightly from 1 to 4-times steaming and drying but increased significantly from 5-times. The catalpol in dried Rehmanniae Radix was not detected after 5 times of steaming and drying. Sucrose, maltose, and glucose were included in dried Rehmanniae Radix before steaming and drying. However, after the process in both Takju impregnation and Cheongju impregnation, galactose and fructose tended to decrease after production and sucrose and glucose tended to decrease after the increase. In this study condition, 6-times and more steaming and drying were appropriate process which met the content criteria (not less than 0.1%) of the Korean Pharmacopoeia (8th edition) for 5-HMF, an index component for quality control of Rehmanniae Radix Preparata.

Development of Strengthening Method Using the Vacuum Impregnation in RC Members (진공함침을 이용한 철근콘크리트 부재에서의 보강공법 개발)

  • Yi, Seong Tae;Song, Yeong Sun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.5
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    • pp.11-18
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    • 2012
  • Deterioration and weakening is advanced in compliance with flowing of time and the change of environment in RC structures. Consequently, strength and serviceability decreases, finally, the life of infrastructure shortens and safety characteristics decreases. Accordingly, in this study, a new method to develop a strengthening method using the vacuum impregnation, which increases durability of the infrastructure occurred the safety reduction due to the performance degradation and increases the life of infrastructure by improving the durability compared to the existing method, was planned. For flexural tests, the maximum strength was a low-end order from high order as follows: (1) vacuum impregnation with 2 fold reinforcement, (2) fiber sheet 2 fold reinforcement, (3) vacuum impregnation with 1 fold reinforcement, (4) fiber sheet 1 fold reinforcement, and (5) nothing. Also, for confirmation results about durability, when the fiber reinforcement is being exposed to the inferior environment, the remaining tensile strength exceeded of 90% or more for all environments. This is because the reinforcement used in this research shows the excellent resistance in severe environment.