• Title/Summary/Keyword: high-purity

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오존발생용 세라믹 방전관 특성에 관한 연구 (A Study on Characteristic of Ceramic Tube for Ozone Generation)

  • 조국희;김영배;이홍식
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 하계학술대회 논문집 C
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    • pp.1724-1726
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    • 2002
  • A novel ozonizer has been developed using a high-frequency surface discharge and a high purity alumina ceramic as its dielectric component. A thin ceramic layer, cylindrical in form, is adhered by a film-like induction electrode. An ac exciting voltage of frequency to 0.6 kHz from 1.0 kHz and $6{\sim}9kV$ peak-to-peak is applied between the electrodes to produce a stable high-frequency silent discharge for generation of ozone. A substantial reduction of the exciting voltage is also enabled by using a thin alumina ceramic layer. As a result, the ozonizer can easily produce ozone concentration($128g/m^2$ for oxygen) and power efficiency(360g/kWh for oxygen) without using a special enrichment means.

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고전계 $SiO_2$진공계에서 전구섬락 광방출 특성 (Characteristics of Preflashover Light Emission in High Field $SiO_2$-vacuum Systems)

  • 김정달;정장근;주성철;장기혁;이세훈;이용길;김동희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 하계학술대회 논문집 E
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    • pp.1794-1797
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    • 1997
  • The preflashover light emission of the $SiO_2$-dielectric system behavior under high electric field is discussed. Time dependence of the voltage drop, electrical current, and light emission, are analyzed for high-purity $SiO_2$-vacuum systems under impulse voltage stress. We will summarize the experimental results showing the main feature of the time-dependent system response up to breakdown.

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Microstructure and Mechanical Properties of Rapidly Solidified Powder Metallurgy Al-Fe-V-Si-X Alloys

  • Genkawa, Takuya;Yamasaki, Michiaki;Kawamura, Yoshihito
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1041-1042
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    • 2006
  • High heat-resistant Al-Fe-V-Si and Al-Fe-V-Si-X rapidly solidified powder metallurgy (RS P/M) alloys have been developed under well-controlled high purity argon gas atmosphere. The $Al_{90.49}Fe_{6.45}V_{0.68}Si_{2.38}$ (at. %) RS P/M alloy exhibited high elevated-temperature strength exceeding 300 MPa and good ductility with elongation of 6 % at 573 K. Reduction of $H_2O$ partical pressure in P/M processing atmosphere led to improvement in mechanical properties of the powder-consolidated alloys under elevated-temperature service conditions. Ti addition to the Al-Fe-V-Si conduced to enhancement of the strength at room temperature. The tensile yeild strength and ultimate strenght were 545 MPa and 722 MPa, respectively.

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Improvement in the Super Low Core-loss Soft Magnetic Materials

  • Maeda, Toru;Sato, Atsushi;Mochida, Yasushi;Toyoda, Haruhisa;Mimura, Koji;Nishioka, Takao
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1284-1285
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    • 2006
  • We reported a P/M soft magnetic material with core loss value of $W_{10/1k}=68W/kg$, which is lower than that of 0.35mm-thick laminated material, by using high purity gas-atomized iron powder. Lack of mechanical strength and high cost of powder production are significant issues for industrial use. In order to achieve both low core loss and high strength by using inexpencive powder, the improvement of powder shape and surface morphology and binder strength was conducted. As the result, the material based on water-atomized powder with 80 MPa of TRS and 108 W/kg of core loss (W10/1k) was achieved.

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Isolation of Fucosterol from Pelvetia siliquosa by High-speed Countercurrent Chromatography

  • Hwang, Seung Hwan;Jang, Jai Man;Lim, Soon Sung
    • Fisheries and Aquatic Sciences
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    • 제15권3호
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    • pp.191-195
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    • 2012
  • We report here the use of high-speed countercurrent chromatography (HSCCC) in the preparative isolation and purification of the bioactive component, fucosterol, from Pelvetia siliquosa. A crude extract was obtained by ultrasonic extraction of powdered P. siliquosa using methylene chloride and was then subjected to separation and purification by HSCCC, coupled with evaporative light-scattering detection. Preparative HSCCC was performed successfully using a two-phase solvent system, n-heptane:methanol (3:2, v/v), to obtain 10.96 mg fucosterol with 96.8% purity from 50 mg of crude extract; the recovery rate was approximately 90.5%.

Growth of High Quality $Cd_{0.96} Zn_{0.04} Te$ Epilayers Used for an Far-infrared Sensor and Radiation Detector

  • Kim, B. J.
    • 한국공작기계학회논문집
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    • 제11권6호
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    • pp.111-117
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    • 2002
  • The high quality and a nearly stoichometric growth of $Cd_{1-y} Zn_y$/Te(y=0.04) epilayers have been successfully grown on GaAs substrate by hot wall epitaxy (HWE) by optimizing the growth condition including the preheating treatment and Cd reservoir temperature. The relationship between quality and thickness was examined and best value of FWHM from X-ray rocking curve of 121 arcsec are obtained. Also, emission peaks related to the recombination of free excitons such as the ground state and the first excited state were observed in the PL spectrum at 4.2K. The ($A^0$, X) emission related to Cd vacancy and deep level emission was not measured. These results indicated that the grown CZT/GaAs epilayer was high qualify and purity.

세라믹 방전관의 오존 발생 특성 (Ozone Generation Characteristic of Ceramic Reactor using Ti-Al-Si)

  • 조국희;박재윤;박상현;이동훈;박홍재
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 추계학술대회 논문집 전기물성,응용부문
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    • pp.206-208
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    • 2002
  • A novel ozonizer has been developed using a high frequence surface discharge and a high purity ceramic as its dielectric component. And A cylindrical thin compound ceramic catalyst in reactor is adhered to inside of the film-like outside electrode. An ac exciting voltage with frequency to 0.6 kHz from 1.0 kHz and $4{\sim}6$ kV of peak-to-peak is applied between the electrodes to produce a stable high-frequency silent discharge for generation of ozone. A substantial reduction of the exciting voltage is also enabled by using a thin ceramic. As a result, the ozonizer can easily produce ozone concentration(50 $g/m^3$ for oxygen) and power efficiency(240 g/kWh for oxygen) without using a special enrichment means.

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Study of Fabrication and Improvement of Mechanical Properties of Mg-based Inorganic Fiber using Reflux Process and Silica Coating

  • Yu, Ri;Kim, YooJin
    • 한국분말재료학회지
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    • 제26권3호
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    • pp.195-200
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    • 2019
  • Whisker-type magnesium hydroxide sulfate hydrate ($5Mg(OH)_2{\cdot}MgSO_4{\cdot}3H_2O$, abbreviated 513 MHSH), is used in filler and flame-retardant composites based on its hydrate phase and its ability to undergo endothermic dehydration in fire conditions, respectively. In general, the length of whiskers is determined according to various synthetic conditions in a hydrothermal reaction with high temperature (${\sim}180^{\circ}C$). In this work, high-quality 513 MHSH whiskers are synthesized by controlling the concentration of the raw material in ambient conditions without high pressure. Particularly, the concentration of the starting material is closely related to the length, width, and purity of MHSH. In addition, a ceramic-coating system is adopted to enhance the mechanical properties and thermal stability of the MHSH whiskers. The physical properties of the silica-coated MHSH are characterized by an abrasion test, thermogravimetric analysis, and transmission electron microscopy.

$Mg_2NiH_x$ 수소저장합금의 미세결정구조 및 수소화 특성평가 (Evaluations of Microstructure and Hydrogenation Properties on $Mg_2NiH_x$)

  • 석송;신경;권순용;어순철;이영근;홍태환
    • 한국수소및신에너지학회논문집
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    • 제16권3호
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    • pp.238-243
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    • 2005
  • Mg and Mg-based alloys are most important hydrogen storage materials. It is a lightweight and low-cost materials with high hydrogen storage capacity. However, the formation of hydride at high temperature, the deterioration effect, the hydriding and dehydriding kinetics are bad factor for application. In this study, Mg and Ni have been produced by hydrogen induced mechanical alloying(HIMA) process. The raw materials, Mg(purity 99.9%) chip and Ni(purity 99.95%) chip was prepared by using a planetary ball mill apparatus(FRITSCH pulverisette 5). The balls to chips mass ratio(BCR) are 30:1. The hydrogen pressure induced 2.0MPa and milling times were 12, 24, 48, 72, 96 hours with a rotating speed of 200rpm. X-ray diffraction(XRD) analysis was made to characterize the crystallite size and misfit strain. The crystallite size measured by laser particle size analysis(PSA). Microstructure changes were investigated by scanning electron microscopy(SEM) and the transmission electron microscopy(TEM). The hydrogen storage properties were evaluated by using an Sivert's type automatic pressure-composition-therm(PCT) apparatus.

γ-spectrometer를 이용한 토양시료의 라돈농도 측정법에 관한 연구 (Study on the Measurement of Radon concentrations in soil samples using γ-spectrometer)

  • 강성아;이상수;최규락;이준행
    • 한국방사선학회논문지
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    • 제7권1호
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    • pp.31-36
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    • 2013
  • 우라늄($^{238}U$)의 붕괴과정에서 생성되는 방사성기체인 라돈($^{222}Rn$)은 발생원 중 토양에서 85 % 이상으로 토양의 공극률이 클수록 토양 밖으로 방출할 수 있는 가능성이 많은 동위원소이다. 라돈으로부터 인체를 보호하기 위해서 적절한 대책을 세우는데 무엇보다도 정확한 측정기술의 개발이 선행되어야 한다. 이에 본 연구는 고순도게르마늄(HPGe) 검출기를 이용한 감마선 분광분석법으로 라돈을 측정할 경우에는 불안정한 자연방사능의 백그라운드 문제를 줄일 수 있고, 라듐과 라돈의 딸 핵종들을 방사평형에 이르게 한 후 라돈 농도를 측정하였으며, 토양시료에서의 감마선 방출핵종 및 에너지 스펙트럼을 분석하였다.