• Title/Summary/Keyword: high speed centrifugal spinning

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Fabrication of Porous Cellulose Acetate Propionate/Polybutylene Succinate Microfibers by High Speed Centrifugal Spinning (초고속 원심방사에 의한 아세트산프로피온산 셀룰로오스/폴리부틸렌 숙시네이트 다공성 마이크론 섬유 제조)

  • Tae Young Kim;Mi Kyung Kim;Jinsoo Kim;Jungeon Lee;Jae Hoon Jung;Youngkwon Kim;Tae Hyeon Kim;Ki Young Kim;Jeong Hyun Yeum
    • Textile Coloration and Finishing
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    • v.35 no.4
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    • pp.239-245
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    • 2023
  • Cellulose is an abundant biodegradable material in nature with excellent properties, but due to its poor processability, it has been widely studied for processing through modification. Cellulose acetate propionate (CAP) is a cellulose derivative in which the hydroxyl group of cellulose is replaced by acetyl and propionyl groups. CAP has several advantages, such as excellent solubility, structural stability, light and weather resistance, and good transparency. Porous nanofibers with excellent specific surface area, which can be applied in various fields, can be easily formed by the phase separation method using highly volatile solvents. High speed centrifugal spinning is a nano/micro fiber preparation method with advantages such as fast spinning and easy alignment control. In this study, a CAP/polybutylene succinate (PBS) spinning solution with chloroform as solvent was prepared to prepare porous microfibers and the fiber morphology was examined as a function of the disk rotation speed in an high speed centrifugal spinning device.

Preparation of Polyethylene Micro-fibers by High Speed Centrifugal Melt Spinning (초고속 용융 원심방사를 이용한 폴리에틸렌 마이크론 섬유의 제조)

  • Yang, Seong Baek;Lee, Jungeon;Ji, Byung Chul;Joo, Nam Sik;Yeum, Jeong Hyun
    • Textile Coloration and Finishing
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    • v.32 no.4
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    • pp.239-244
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    • 2020
  • Polyethylene (PE) micro-fiber have been prepared at different hot air temperature (60, 80 and 100 ℃) and different pressure (20, 40, 60 and 80 kPa) by melt centrifugal spinning technique. The parameters of melting centrifugal spinning including polymer contents, rotational velocity, temperature of hot air and pressure were optimized for the fabrication process. The study showed that 8000 rpm rotational velocity, 80 ℃ heated hot air and 40 kPa air pressure are the best condition to obtain uniform and strong PE fiber. The prepared PE fibers were analyzed by field emission scanning electron microscope and universal testing machine and found that fibers with reduced diameter and improved tensile strength are obtained at hot air condition.

Preparation of Poly(vinyl alcohol)/polypropylene Nano-filter by High Speed Centrifugal Solution Spinning (초고속 용액 원심방사를 이용한 폴리비닐알코올/폴리프로필렌 나노필터 제조)

  • Yang, Seong Baek;Lee, Jungeon;Park, Jae Min;Jung, Jae Hoon;Kim, Tae Young;Kim, Ki Young;Lee, Sang Jun;Yeum, Jeong Hyun
    • Textile Coloration and Finishing
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    • v.34 no.1
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    • pp.20-26
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    • 2022
  • Centrifugal spinning is an emerging technique for fabricating micro-to-nano-fibers in recent years. To obtain fibers with the desired size and morphology, it is necessary to configure and optimize the parameters used in centrifugal spinning. In this study, it was controlled by changing the solution's concentration (7.5, 10, and 12.5 wt.%) and disk's rotational velocity (6,000, 8,000, and 10,000 rpm) to prepare centrifugal spun nano-filter. The morphological property, air permeability, and dust collection efficiency of the PVA/PP bi-layer nanoweb prepared by centrifugal spun PVA on the PP micron nonwoven substrate are studied using a field emission scanning electron microscope, an air permeability tester, and a filter tester equipment, and the analysis results indicate that it is suitable as a nano-filter when the concentration of PVA solution is 10 wt.% and the rotational velocity of the disk is 8,000 rpm. The resultant reduced diameter and uniform fibers also proved that an excellent dust collection efficiency filter could be made.

Analysis of Tilting Pad Journal Bearing Characteristics and Rotordynamics for Centrifugal Compressors Using Multiphysics Software (Multiphysics Software를 활용한 원심 압축기용 틸팅 패드 저널 베어링 특성과 회전체 동역학 분석)

  • Soyeon Moon;Jongwan Yun;Sangshin Park
    • Tribology and Lubricants
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    • v.39 no.6
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    • pp.268-272
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    • 2023
  • This study explores the characteristics of tilting pad journal bearings used in the high-speed rotating shaft systems of centrifugal compressors. A centrifugal compressor is a high-speed rotating machine that is widely used to compress gases or vapors employed in various industrial applications. It transfers the centrifugal force of a fast-spinning impeller to the fluid and compresses it under high pressure. Many high-speed rotating shaft systems, which require high stability, use tilting pad journal bearings. The characteristics of these bearings can vary depending on several properties, and identifying the appropriate characteristics is essential to optimize the design on a case-to-case basis. In this study, the authors perform a time-dependent analysis of the properties of tilting pad journal bearings and the rotordynamics of the rotating shaft system using COMSOL Multiphysics software. Specifically, the authors analyze the characteristics of the tilting pad journal bearings by performing a parametric sweep using parameters such as pad clearance, maximum tilting angle, preload, number of pads, and pad pivot offset. The authors then use the results of the bearing-characteristics analysis to evaluate the vibration of the rotating shaft and verify its operation within a desirable range. The understanding gained from this study will allow us to determine the optimal properties of these bearings and the limiting operational speed using COMSOL Multiphysics software.

A Study on the Rotating Ring Using Air Bearing in Yarn Manufacturing Process (방적공정에 있어서 공기 베어링을 이용한 회전링에 관한 연구)

  • Jang, Seung-Ho
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.5
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    • pp.622-630
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    • 2010
  • The increase of the spindle speed to enhance the productivity in ring spinning processes has been limited by yarn tension and heat generation of the traveller/ring. The main causes of yarn tension are 1) the force added directly to the yarn by the rotation of the spindle and 2) the centrifugal force exerted by the yarn balloon generated by traveller rotation. The dominant causes of heat generation are 1) the friction between the ring and traveller and 2) the friction between the traveller and yarn. These factors cause yarn end-breaks and heat damage. In the case of the staple yarn manufacturing process for PET (polyester) and nylon (a heat plasticity material), the rotational speed of the ring spinning system has deteriorated to 10,000rpm. The objective of this study was to develop a rotating ring which has dynamic stability, high productivity and a simple structure to overcome the limitations of the conventional fixed ring/traveller system. The results of this study revealed that the spinning tension could be reduced by 67.8% using the newly developed rotating ring.

Antimicrobial polyhydroxybutyrate submicron fiber mat loaded with extract of Hypericum perforatum

  • Beran, Milos;Horna, Ales;Vorisek, Viktor;Berkova, Eliska;Korinkova, Radka;Trousil, Vojtech;Hrubanova, Marketa
    • Journal of Plant Biotechnology
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    • v.49 no.3
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    • pp.257-270
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    • 2022
  • The aim of this work was to prepare a new biodegradable polyhydroxybutyrate (PHB) submicron fiber mat loaded with hypericin-rich Hypericum perforatum raw extract by centrifugal spinning technology, an alternative approach to the traditional method of electrospinning to fabricate nanofibers or microfibers from solutions at high speed and low cost. Hypericins in methanol/acetone extract of H. perforatum were determined by UHPLC-MS/MS and HPLC/PDA. Submicron fiber mats composed of pure PHB or PHB enriched with H. perforatum extract were prepared using a pilot plant demonstrator for the centrifugal spinning technology and characterized by SEM. Singlet oxygen production was quantified by the 1,3-diphenylisobenzofuran (DPIBF) method in hexane. The results proved a significant production of singlet oxygen by the prepared submicron fiber mat. We also found a significant antibacterial activity against the bacterial strain Escherichia coli CCM 5417 by a method in accordance with JIS Z 2801/ISO 22196 standards. The H. perforatum extract-enriched PHB submicron fiber mats showed potential for the development of self-cleaning and antimicrobial air filters.

Model order reduction for Campbell diagram analysis of shaft-disc-blade system in 3D finite elements

  • Phuor, Ty;Yoon, GilHo
    • Structural Engineering and Mechanics
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    • v.81 no.4
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    • pp.411-428
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    • 2022
  • This paper presents the Campbell diagram analysis of the rotordynamic system using the full order model (FOM) and the reduced order model (ROM) techniques to determine the critical speeds, identify the stability and reduce the computational time. Due to the spin-speed-dependent matrices (e.g., centrifugal stiffening matrix), several model order reduction (MOR) techniques may be considered, such as the modal superposition (MS) method and the Krylov subspace-based MOR techniques (e.g., Ritz vector (RV), quasi-static Ritz vector (QSRV), multifrequency quasi-static Ritz vector (MQSRV), multifrequency/ multi-spin-speed quasi-static Ritz vector (MMQSRV) and the combined Ritz vector & modal superposition (RV+MS) methods). The proposed MMQSRV method in this study is extended from the MQSRV method by incorporating the rotational-speed-dependent stiffness matrices into the Krylov subspace during the MOR process. Thus, the objective of this note is to respond to the question of whether to use the MS method or the Krylov subspace-based MOR technique in establishing the Campbell diagram of the shaft-disc-blade assembly systems in three-dimensional (3D) finite element analysis (FEA). The Campbell diagrams produced by the FOM and various MOR methods are presented and discussed thoroughly by computing the norm of relative errors (ER). It is found that the RV and the MS methods are dominant at low and high rotating speeds, respectively. More precisely, as the spinning velocity becomes large, the calculated ER produced by the RV method is significantly increased; in contrast, the ER produced by the MS method is smaller and more consistent. From a computational point of view, the MORs have substantially reduced the time computing considerably compared to the FOM. Additionally, the verification of the 3D FE rotordynamic model is also provided and found to be in close agreement with the existing solutions.

Spin Test of 5 kWh Composite Flywheel Rotor (5 kWh 복합재 플라이휠 로터의 회전 시험)

  • Han, Hoon-Hee;Ha, Sung-Kyu;Kim, Jae-Hyuk
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.9
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    • pp.3135-3140
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    • 2010
  • A 5 kWh composite flywheel rotor was designed and manufactured, and its spin test was performed to monitor strain distribution and burst speed. Strain distribution in radial and circumferential directions of the rotor were measured using a wireless telemetry system based on bluetooth technology for real-time strain measurement. The strains was compared with pre-calculated design values to verify the initial rotor design. We noticed the rotor failed at 19,499 rpm in the spin test, 11 % lower than the predicted burst speed of 22,000 rpm. Failure occurred at the hub which connects the shaft and the composite rotor. The performance of the composite rotor was confirmed in a general sense, and the danger of unexpected failure of composite rotor during high-speed spinning was also demonstrated in this paper. Special attention should be paid to not only composite rotor but also hub when designing a flywheel energy storage system. The telemetry system needs to be further developed, especially enduring the high centrifugal forces, and can be used in a real time monitoring system for the flywheel energy storage system.