• Journal of the Korean Society for Heat Treatment
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• v.28 no.2
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• pp.68-74
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• 2015

The low cycle fatigue (LCF) and creep-fatigue (hold time tension fatigue, HTTF) tests were performed on the modified 25Cr-13Ni cast stainless steel, which was selected as a candidate material for exhaust manifold in automotive engine. The exhaust manifold is subjected to an environment in which heating and cooling cycle occur due to the running pattern of automotive engine. Several types of fatigue behaviour such as thermal fatigue, thermal mechanical fatigue and creep-fatigue are belong to the main failure mechanisms. High temperature tensile test was firstly carried out to compare the sample with the traditional cast steel for the component. The low cycle fatigue and HTTF tests were carried out under the strain controlled condition with the total strain amplitude from ${\pm}0.6%$ to ${\pm}0.7%$ at $800^{\circ}C$. The hysteresis loops of HTTF tests showed significant stress relaxation during tension hold time. With the increase of tension hold time, the fatigue life was remarkably deceased which caused from the formation of intercrystalline crack by the creep failure mechanism.

• Journal of the Korean institute of surface engineering
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• v.27 no.2
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• pp.74-82
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• 1994

The structure and properties such as adhesion and corrosion resistance of Cr and $Cr_2O_3$ films, deposited on steel plates by the vacuum evaporation method, were investigated. According to the ESCA and AES analy-sis, it could be concluded that chromium oxide with uniform composition could be formed on the steel sub-strate. The deposited Cr and $Cr_2O_3$ films had high adhesion strength, and they did not peeled off by the tape test. The adhesion property, however, was deteriorated as the film thciknes increased. After bending of the deposited specimen many cracks were observed by SEM, and they were assumed to have propagated along co-lumnar boundaries by the bending test. The corrosion resistance of the films was not generally good, which in-dicates that the films had a porous structure with a large number of defects such as pin holes and voids.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.11
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• pp.1979-1985
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• 2003

Fretting is a kind of surface degradation mechanism observed in mechanical components and structures. The fretting damage decreases in 50-70% of the plain fatigue strength. This may be observed in the fossil power plant and the nuclear power plant used in special environments and various loading conditions. The thermal degradation of material is observed when the heat resisting steel is exposed for long period time at the high temperature. In the present study, the degraded 1Cr-0.5Mo steel used for long period time at high temperature (about 515$^{\circ}C$) and artificially reheat-treated materials are prepared. These materials are used for evaluating an effect of thermal aging on the fretting fatigue behavior. Through the experiment, it is found that the fretting fatigue endurance limit of the reheat-treated 1Cr-0.5Mo steel decreased about 46% from the non-fretting fatigue endurance limit, while the fretting fatigue endurance limit of the degraded 1Cr-0.5Mo steel decreased about 53% from the non-fretting fatigue endurance limit. The maximum value of fatigue endurance limit difference is observed as 57%(244 MPa) between the fretting fatigue of degraded material and non-fretting fatigue of reheat-treated material. These results can be a basic data to a structural integrity evaluation of heat resisting steel considered to thermal degradation effect.

• Journal of the Korean institute of surface engineering
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• v.53 no.2
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• pp.72-79
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• 2020

Two Fe-Cr steels of T22 steel and STS430 steel were corroded at 650 and 750℃ for 100hr in sewage sludge-(0.3% SO₂-6% O₂-10% H₂O-balance CO₂) mixed gas environment. T22 steel corroded faster than STS430, indicating that the Cr content significantly influence the corrosion rates. T22 formed thick and non-protective Fe₂O₃ as the major oxide and Fe₃O₄ as the minor one. With an increase in corrosion temperature, their corrosion rates increased, being accompanied with formation of pores and cracks in the thickened oxide scales that were non-adherent. STS430 steel formed Fe₂O₃, Fe₃O₄ as the outer scale and (Fe, Cr)-O as the inner layer by which its corrosion rate is greatly reduced. Both the T22 and STS430 steel samples formed multi-layered scales by outward diffusion of Fe ions and inward diffusion of oxygen and sulfur ions at high-temperature more than 650℃.

• Clinical Endoscopy
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• v.57 no.2
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• pp.237-245
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• 2024

Background/Aims: Endoscopic ultrasound-guided tissue acquisition (EUS-TA) using Franseen needles is reportedly useful for its high diagnostic yield. This study compared the diagnostic yield and puncturing ability of EUS-TA using 22-gauge cobalt-chromium (CO-Cr) needles with those of stainless-steel Franseen needles in patients with solid pancreatic lesions. Methods: Outcomes were compared between the 22-gauge Co-Cr Franseen needle (December 2019 to November 2020; group C) and stainless-steel needle (November 2020 to May 2022; group S). Results: A total of 155 patients (group C, 75; group S, 80) were eligible. The diagnostic accuracy was 92.0% in group C and 96.3% in group S with no significant intergroup differences (p=0.32). The rate of change in the operator (from training fellows to experts) was 20.0% (15/75) in group C and 7.5% (6/80) in group S. Stainless-steel Franseen needles showed less inter-operator difference than Co-Cr needles (p=0.03). Conclusions: Both Co-Cr and stainless-steel Franseen needles showed high diagnostic ability. Stainless-steel Franseen needles are soft and flexible; therefore, the range of puncture angles can be widely adjusted, making them suitable for training fellows to complete the procedure.

• Corrosion Science and Technology
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• v.19 no.1
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• pp.43-50
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• 2020

In this study, the effects of KCl(s) and K₂SO₄(s) on the oxidation characteristics of 2.25Cr-1Mo steel were investigated for 500 h in 10O₂ + 10CO₂ (vol%) gas environmen at 650 ℃. Oxidation kinetics were characterized by weight gain, oxide layer thickness, and fitted models for the experiment data were proposed. The fitted models presented considerable agreement with the experimental data. The oxide layer was analyzed using the scanning electron microscope, optical microscope, and energy dispersive X-ray spectroscopy. The oxidation kinetics of 2.25Cr-1Mo steel with KCl and K₂SO₄ coatings showed significantly different oxidation kinetics. KCl accelerated the oxidation rate very much and had linear oxidation behavior. In contrast, K₂SO₄ had no significant effect, which had parabolic kinetics. The oxide layer was commonly composed of Fe₂O₃, Fe₃O₄, and FeCr₂O₄ spinel. KCl strongly accelerated the oxidation rates of 2.25Cr-1Mo steel in the high-temperature oxidation environment. Conversely, K₂SO₄ had little effect on the oxidation rates.

• Journal of the Korean Society for Precision Engineering
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• v.14 no.11
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• pp.69-76
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• 1997

The rotating bending fatigue tests were performed using the specimens taken from Cr-Mo-V steel, widely sued in thermal power plant turbines, at various temperatures such as room temperature, 300 .deg. C, 425 .deg. C and 550 .deg. C. The characteristics of fatigue crack propagation were examined and analyzed by using fracture mechanics parameter. The plastic replica method was also applied in order to measure the crack length on the basis of serial observation of fatigue crack propagation behavior on the defected specimen surface. The fatigue crack propagation behavior of Cr-Mo-V steel was investigated within the frame work of elastic-plastic fracture mechanics. The propagation law of fatigue crack is obtained uniquely by using the term .sigma. $^{n}$ sub a/where .sigma. $_{a}$ is the service stress, a is the crack length and n is a constant. The values of constant n are nearly equal to 2.48, 2.60 and 8.61 at room temperature, 300 .deg. C and 425 .deg. C.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.210-215
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• 2001

The ferritic 2.25CrMo steel has been used for high temperature structure applications such as turbine rotors, boilers and pressure vessels in fossil plant and petroleum chemical facilities. However, this steel is known to result in aging degradation due to temper embrittlement, carbide induced brittleness and softening of matrix after long time exposure to high temperature. This research investigated the microstructural and mechanical changes after artificial degradation treatment and evaluated the degree of degradation by several nondestructive methods. The decrease of electrical resistivity and increase of magnetic Barkhausen noise(RMS voltage) with increasing aging time were observed. The change of electrical resistivity and Barkhausen noise showed a good correlation with the ductile-brittle transition temperature.

• Journal of the Korean Society for Heat Treatment
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• v.29 no.4
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• pp.181-189
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• 2016

The variation in microstructure and mechanical properties during heat treatment was examined in a series of 0.27% C-1.0% Si-1.5% Mn steels with chromium contents in the range of 0 to 1.0 wt%. It was found that chromium decreased the martensite packet size through the austenite grain refinement and increased tensile strength in the as-quenched steel, about 70 MPa per 1.0 wt%. The 0.27% C-1.0% Si-1.5% Mn-1.0% Cr steel showed tensile strength of 1700 MPa in the as-quenched steel. The 0.27% C-1.0% Si-1.5% Mn-1.0% Cr steel revealed a full martensitic structure after air cooling from $900^{\circ}C$ to room temperature, showing air hardening characteristics. Tempering at $150^{\circ}C$ slightly decreased the tensile strength and increased elongation, which is in a good agreement with impact toughness result.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.1
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• pp.103-110
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• 2010

In this study, an assessment method on creep-fatigue crack initiation and crack growth for a Mod.9Cr-1Mo steel (ASME Grade 91) structure has been developed with an extension of the French RCC-MR A16 procedure. The current A16 guide provides defect assessment procedure for a creep-fatigue crack initiation and crack growth for an austenitic stainless steel, but no guideline is available yet for a Mod.9Cr-1Mo steel which is now widely being adopted for structural materials of future nuclear reactor system as well as ultra super critical (USC) thermal plant. In the present study an assessment method on creep-fatigue crack initiation and crack growth is provided for the FMS (Ferritic-Martensitic Steel) and assessment on the creep-fatigue crack behavior for a structure has been carried out. The assessment results were compared with the observed images from a structural test.