• Title/Summary/Keyword: grain composition

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Effects of Annealing on the Microstructure and Electrical Properties of ZnO Varistor (ZnO 바리스터 제조시 소결후 열처리 조건에 따른 미세구조 및 전기적 특성에 관한 연구)

  • Soh, J.J.;Han, S.W.;Kim, H.S.
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1679-1681
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    • 1996
  • ZnO varistor with composition of 89wt%-ZnO, 3.0wt%-$Bi_{2}O_{3}$, 3.6wt%-$Sb_{2}O_{3}$, 1.16wt%-CoO, 0.88wt%-NiO, 0.71wt%-$MnO_2$, 0.93wt%-$Cr_{2}O_{3}$, 0.013wt%-$Al_{2}O_{3}$ was fabricated by sintering methods. The effects of annealing on the J-E characteristics of ZnO varistors were investigated. These changes of electric properties were found to be caused by the variation of grains and grain boundary related to annealing. And the conductive mechanism and micostructure of ZnO varistor were researched using I-V meter, SEM and XRD.

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Microstructural Properties of (Pb)(La,Ce)$TiO_3$ ceramics as a function of $MnO_2$ addition ($MnO_2$ 첨가에 따른 (Pb)(La,Ce)$TiO_3$ 세라믹스의 미세구조특성)

  • Oh, D.U.;Min, S.K.;Yoon, K.H.;Yoo, J.H.;Park, C.Y.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.442-445
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    • 2001
  • In this study, microstructural and dielectric properties of $Pb_{0.83}(La_{0.2}Ce_{0.8})_{0.08}TiO_3$(PCT) ceramics as a function of $MnO_2$ addition were investigated for 30MHz ceramic resonator application. Grain size was gradually increased according to the increase of $MnO_2$ addition amount and showed the highest value of $1.502{\mu}m$ at the 0.9wt% $MnO_2$. Moreover, density showed the highest value of $7.582 g/cm^3$ at the 0.7wt% $MnO_2$.All the composition ceramics,curie temperature was nearly constant around $330^{\circ}C$

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Study on the Preparation of Ferrite Powder for Bonded Magnets (본드 자석용 페라이트 분말의 제조에 관한 연구)

  • 진성빈;임재근;문현욱;신용진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1994.11a
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    • pp.65-66
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    • 1994
  • This paper describes study on the preparation of ferrite powder for bonded mallets. The specimen which has the basic composition of SrO$.$nF$_2$O$_3$ with n=5.9 is in nonstoichiomatric region. Calcination is performed under N$_2$ atmosphere 1175$^{\circ}C$, 1200$^{\circ}C$, 1225$^{\circ}C$, 1250$^{\circ}C$ and 1275$^{\circ}C$ respectively. Then, Cooling is carried out in the furnace. In order to increase coecivity and obtain uniform grain size, we add to the specimen 0.7wt%CaCO$_3$, 0.3wt % SiO$_2$, 0.5wt%Na$_2$SiO$_3$ and 0.5wr% Al$_2$O$_3$. Also, in order to increase milling effect, carbon coating on sample particles is tried. As the result, single magnetic domain partic1e with Size of 1$\mu\textrm{m}$ in obtained and magnetic properties are improved.

Analysis of C-V and Frequency Characteristics of the ZnO nano-powder Varistors (ZnO 나노파우더 바리스터의 C-V 및 주파수 특성 분석)

  • Wang, Min-Sung;Jeong, Jong-Yub;Song, Min-Jong;Park, Choon-Bae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.183-184
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    • 2005
  • In this study, our varistors based on M.Matsuoke's composition were fabricated with ZnO nano-powder whose sizes were 50nm and 100nm. Electrical properties of ZnO nano-powder varistors were obtained by capacitance-voltage and frequency-real impedance. nano-powder varistors are indicated the change of the interface defects density $N_t$ at the grain boundaries and the donor concentration $N_d$ in the ZnO grains. Frequency analysis was accomplished to understand the equivalent circuit.

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Structural Properties of $MgTiO_3-SrTiO_3$ Geramics with Sintering Temperature (소결온도에 따른 $MgTiO_3-SrTiO_3$ 세라믹의 구조적 특성)

  • Choi, Eui-Sun;Lee, Moon-Kee;Ryu, Ki-Won;Lee, Young-Hie
    • Proceedings of the KIEE Conference
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    • 1999.11d
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    • pp.953-955
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    • 1999
  • The (1-x)$MgTiO_3-SrTiO_3$ (x=0. 0.1, 0.2, 0.3) ceramics were prepared by the conventional mixed oxide method. The structural properties were investigated with sintering temperature and composition ratio by XRD, SEM and BT-TGA. Increasing the sintering temperature from $1300^{\circ}C$ to $1600^{\circ}C$, second phase was decreased and grain size was increased. The average gram size of the 0.8$MgTiO_3-SrTiO_3$ ceramics sintered at $1600^{\circ}C$ were $3.61{\mu}m$.

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Machinability evaluation of non-coated end mill tool fabricated by ultra-fine WC (초미립 WC로 제작된 무코팅 엔드밀 공구의 가공성 평가)

  • Kim D.H.;Kwon D.H.;Kang I.S.;Kim J.S.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.13-14
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    • 2006
  • The quality of tool material is very important factor in machining evaluation. The characteristics of tungsten carbide, such as grain size and hardness, and density are depending on the variation of Co composition and WC size. In this study, the non-coated end mill which is made of ultra-fine tungsten carbide is investigated by measuring tool wear and tool lift test. The machining test is conducted with high hardened workpiece under high-speed cutting condition.

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Effect of base metal and welding heat input on the properties of low temperature steel welds made by Electro Gas Welding (저온용 강재 Electro Gas 용접부 물성에 미치는 모재와 용접 입열의 영향)

  • Sung, Hee-Joon;Goo, Yeon-Baeg;Kim, Kyeong-Ju
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.51-51
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    • 2009
  • In order to understand the properties of high heat input welds made by electro gas welding, two kinds of low temperature steel were welded. Welding heat inputs were controlled by width of root gap and ranged from 118 to 143kJ/cm. Chemical composition and micro-structural analysis were performed. To understand low temperature impact properties, Charpy impact test was conducted at several temperatures. The results were summarized as follows; 1) Grain size of weld metal and heat affected zone was increased with an increase in welding heat input. 2) Impact test values at fusion line were severely fluctuated regardless of base metals, showing enormous difference among the values at the same test temperature.

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Settling Mode of the Dredged Soil (준설토의 침강형태에 관한 연구)

  • 윤상묵;장병욱;차경섭
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.45 no.1
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    • pp.63-73
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    • 2003
  • The settling of the dredged soil may vary with mineral composition, grain size distribution, initial water content and salt concentration of suspension of the site. A series of settling column test was performed to investigate the behaviour of solid suspension material from dredging and reclamation. Settling mode was divided into four types from the observation of interface and settling curves of clay minerals and marine clay samples, and the relationship charts of salt concentration and the initial water content were established to use in the dredging operation with any salt concentration. The critical initial water content which was defined as a threshold of zone settling and the consolidation settling was varied with salt concentration of water and was proportional to the plasticity of soil in sea water.

Occurrence of Electrum from the Namseong Gold Mine (남성(南星) 금광산산(金鑛山産) 에렉트럼의 산상(産狀))

  • Lee, Hyun Koo;Kim, Sang Jung;Choi, Seon Gyu
    • Economic and Environmental Geology
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    • v.20 no.4
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    • pp.223-234
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    • 1987
  • This paper describes the mode of occurrence and mineralogical properties of electrum from the Namseong Gold-Silver deposits, for the purpose of obtaining data on the characteristics of the ore deposits and the behavior of gold and silver during the mineralization. The gangue minerals are quartz, calcite, fluorite. Ore minerals are mainly composed of pyrite, sphalerite, chalcopyrite and galena with minor amount of argentite, electrum, pyrargyrite, native silver and unidenfied mineral(Cu-Fe-Ag-S series). Three stage of mineralization recognized are, from early to later, (I) pyrite-electrum stage (II) sphalerite-chalcopyrite-galena-argentite-electrum stage (III) sulfosalts stage. The filling temperature of fluid inclusions in quartz ranges from $225^{\circ}$ to $335^{\circ}C$. The value of sulfur fugacity estimated by means of electrum-tarnish method ranges from $10^{-11.5}$ to $10^{-14}$ atm. The compositional heterogeneity within a single grain with respect to gold concentration is common in the Namseong electrums Chemical composition of electrum ranges generally between 25~45 atom% Au. Its gold content decreases in late stages of mineralization.

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Tailings Behavior and Performance of the Tailings Return Unit of the Head-feed Combine(I) -Ratio and Compositions of Tailings- (자탈형(自脱型) 콤바인 환원장치(還元裝置)의 환원물(還元物) 유동현상(流動現象)과 환원성능(還元性能) 개선(改善)에 관한 연구(硏究)(I) -환원율(還元率)과 조성비(組成比)-)

  • Cho, Y.K.;Chung, C.J.;Choi, K.H.;Park, P.K.
    • Journal of Biosystems Engineering
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    • v.16 no.1
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    • pp.18-26
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    • 1991
  • This study was undertaken to investigate the ratio and compositions of tailings of the tailings return unit in the commercially available head-feed combines. The ratio of the returned tailings to the sum of the threshed grain and the returned tailings was 2.3~7.2% for various varieties of rice and operational conditions of combines tested and increased as the feeding rate and the cleaning air volume increased. The analysis of the returned tailings showed that the composition of rubbish and short straw was decreased as the feeding rate and the cleaning air volume increased.

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