• Title/Summary/Keyword: hole formation

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Film Properties of MOCVD TiN prepared by TDMAT and TDMAT/$NH_3$ (TDMAT와 TDMAT/$NH_3$ 로 형성한 MOCVD(Metal Organic Chemical Vapor Deposition) Titanium Nitride 박막의 특성)

  • Baek, Su-Hyeon;Kim, Jang-Su;Park, Sang-Uk;Won, Seok-Jun;Jang, Yeong-Hak;O, Jae-Eung;Lee, Hyeon-Deok;Lee, Sang-In;Choe, Jin-Seok
    • Korean Journal of Materials Research
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    • v.5 no.7
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    • pp.775-780
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    • 1995
  • Thin films of titanium nitride are formed using the tetrakis-dimethyl-amino-titanium (TDMAT(Ti[N($CH_3$)$_2$]$_4$)) under various conditions. The formation of TiN films has been obtained from the thermal decomposition of the Ti-precursor and the gas phase reaction between TDMAT and ammonia(NH$_3$). The resistivity of the MOCVD film can be attributed to their impurity. Especially the curve fitting graph of XPS data is revealed that main impurities in the films as carbon and oxygen make various interstitial compounds which has influenced physical and electrical properties of the film. In the contact hole with the aspect ratio of 3:1 and the diameter of 0.5${\mu}{\textrm}{m}$, the SEM morphology shows that the step coverage is more decreased in the films formed y flowing ammonia additionally than the films formed by pyrolysis of TDMAT and the phenomenon is probably related with the activation energy.

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A study on slim-hole density logging based on numerical simulation (소구경 시추공에서의 밀도검층 수치모델링 연구)

  • Ku, Bonjin;Nam, Myung Jin;Hwang, Seho
    • Geophysics and Geophysical Exploration
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    • v.15 no.4
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    • pp.227-234
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    • 2012
  • In this study, we make simulation of density log using a Monte Carlo N-Particle (MCNP) algorithm to make an analysis on density logging under different borehole environments, since density logging is affected by various borehole conditions like borehole size, density of borehole fluid, thickness and type of casing, and so on. MCNP algorithm has been widely used for simulation of problems of nuclear particle transportation. In the simulation, we consider the specific configuration of a tool (Robertson Geologging Co. Ltd) that Korea institute of geoscience and mineral resources (KIGAM) has used. In order to measure accurate bulk density of a formation, it is essential to make a calibration and correction chart for the tool under considerations. Through numerical simulation, this study makes calibration plot of the density tool in material with several known bulk densities and with boreholes of several different diameters. In order to make correction charts for the density logging, we simulate and analyze measurements of density logging under different borehole conditions by considering borehole size, density of borehole fluid, and presence of casing.

Influence of Polarization Behaviors on the ECM Characteristics of SnPb Solder Alloys in PCB (PCB에서의 ECM 특성에 미치는 SnPb 솔더 합금의 분극거동의 영향)

  • Lee Shin-Bok;Yoo Young-Ran;Jung Ja-Young;Park Young-Bae;Kim Young-Sik;Joo Young-Chang
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.2 s.35
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    • pp.167-174
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    • 2005
  • Smaller size and higher integration of electronic components make smaller gap between metal conducting layers in electronic package. Under harsh environmental conditions (high temperature/humidity), electronic component respond to applied voltages by electrochemically ionization of metal and metal filament formation, which lead to short failure and this phenomenon is termed electrochemical migration(ECM). In this work, printed circuit board(PCB) is used for determination of ECM characteristics. Copper leads of PCB are soldered by eutectic solder alloys. Insulation breakdown time is measured at $85^{\circ}C,\;85{\%}RH$. CAF is the main mechanism of ECM at PCB. Pb is more susceptible to CAF rather than Sn, which corresponds well to the corrosion resistance of solder materials in aqueous environment. Polarization tests in chloride or chloride-free solutions fur pure metal and eutectic solder alloys are performed to understand ECM characteristics. Lifetime results show well defined log-normal distribution which resulted in biased voltage factor(n=2) by voltage scaling. Details on migration mechanism and lifetime statistics will be presented and discussed.

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In-situ Observations of Gas Phase Dynamics During Graphene Growth Using Solid-State Carbon Sources

  • Kwon, Tae-Yang;Kwak, Jinsung;Chu, Jae Hwan;Choi, Jae-Kyung;Lee, Mi-Sun;Kim, Sung Youb;Shin, Hyung-Joon;Park, Kibog;Park, Jang-Ung;Kwon, Soon-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.131-131
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    • 2013
  • A single-layer graphene has been uniformly grown on a Cu surface at elevated temperatures by thermally processing a poly(methyl methacrylate) (PMMA) film in a rapid thermal annealing (RTA) system under vacuum. The detailed chemistry of the transition from solid-state carbon to graphene on the catalytic Cu surface was investigated by performing in-situ residual gas analysis while PMMA/Cu-foil samples being heated, in conjunction with interrupted growth studies to reconstruct ex-situ the heating process. The data clearly show that the formation of graphene occurs with hydrocarbon molecules vaporized from PMMA, such as methane and/or methyl radicals, as precursors rather than by the direct graphitization of solid-state carbon. We also found that the temperature for vaporizing hydrocarbon molecules from PMMA and the length of time the gaseous hydrocarbon atmosphere is maintained, which are dependent on both the heating temperature profile and the amount of a solid carbon feedstock are the dominant factors to determine the crystalline quality of the resulting graphene film. Under optimal growth conditions, the PMMA-derived graphene was found to have a carrier (hole) mobility as high as ~2,700 cm2V-1s-1 at room temperature, superior to common graphene converted from solid carbon.

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Formation of Si Nanodot by Using SiNx Thin Films (SiNx 박막을 이용한 Si Nanodot의 형성)

  • Lee, Jang Woo;Park, Ik Hyun;Shin, Byul;Chung, Chee Won
    • Applied Chemistry for Engineering
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    • v.16 no.6
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    • pp.768-771
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    • 2005
  • The deposition of silicon nitride ($SiN_x$) thin films was carried out on $SiO_2/Si$ substrate at room temperature by reactive dc magnetron sputtering. The analysis of deposited $SiN_x$ films using x-ray photoelectron spectroscopy indicated that the composition of $SiN_x$ films was Si-rich. The deposited $SiN_x$ thin films were annealed by varying annealing temperature and time. X-ray diffraction (XRD) analysis was performed in order to examine the crystallization of Si in $SiN_x$ thin films. The optical and electrical properties of $SiN_x$ thin films were measured for the observation of Si nanodot. As a result, we observed the XRD peaks that might be the Si crystals. As the annealing time and annealing temperature increased, the photoluminescence intensity of $SiN_x$ films gradually increased. The capacitance-voltage characteristics of $SiN_x$ film measured before and after annealing indicated that the trap effect of electrons or holes occurred due to the existence Si nanodots in the $SiN_x$ thin films.

Development and Lab-scale Plant Study of Coagulation Sedimentation Module using Cyclone (선회류를 이용한 응집침전모듈의 개발 및 실증 연구)

  • Moon, Jinyoung;Cho, Young-Gun;Song, Seung-Jun;Kim, Jin-Han
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.5
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    • pp.3336-3344
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    • 2014
  • The purpose of this study is small scale coagulation module is developed and demonstrated through a lab-scale test. Recent as a sewage treatment rate increases, have heightened the interest in the necessity on the nonpoint source and developing a small processing unit has been increased. Coagulation sedimentation module in this study is additional growth of floc through swirling in the outside zone, reduction of microstructure floc number and the internal settling zone through vertical/level flow complex sedimentation method after the coagulation process precipitation method as an effective high separation efficiency can be divided was also assessed. Coagulation sedimentation module can increase the load factor was 4.4 times compared to conventional clarifier base on the same volume and surface area through vertical/level flow. In this study, this process was selected formation and maintenance of swirling and uniform flow distribution in the internal settling zone as an important design factor, to derive its FLUENT was used to characteristics of the flow model. Through the simulation of swirling, influent velocity, dimensions of external basin, hopper depth of bottom cone was determined and through analysis of velocity distribution, flow distribution detailed specifications are derived like as diameter and number of effluent hole. Lab-scale($120{\ell}/hr$) test results, influent of 300~800 NTU to less than 10 NTU without polymer feeding was able to operate in the 20minutes retention time(surface loading rate $37.3m^3/m^2$-day), and through analysis FLUENT the possibility of using design parameters were derived.

A Suture Bridge Transosseous-Equivalent Technique for Bankart Lesions with Deficient Bony Stability - Technical Note - (골안정성 결손을 가진 Bankart 병변에 대한 경 골-유사 교량형 봉합술식 - 술기 보고 -)

  • Choi, Chang-Hyuk;Kim, Shin-Kun;Chang, Il-Woong;Chae, Sung-Bum
    • Journal of the Korean Arthroscopy Society
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    • v.13 no.2
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    • pp.179-182
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    • 2009
  • Purpose: Point fixation at the margin of the glenoid is a limitation of conventional arthroscopic stabilization using suture anchors, and does not afford sufficient footprint healing, especially in glenoid bone deficiency. So, we introduce an arthroscopic suture bridge transosseous-equivalent technique for bony Bankart lesions to avoid the technical disadvantage of point contact with anchor fixation and to improve mechanical stability through cross compression of the labrum. Surgical approach: The technique was adapted from the transosseous-equivalent rotator cuff repair technique using suture bridges, which improved the pressurized contact area and mean pressure between the tendon and footprint. After preparation of the glenoid bed by removal, reshaping, or mobilization of the bony lesion, two anchors (3.0 mm Biofastak, $Arthrex^{(R)}$, Naples, FL) were inserted into the superior and inferior portion of the bony Bankart lesion. Using a suture hook, medial mattress sutures were applied around the capsulolabral portion of the IGHL complex to obtain sufficient depth of glenoid coverage. A 3.5 mm pushloc anchor ($Arthrex^{(R)}$, Naples, FL) hole was made in the articular edge of the anterior glenoid rim. distal, suture bridge was applied, and proximal was inserted to mobilize the labrum in the proximal direction. This avoided the technical disadvantage of point contact with anchor fixation and decreased the level of gap formation through cross-compression of the labrum.

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Topographical Analysis of the Potholes in Jakgwaecheon Stream in Ulsan (울산 작괘천의 포트홀에 관한 지형분석)

  • Kim, Tae-hyeong;Kong, Dal-yong;Lim, Jong-deock;Jung, Seung-ho;Yu, Yeong-wan
    • Korean Journal of Heritage: History & Science
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    • v.46 no.3
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    • pp.68-77
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    • 2013
  • This report is based on the investigation of potholes which are formed by fluvial erosion. A pothole is called so because it is a hole that looks like a coffeepot. The results of previous studies are applied to the 'Jakgwaecheon Porthole' of this study. The study is focused on the dimension and morphology of the Pothole and investigates the effects of stream sediments, river flow, geological structural lines, etc. on the formation of potholes. As a result of measuring 61 potholes in this area, we recognized that the elliptical dish-shaped cross sections are dominant and inferred that their longitudinal direction on the plain is affected by the direction of the stream flow. Also, 'Jakgwaecheon Pothole' is very characterized in terms of scale and morphology. Furthermore, it is harmonious with the beautiful landscape, humanity, and historical values and it can be suggested that it is qualified to be registered as a geoheritage structure.

An Experimental Study on the Biomechanical Effectiveness of Bone Cement-Augmented Pedicle Screw Fixation with Various Types of Fenestrations

  • Yoon, Sang Hoon;Lee, Sang Hyung;Jahng, Tae-Ahn
    • Journal of Korean Neurosurgical Society
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    • v.65 no.6
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    • pp.779-789
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    • 2022
  • Objective : To analyze the effects of the number and shape of fenestrations on the mechanical strength of pedicle screws and the effects of bone cement augmentation (BCA) on the pull-out strength (POS) of screws used in conventional BCA. Methods : For the control group, a conventional screw was defined as C1, a screw with cannulated end-holes was defined as C2, a C2 screw with six pinholes was defined as C3, and the control group type was set. Among the experimental screws, T1 was designed using symmetrically placed thru-hole type fenestrations with an elliptical shape, while T2 was designed with half-moon (HM)-shaped asymmetrical fenestrations. T3 and T4 were designed with single HM-shaped fenestrations covering three pitches and five pitches, respectively. T5 and T6 were designed with 0.6-mm and 1-mm wider fenestrations than T3. BCA was performed by injecting 3 mL of commercial bone cement in the screw, and mechanical strength and POS tests were performed according to ASTM F1717 and ASTM F543 standards. Synthetic bone (model #1522-505) made of polyurethane foam was used as a model of osteoporotic bone, and radiographic examinations were performed using computed tomography and fluoroscopy. Results : In the fatigue test, at 75% ultimate load, fractures occurred 7781 and 9189 times; at 50%, they occurred 36122 and 82067 times; and at 25%, no fractures occurred. The mean ultimate load for each screw type was 219.1±52.39 N for T1, 234.74±15.9 N for T2, 220.70±59.23 N for T3, 216.45±32.4 N for T4, 181.55±54.78 N for T5, and 216.47±29.25 N for T6. In comparison with C1, T1, T2, T3, T4, and T6 showed significantly different ultimate load values (p<0.05). However, when the values for C2 and the fenestrated screws were evaluated with an unpaired t test, the ultimate load value of C2 significantly differed only from that of T2 (p=0.025). The ultimate load value of C3 differed significantly from those of T1 and T2 (C3 vs. T1 : p=0.048; C3 vs. T2 : p<0.001). Linear correlation analysis revealed a significant correlation between the fenestration area and the volume of bone cement (Pearson's correlation coefficient r=0.288, p=0.036). The bone cement volume and ultimate load significantly correlated with each other in linear correlation analysis (r=0.403, p=0.003). Conclusion : Fenestration yielded a superior ultimate load in comparison with standard BCA using a conventional screw. In T2 screws with asymmetrical two-way fenestrations showed the maximal increase in ultimate load. The fenestrated screws can be expected to show a stable position for the formation of the cement mass.

Analysis of the Damaged Range Caused by LPG Leakage and Vapor Clouds Considering the Cold Air Flow (찬공기 흐름을 고려한 LPG 누출 및 증기운에 의한 피해 영향 범위 분석)

  • Gu, Yun-Jeong;Song, Bonggeun;Lee, Wonhee;Song, Byunghun;Shin, Junho
    • Journal of the Korean Institute of Gas
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    • v.26 no.4
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    • pp.27-35
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    • 2022
  • When LPG leaks from the storage tank, the gas try to sink to the ground because LPG is heavier than air. The gas easily creates vapor clouds causing aggressive accidents in no airflow. Therefore, It is important to prevent in advance by analyzing the damaged range caused from LPG leakage and vapor clouds. So, this study analyzed the range of damaged by LPG leakage and vapor clouds with consideration of the cold air flow which is generated by the topographical characteristics and the land use status at night time in the Jeju Hagari. As a result of the cold air flow using KLAM_21, about 2 m/s of cold air was introduced in from the southeast due to the influence of the terrain. The range of damaged by LPG leakage and vapor cloud was analyzed using ALOHA. When the leak hole size is 10 cm at the wind speed of 2 m/s, the range corresponding to LEL 60 % (12,600 ppm) was 61 m which range is expected to influence in nearby residential areas. These results of this study can be used as basic data to prepare preventive measures of accidents caused by vapor cloud. Forward, it is necessary to apply CFD modeling such as FLACS to check the vapor cloud formation due to LPG leakage in a relatively narrow area and to check the cause analysis.