• 동력기계공학회지
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• 제5권2호
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• pp.63-70
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• 2001

To obtain the optimal condition of heat treatment of wear-resistant alloy, hardness and Charpy V-notch test have been performed with Co-based Stellite No.4, No.6 and Tribaloy 800 alloys, following by heat treatment at the various conditions. Heat treatment at $1250^{\circ}C$ for 1 hours caused the as-casted Tribaloy 800 with FCC crystal structure to transform to HCP structure and lamellar eutectic structure was disappeared, which did not influence on the hardness. Aging at $800^{\circ}C$ for 20 hours, following by $1250^{\circ}C$ for 2 hours heat treatment has enhanced hardness significantly, which is due to the precipitation of large amounts of Laves-phase. The hardness of Stellite alloys was increased by the aging at $800^{\circ}C$ to 5 hours, and was nearly constant by the aging over 5 hours. The toughness of Stellite alloys was a few influenced by the aging treatment.

• Elastomers and Composites
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• 제40권2호
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• pp.119-127
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• 2005

고무부품의 신뢰성을 확보하기 위해서 고무재료의 물성파악과 수명평가는 매우 중요하다 하겠다. 본 연구에서는 냉장고 콤프레샤 모터에서 발생되는 소음 및 진동 제어 목적으로 고무마운트에 사용되는 고무재료인 NBR과 EPDM에 대해 상온과 $70^{\circ}C,\;85^{\circ}C,\;100^{\circ}C$에서 75일 동안 노화시킨 상태에서 단축 인장과 이축 인장으로 물성시험을 수행하여 가교밀도, 100% 모듈러스 변화와 응력-변형률 관계를 파악하였다. 또한, 고무소재의 노화수명을 예측하기 위해 가속열 노화시험을 수행하여 시간-온도 환산식인 아레니우스 관계식을 구하였다.

• 한국구조물진단유지관리공학회 논문집
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• 제25권6호
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• pp.103-110
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• 2021

유연한 고무재료와 강재 보강판을 적층으로 구성한 탄성받침은 우수한 수직강성과 유연한 횡강성으로 교량의 내진보강용으로 널리 사용되고 있다. 무엇보다 시공이 간단하고 비용이 높지 않다는 장점을 지니고 있다. 고무재료의 한 종류인 합성고무는 천연고무에 비해 노화에 대한 저항성이 크지만 이 역시 다양한 열화요인으로 성능이 저하된다. 내진설계기준 및 내진성능평가요령에서는 이러한 노화의 특성을 반영하고 있지 않지만 관련 연구가 축적되면 이를 반영하는 것이 합리적이다. 합성고무를 대상으로 노화촉진시간과 노출시간을 변수로 하여 노화촉진시험을 수행하여 전단특성의 변화를 분석하였다. 노화가 진행될수록 최대전단응력과 전단변형율은 감소한다. 또한 동일한 전단변형률에서 전단강성이 크게 증가한다.

• Elastomers and Composites
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• 제47권3호
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• pp.201-209
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• 2012

그로멧은 자동차의 고무부품들 중의 하나로 에틸렌 프로필렌 고무로 구성되어 있으며, 고무의 비선형 초탄성 성질은 고무제품의 거동을 예측하는데 중요하다. 본 논문에서는, 일축인장시험과 이축인장시험을 통하여 안정된 응력-변형률 관계를 구하고 그로멧에 대한 유한요소해석을 수행하였고, 수명예측을 위한 노화시험을 소개하였다.

• Journal of Advanced Marine Engineering and Technology
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• 제27권3호
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• pp.453-459
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• 2003

In this study, the effect of heat treatment to the electrochemical polarization resistance for the Ti-6Al-4V alloy was measured. The solution heat treatments were carried out at $1066^{circ}E, 966^{\circ}$E$, followed by aging heat treated $550^{circ}E, 600^{circ}E, and 650^{circ}E$. The electrochemical polarization resistance behavior was measured by potentio-dynamic polarization in the 1N $HNO_3$ + 15ppm HF solution. The obtained results were as follows. 1. As solution heat temperature increased. the corrosion potential was increased, whereas passive current density and critical current density were decreased. 2. As aging heat temperature increased, the corrosion potential was almost constant, but passive current density was decreased 3. The results of composition test measured by EDS at grain boundary and near $\gamma'$ precipitates indicated that S, Cl. and Si which originated from base metal were segregated at the grain boundaries Al and Ti which were the main alloying element in $\gamma'$ were depleted at the $\gamma'$ precipitated. The depletion of Al and Ti in $\gamma'$ was caused to early breakdown of passive film.

• Journal of Advanced Marine Engineering and Technology
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• 제23권6호
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• pp.761-769
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• 1999

In this paper the effect of aging heat treatment to the Corrosion behavior for the Nimonic 80A superalloy was studied by AC Impedance methods. Tested solution was 3.5% with tempera-ture $25^{\circ}C$ Electro-chemical corrosion test were carried out for the Nimonic 80A super-alloy which solution heat treated at $1080^{\circ}C$ for 8 hours followed by aging heat treated at $650^{\circ}C,\;700^{\circ}C,\;750^{\circ}C\;800^{\circ}C$ and $850^{\circ}C$ with 16hours under vacuum environment. The obtained results were as follows; 1. Base metal and solution-treated materials were exhibited similar corrosion tendency as Ran-dle equivalent cell. The value of passive film resistance was 579 ohms for the base metal and 124,770 ohms for the solutionized metal such a difference was arose by the ${{\gamma}_^'}$ precipitate on the metal surface during heat treatment. 2. The measure value of $R_p$ for heat-treated at $650^{\circ}C,\;700^{\circ}C,\;800^{\circ}C$and $850^{\circ}C$ were 97,943, 93, 111, 26,961, 15,798 and 11,780ohm respectively. Which indicated that the passive film resistance Rp was reduced as aging temperature increased due to the growth of grain size and sensitization at the grain boundary. 3. The similar tendency was exhibited for corrosion behavior of the electro-chemical corrosion polarization method and AC impedance method and confirmed that AC impedance method was useful tool for corrosion research.

• 한국표면공학회지
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• 제50권5호
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• pp.380-385
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• 2017

Mechanical characteristics of the STS 304 which is heat resistance steel were investigated after artificial aging at $650^{\circ}C$ with 1,000 hours. Tensile test specimens and small test pieces were done artificial aging up to 1,000 hours in the high temperature atmospheric environment. The results present that as the aging time increased, tensile properties were deteriorated. In the case of failure mechanism, the configuration of the fractography presented drastic change from ductile to brittle with aging time. $M_{23}C_6$ carbide leading to the change of the mechanical properties and fracture mode of the aged STS 304 steel continuously precipitated along the grain boundaries of austenite microstructure.

• 한국구조물진단유지관리공학회 논문집
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• 제25권6호
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• pp.95-102
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• 2021

유연한 고무재료를 사용하는 탄성받침은 최근 교량의 내진보강용으로 많이 적용되고 있다. 그러나 다양한 요인에 의하여 고무재료의 노화가 진행되고 이로 인해 탄성받침의 전단강성에 변화가 생기고 이는 교량의 내진성능에 영향을 미친다. 천연고무를 대상으로 노화촉진시간과 노출시간을 변수로 하여 노화촉진시험을 수행하여 전단특성의 변화를 분석하였다. 노화가 진행될수록(노화촉진온도 및 노출시간이 증가할수록) 최대전단응력과 전단변형율은 감소한다. 또한 동일한 전단변형률에서 전단강성이 크게 증가한다. 이는 고무재료가 경화됨을 의미하며 탄성받침의 내진성능이 저하되는 것을 암시한다.

• 대한전기학회논문지
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• 제45권4호
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• pp.553-557
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• 1996

Heat cycle aging of insulating materials in large generator stator winding has been investigated using both on-line and off-line test methods. On this study, principally, off-line test against actual generator in service was carried out to acquire information about polarization index(PI) and dissipation factor, dissipation factor tip-up, maximum partial discharge for the purpose of remnant breakdown voltage and life assessment. It was found from the tests that both dissipation factor and maximum partial discharge decreased with the increase of operating hours and starting numbers. It was found from off-line tests that the remnant breakdown voltage had a strong relationship with both dissipation factor and maximum partial discharge the remnant breakdown voltage as a results of both operating hours and starting number and the nondestructive tests were proposed as parameters which can predict the remnant lifetime of insulating materials in large generator stator windings. (author). 8 refs., 8 figs., 2 tabs.

• 해양환경안전학회지
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• 제22권1호
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• pp.138-144
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• 2016

티타늄은 표면에 형성되는 보호성 부동태 피막 때문에 일반부식과 해수에서 내식성이 강하지만 염산, 황산, 인산 등의 산에서는 보호성 산화물 피막이 파괴된다고 알려져 있다. 본 연구에서는 Ti에 Al 및 V등을 첨가한 ${\alpha}+{\beta}$계에 대하여 $1066^{\circ}C$와 $966^{\circ}C$에서 5시간 용체화 열처리를 실시하고, 이 시편을 $550^{\circ}C$, $600^{\circ}C$, 및 $650^{\circ}C$에서 각각 1시간, 4시간, 8시간 및 16시간 시효열처리한 후 마이크로비커스 경도를 측정하고, 이 시편을 1N $H_2SO_4$ 용액에서 전기화학적 분극법으로 부식을 계측하였으며, 분극을 마친 시편의 표면을 현미경 조직사진으로 부식상태를 검토하였다. 시험 결과 용체화열처리한 시편이 모재와 시효열처리한 시편보다 높은 내식성을 나타내며. 용체화 온도가 높고 시간이 길어질수록 내식성은 증가하였다.