• Title/Summary/Keyword: fracture surfaces

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Effects of Interface Boundary Strength on Wear and Wear Transition during Sliding in Silicon Carbide Ceramics (탄화규소계 세라믹스에서 미끄럼시의 마모 및 마모천이에 미치는 계면강도의 영향)

  • Kim, Dong-Jin;Park, Seong-Khil;Ryu, Hyun;Um, Chang-Do;Cho, Seong-Jai;Kim, Seock-Sam
    • Tribology and Lubricants
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    • v.11 no.4
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    • pp.21-27
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    • 1995
  • The effects of interface boundary strength on wear and wear transition during sliding have been investigated in silicon carbide ceramics. Three different microstructures, i.e., solid state sintered silicon carbide, liquid phase sintered silicon carbide and liquid phase sintered silicon carbide composite reinforced with TiB$_{2}$ particulates, were designed by hot pressing. Examinations of crack patterns and fracture modes indicated that interface boundaries were relatively strong between silicon carbide grains in the solid state sintered silicon carbide, intermediate in the liquid phase sintered silicon carbide and weak between silicon carbide grains and TiB$_{2}$ particles in the composite. Wear data and examinations of worn surfaces revealed that the wear behavior of these silicon carbide ceramics could be significantly affected by the interface strength. In the solid state sintered silicon carbide, the wear occurred by a grooving process. In the liquid phase sintered silicon carbide and composite, on the other hand, an abrupt transition in wear mechanism from initial grooving to grain pull-out process occurred during the test. The transition occurred significantly earlier in the composite than in the carbide.

Processing and Mechanical, Thermal and Morphological Properties of Poly(lactic acid)/Poly(butylene succinate) Blends (폴리유산/폴리부틸렌숙시네이트 블랜드의 가공 및 기계적, 열적, 형태학적 특성)

  • Kim, Dae Keun;Cho, Donghwan
    • Journal of Adhesion and Interface
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    • v.15 no.1
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    • pp.14-21
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    • 2014
  • In the present work, PLA/PBS blends with poly(lactic acid) (PLA) and poly(butylene succinate) (PBS) at different contents were processed by using a twin-screw extruder and an injection molding machine, and then their mechanical, thermal and morphological properties were investigated. The mechanical properties such as flexural strength, flexural modulus, tensile strength and tensile modulus and thermal properties such as melting behavior, dynamic mechanical thermal properties and thermal stability significantly depended on the contents of PLA and PBS. However, the heat deflection temperature of the blends was not significantly influenced by the contents of PLA and PBS. Also, the fracture surfaces of PLA/PBS blends were changed from a brittle pattern to a ductile pattern with increasing the PBS contents.

Influence of Hold Time and Stress Ratio on Cyclic Creep Properties Under Controlled Tension Loading Cycles of Grade 91 Steel

  • Kim, Woo-Gon;Park, Jae-Young;Ekaputra, I Made Wicaksana;Kim, Seon-Jin;Jang, Jinsung
    • Nuclear Engineering and Technology
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    • v.49 no.3
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    • pp.581-591
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    • 2017
  • Influences of hold time and stress ratio on cyclic creep properties of Grade 91 steel were systemically investigated using a wide range of cyclic creep tests, which were performed with hold times (HTs) of 1 minute, 3 minutes, 5 minutes, 10 minutes, 20 minutes, and 30 minutes and stress ratios (R) of 0.5, 0.8, 0.85, 0.90, and 0.95 under tension loading cycles at $600^{\circ}C$. Under the influence of HT, the rupture time increased to HT = 5 minutes at R = 0.90 and R = 0.95, but there was no influence at R = 0.50, 0.80, and 0.85. The creep rate was constant regardless of an increase in the HT, except for the case of HT = 5 minutes at R = 0.90 and R = 0.95. Under the influence of stress ratio, the rupture time increased with an increase in the stress ratio, but the creep rate decreased. The cyclic creep led to a reduction in the rupture time and an acceleration in the creep rate compared with the case of monotonic creep. Cyclic creep was found to depend dominantly on the stress ratio rather than on the HT. Fracture surfaces displayed transgranular fractures resulting from microvoid coalescence, and the amount of microvoids increased with an increase in the stress ratio. Enhanced coarsening of the precipitates in the cyclic creep test specimens was found under all conditions.

A Calibration Method of the CSC Model for Considering Material Properties of Ultra-high Performance Concrete (초고성능 강섬유 보강 콘크리트 물성 반영을 위한 소성 기반 콘크리트 CSC 모델 보정기법)

  • Gang-Kyu, Park;MinJoo, Lee;Sung-Wook, Kim;Hyun-Seop, Shin;Jae Heum, Moon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.4
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    • pp.402-410
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    • 2022
  • The present study introduces a calibration method of the CSC model implemented in the LS-DYNA program for considering the material properties of ultra-high performance concrete(UHPC). Based on previous experimental studies, various parameters, which constitute three shear failure surfaces, pressure-volumetric strain curve, fracture energy, dynamic increase factor(DIF), and so on, are modified. Then, the proposed calibration method is verified by comparing the numerical result with the experimental data through the single element analysis. In addition, based on the established finite element models, the applicability of the calibrated CSC model is examined for UHPC structures subjected to impact and blast loadings.

Damage Analysis of Train Rail Fishplate (전동차 선로 이음매 판의 파손 해석)

  • Seo-Hyun Yun;Byoung-Chul Choi;Ki-Hang Shin;Ki-Woo Nam
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.2_2
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    • pp.341-347
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    • 2023
  • The subway is one of the most common and important means of transportation in modern society. In order to use the subway safely, tracks are necessary, but trains are prone to derailment and collisions. In order for the train to run safely on the track, the fishplate that connects the line connection is used. The damaged railway was a fishplate for connecting subway lines used for 11 years, and damage analysis and countermeasures were presented. Beach marks were observed on both fracture surfaces, and striations appeared at the range of crack propagation. The damaged part is Cr carbide, which has a higher hardness than the base metal, and is judged to be embrittled and destroyed by fatigue. The SM50C fishplate was subjected to a cyclic stress of about 59% of the upper limit of tensile-compression fatigue limit, but inclusions were the cause of failure. In order to prevent fatigue failure of the SM50C steel fishplate, the occurrence of inclusions should be minimized and processed to have a homogeneous structure when manufacturing the fishplate. In addition, compressive residual stress is given through surface modification such as peening to control crack generation. It is necessary to minimize the change in shape that can become a stress concentration part along with accurate fastening of the bolt, and to design the stress distribution to be as uniform as possible.

A new formulation of cracking in concrete structures based on lumped damage mechanics

  • Daniel V.C. Teles;Rafael N. Cunha;Ricardo A. Picon;David L.N.F. Amorim;Yongtao Bai;Sergio P.B. Proenca;Julio Florez-Lopez
    • Structural Engineering and Mechanics
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    • v.88 no.5
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    • pp.451-462
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    • 2023
  • Lumped Damage Mechanics (LDM) is a theory proposed in the late eighties, which assumes that structural collapse may be analyzed as a two-phase phenomenon. In the first (pre-localization) stage, energy dissipation is a continuous process and it may be modelled by means of the classic versions of the theory of plasticity or Continuum Damage Mechanics (CDM). The second, post-localization, phase can be modelled assuming that energy dissipation is lumped in zones of zero volume: inelastic hinges, hinge lines or localization surfaces. This paper proposes a new LDM formulation for cracking in concrete structures in tension. It also describes its numerical implementation in conventional finite element programs. The results of three numerical simulations of experimental tests reported in the literature are presented. They correspond to plain and fiber-reinforced concrete specimens. A fourth simulation describes also the experimental results of a new test using the digital image correlation technique. These numerical simulations are also compared with the ones obtained using conventional Cohesive Fracture Mechanics (CFM). It is then shown that LDM conserves the advantages of both, CDM and CFM, while overcoming their drawbacks.

Effect of Adding Graphene/Carbon Nanotubes (FCN) on the Mechanical Properties of Polyamide-Nylon 6 (그래핀/탄소나노튜브(FCN) 첨가에 따른 Polyamide-Nylon 6의 기계적 특성에 미치는 영향)

  • Seung-Jun Yeo;Hae-Reum Shin;Woo-Seung Noh;Man-Tae Kim
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.6_3
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    • pp.1297-1303
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    • 2023
  • Research on enhancing the mechanical strength, lightweight properties, electrical conductivity, and thermal conductivity of composite materials by incorporating nano-materials is actively underway. Thermoplastic resins can change their form under heat, making them highly processable and recyclable. In this study, Polyamide-Nylon 6 (PA6), a thermoplastic resin, was utilized, and as reinforcing agents, fused carbon nano-materials (FCN) formed by structurally combining Carbon Nanotube(CNT) and Graphene were employed. Nano-materials often face challenges related to cohesion and dispersion. To address this issue, Silane functional groups were introduced to enhance the dispersion of FCN in PA6. The manufacturing conditions for the composite materials involved determining the use of a dispersant and varying FCN content at 0.05 wt%, 0.1 wt%, and 0.2 wt%. Tensile strength measurements were conducted, and FE-SEM analysis was performed on fracture surfaces. As a result of the tensile strength test, it was confirmed that compared to pure PA6, the strength of the polymer composite with a content of 0.05 wt% was improved by about 60%, for 0.1 wt%, about 65%, and for 0.2 wt%, the strength was improved by 50%. Also, when compared according to the content of FCN, the best strength value was shown when 0.1 wt% was added. The elastic modulus also showed an improvement of about 15% in the case of surface treatment compared to the case without surface treatment, and an improvement of about 70% compared to pure PA6. Through FE-SEM, it was confirmed that the matrix material and silane-modified nanomaterial improved the dispersibility and bonding strength of the interface, helping to support the load evenly and enabling effective stress transfer.

MARGINAL MICROLEAKAGE AND SHEAR BOND STRENGTH OF COMPOSITE RESIN ACCORDING TO TREATMENT METHODS OF ARTIFICIAL SALIVA-CONTAMINATED SURFACE AFTER PRIMING (접착강화제 도포후 인공타액에 오염된 표면의 처리방법에 따른 복합레진의 번연누출과 전단결합강도)

  • Cho, Young-Gon;Ko, Kee-Jong;Lee, Suk-Jong
    • Restorative Dentistry and Endodontics
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    • v.25 no.1
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    • pp.46-55
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    • 2000
  • During bonding procedure of composite resin, the prepared cavity can be contaminated by saliva. In this study, marginal microleakage and shear bond strength of a composite resin to primed enamel and dentin treated with artificial saliva(Taliva$^{(R)}$) were evaluated. For the marginal microleakage test, Class V cavities were prepared in the buccal surfaces of fifty molars. The samples were randomly assigned into 5 groups with 10 samples in each group. Control group was applied with a bonding system (Scotchbond$^{TM}$ Multi-Purpose plus) according to manufacture's directions without saliva contamination. Experimental groups were divided into 4 groups and contaminated with artificial saliva for 30 seconds after priming: Experimental 1 group ; artificial saliva was dried with compressed air only, Experimental 2 group ; artificial saliva was rinsed and dried. Experimental 3 group ; cavities were etched with 35% phosphoric acid for 15 seconds after rinsing and drying artificial saliva. Experimental 4 group ; cavities were etched with 35% phosphoric acid for 15 seconds and primer was reapplied after rinsing and drying artificial saliva. All the cavities were applied a bonding agent and filled with a composite resin (Z-100$^{TM}$). Specimens were immersed in 0.5% basic fuschin dye for 24 hours and embedded in transparent acrylic resin and sectioned buccolingually with diamond wheel saw. Four sections were obtained from one specimen. Degree of marginal leakage was scored under stereomicroscope and their scores were averaged from four sections. The data were analyzed by Kruscal-Wallis test and Fisher's LSD. For the shear bond strength test, the buccal or occlusal surfaces of one hundred molar teeth were ground to expose enamel(n=50) or dentin(n=50) using diamond wheel saw and its surface was smoothed with Lapping and Polishing Machine(South Bay Technology Co., U.S.A.). Samples were divided into 5 groups. Treatment of saliva-contaminated enamel and dentin surfaces was same as the marginal microleakage test and composite resin was bonded via a gelatin capsule. All specimens were stored in distilled water for 48 hours. The shear bond strengths were measured by universal testing machine (AGS-1000 4D, Shimaduzu Co., Japan) with a crosshead speed of 5 mm/minute. Failure mode of fracture sites was examined under stereomicroscope. The data were analyzed by ANOVA and Tukey's studentized range test. The results of this study were as follows : 1. Enamel marginal microleakage showed no significant difference among groups. 2. Dentinal marginal microleakages of control, experimental 2 and 4 groups were lower than those of experimental 1 and 3 groups (p<0.05). 3. The shear bond strength to enamel was the highest value in control group (20.03${\pm}$4.47MPa) and the lowest value in experimental 1 group (13.28${\pm}$6.52MPa). There were significant differences between experimental 1 group and other groups (p<0.05). 4. The shear bond strength to dentin was higher in control group (17.87${\pm}$4.02MPa) and experimental 4 group (16.38${\pm}$3.23MPa) than in other groups, its value was low in experimental 1 group (3.95${\pm}$2.51 MPa) and experimental 2 group (6.72${\pm}$2.26MPa)(p<0.05). 5. Failure mode of fractured site on the enamel showed mostly adhesive failures in experimental 1 and 3 groups. 6. Failure mode of fractured site on the dentin did not show adhesive failures in control group, but showed mostly adhesive failure in experimental groups. As a summary of above results, if the primed tooth surface was contaminated with artificial saliva, primer should be reapplied after re-etching it.

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Geochemical Characterization of Rock-Water Interaction in Groundwater at the KURT Site (물 암석 반응을 고려한 KURT 지하수의 지구화학적 특성)

  • Ryu, Ji-Hun;Kwon, Jang-Soon;Kim, Geon-Young;Koh, Yong-Kwon
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.10 no.3
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    • pp.189-197
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    • 2012
  • Geochemical composition of fracture filling minerals and groundwater was investigated to characterize geochemical characteristics of groundwater system at the KURT site. Minerals such as calcite, illite, laumontite, chlorite, epidote, montmorillonite, and kaolinite, as well as I/S mixed layer minerals were detected in the minerals extracted from the fracture surfaces of the core samples. The groundwater from the DB-1, YS-1 and YS-4 boreholes showed alkaline conditions with pH of higher than 8. The electrical conductivity (EC) values of the groundwater samples were around $200{\mu}S/cm$, except for the YS-1 borehole. Dissolved oxygen was almost zero in the DB-1 borehole indicating highly reduced conditions. The Cl- concentration was estimated around 5 mg/L and showed homogeneous distribution along depths at the KURT site. It might indicate the mixing between shallow groundwater and deep groundwater. The shallow groundwater from boreholes showed $Ca-HCO_3$ type, whereas deep groundwater below 300 m from the surface indicated $Na-HCO_3$ type. The isotopic values observed in the groundwater ranged from -10.4 to -8.2‰ for ${\delta}^{18}O$ and from -71.3 to -55.0‰for ${\delta}D$. In addition, the isotope-depleted water contained higher fluoride concentration. The oxygen and hydrogen isotopic values of deep groundwater were more depleted compared to the shallow groundwater. The results from age dating analysis using $^{14}C$ indicated relatively younger (2000~6000yr old) groundwater compared to other european granitic groundwaters such as Stripa (Sweden).

Effect of Application of ZirLiner® and Blasting Treatments on Shear Bond Strength of Zirconia-Veneered Porcelain Interface (지르코니아-전장도재 계면의 전단결합강도에 대한 ZirLiner® 적용과 분사처리의 영향에 관한 연구)

  • Shin, Young-Ho;Lee, Yu-Na;Lee, Hae-Hyoung;Dong, Jin-Keun;Oh, Sang-Chun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.24 no.1
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    • pp.113-127
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    • 2008
  • The purpose of this study was to evaluate effect of application of $ZirLiner^{(R)}$ and blasting treatments on shear bond strength of zirconia-veneered porcelain interface. 60 uncolored zirconia plates and 30 colored zirconia plates were fabricated and divided into nine groups of 10 according to blasting treatment such as as-ground, glass blasting and alumina blasting and zirliner application. Veneering porcelains were built up over the center of the treated zirconia ceramic surface using jig and fired according to the manufacturers' instructions. Each specimen was completely embedded in acrylic resin. The specimens were placed in a mounting jig and subjected to shear force by a universal testing machine. Load was applied at a crosshead speed of 0.5㎜/min until failure. Average shear strengths were analyzed with two-way analysis of variance and one-way analysis of variance and the Duncan's post-hoc test. The fracture surfaces of the failed specimens were examined by SEM. The obtained results were as follows: 1. Depending on surface treatment by blasting, the degree of roughness is revealed in the order of Glass-blasted, As-ground, and Alumnia-blasted. The roughness average of uncolored and colored zirconia ceramic were not significantly different from blasting treatments. 2. In uncolored zirconia ceramic, the shear bond strength were not significantly different from blasting treatments. However, the shear bond strength were significantly different from Zirliner application. 3. Used ZirLiner, mean shear bond strength of colored zirconia was lower than uncolored zirconia. Especially, mean shear bond strength of colored zirconia was quite low with alumina-blasting treatment. 4. SEM analysis showed that veneered porcelain failed in zirconia ceramic interface and there was no cohesive failure.