• Advances in materials Research
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• v.3 no.3
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• pp.151-161
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• 2014

Geopolymer composites reinforced with different layers of woven flax fabric are fabricated using lay- up technique. Mechanical properties, such as flexural strength, flexural modulus and fracture toughness of geopolymer composites reinforced with 2.4, 3 and 4.1 wt% flax fibres are studied. The fracture surfaces of the composites are also examined using scanning electron microscopy. The results show that all the mechanical properties of the composites are improved by increasing the flax fibre contents. It is also found that the mechanical properties of flax fabric reinforced geopolymer composites are superior to pure geopolymer matrix. Micro-structural analysis of fracture surface of the composites indicated evidence of various toughening mechanisms by flax fabrics in the composites.

• Journal of the Korean Society of Safety
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• v.17 no.4
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• pp.38-44
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• 2002

The application of fractal concept provides an useful method in the study for the quantitative analysis of irregular variations like the fracture surfaces and crack profiles. Fractal curves have characteristics that represents a self-similarity based on the fractal dimension. The fractal dimensions were obtained by the box counting method. In this report, we obtained the nearly stable fractal dimensions of fracture crack profiles for STS316 with CT specimen as the crack advances and the relationships between crack length and fractal dimension. Moreover fractal fracture parameter that corresponds to J-R curve is shown by the relationships between fractal dimension and crack extension. From the results, we concluded that crack extension of high toughness material also shows the fractal characteristics, which can be used in order to evaluate the crack life precisely.

• Journal of the Korean institute of surface engineering
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• v.33 no.4
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• pp.241-250
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• 2000

Popcorn cracking phenomena frequently occur in thin plastic packages during the solder reflow process, which are definitely affected by poor adhesion of Cu-based leadframe to epoxy molding compounds (EMCs). In the present work, in order to enhance the adhesion strength, a brown-oxide treatment on the Cu-based leadframe was carried out and the adhesion strength of leadframe/EMC interface was measured in terms of fracture toughness by using sandwiched double-cantilever beam (SDCB) specimens. After the adhesion tests, fracture surfaces were analyzed by SEM, AES, EDS and AFM to make the failure path clear. Results showed that failure path was closely related to the oxidation time and the interfacial fracture toughness.

• Transactions of Materials Processing
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• v.30 no.5
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• pp.247-254
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• 2021

This study reviews dynamic deformation behavior of ultra-fine-grained Al alloys, ultra-fine-grained conventional low carbon steel and dual phase steel and Zr-based amorphous alloys. Dynamic tests were conducted using a Kolsky bar then the test data was analyzed in relation to resultant microstructures, mechanical properties and propensity of adiabatic shear band. In addition, deformed microstructures and fracture surfaces were used to investigate the behavior of both the dynamic deformation and fracture, and adiabatic shear banding. As a result, increasing microstructural homogeneity, strain hardenability and forming multiple shear bands could be a better way to increase the fracture resistance under dynamic loading as the formation of adiabatic shear bands was reduced or prevented.

• Restorative Dentistry and Endodontics
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• v.24 no.4
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• pp.604-613
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• 1999

This study was performed to evaluate the effect of resin and filler type on the fracture toughness of light-activated composites. Experimental composites were prepared using urethane tetramethacrylate(UTMA) and bisphenol glycidylmethacrylate(Bis-GMA) monomers and five different types of silica fillers. Fracture toughness was measured by a single edge V-notched beam(SEVNB) method, which was discussed from ASTM E399-78. Rectangular bars of $2.5{\times}5{\times}26mm$ were prepared with experimental composites and a notch about 2.25mm deep was carved at the center of the long axis of the specimen using a dental diamond disk driven by a dental micro engine. The flexural test was carried out at a crosshead speed of 0.05mm/min and fracture surfaces were observed under scanning electron microscope. The results obtained were summarized as follows: 1. The fracture toughness values of UTMA-based composites were relatively higher than those of Bis-GMA-based composites. 2. The highest fracture toughness value was observed in the UTMA-based composite containing the $1.5{\mu}m$-spherical fillers. 3 Aging in the distilled water at $37^{\circ}C$ for 10 days showed the increase of fracture toughness, which was severer in the Bis-GMA-based composites than those of UTMA-based composites. 4. The AE amplitude occurring during the fracture toughness tests was the highest at the point of macroscopic fracture.

• Restorative Dentistry and Endodontics
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• v.29 no.3
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• pp.267-272
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• 2004

The purpose of this in vitro study was to evaluate the effect of surface defects and cross-sectional configuration of NiTi rotary files on the fatigue life under cyclic loading. Three NiTi rotary files ($K3^{TM},{\;}ProFile^{\circledR},{\;}and{\;}HERO{\;}642^{\circledR}$) with ＃30/.04 taper were evaluated. Each rotary file was divided into 2 subgroups : control (no surface defects) and experimental group (artificial surface defects), A total of six groups of each 10 were tested. The NiTi rotary files were rotated at 300rpm using the apparatus which simulated curved canal (40 degree of curvature) until they fracture. The number of cycles to fracture was calculated and the fractured surfaces were observed with a scanning electron microscope. The data were analyzed statistically. The results showed that experimental groups with surface defects had lower number of cycles to fracture than control group but there was only a statistical significance between control and experimental group in the $K3^{TM}$ (p<0.05), There was no strong correlation between the cross-sectional configuration area and fracture resistance under experimental conditions. Several of fractured files demonstrated characteristic patterns of brittle fracture consistent with the propagation of pre-existing cracks. This data indicate that surface defects of NiTi rotary files may significantly decrease fatigue life and it may be one possible factor for early fracture of NiTi rotary files in clinical practice.

• Journal of the Korean Association of Oral and Maxillofacial Surgeons
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• v.28 no.1
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• pp.16-23
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• 2002

To understand the micro-mechanical changes and the effects of the fluoride on rat's femur after administration of sodium fluoride, the three-point bending test, acoustic emission analysis during the three-point bending test and scanning electron microscopy were performed. The obtained results were as follows: 1. Bone strength increased in the rats given 1, 5, 10 and 20 ppm of fluoride but, there were no statistical significances (p>0.05). 2. With increasing the concentration of fluoride, most AE events released rapidly just before the maximum load and smaller events were recorded than the control group's. The average of cumulative AE event counts until maximum load of the femur in 20 ppm group were significantly small with respect to the control group's (p<0.05). 3. Fracture surfaces were well coincide with the results of acoustic emission behavior. Analyses of fracture surfaces indicated that, consistent with its the highest load, rat femur in 20 ppm fluoride group displays the roughest surface.

• Restorative Dentistry and Endodontics
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• v.22 no.2
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• pp.792-800
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• 1997

The purpose of this study was to evaluate the adaptation of self-cured glass ionomer cement and resin-modified glass ionomer cement and polyacid-modified resin composite, which are light-cured giass ionomer cements, to dentin surface. Twelve extracted human maxillary and mandibular molar teeth were used in this study. The entire occlusal dentin surfaces of teeth were exposed with Diamond Wheel Saw and smoothed with sand papers (300, 600, 1200grits). They were randomly assigned into 3 groups according to glass ionomer cements used; Control group- Fuji II, Expeimental group 1 - Fuji II LC, Expeimental group 2 - Dyract. According to the manufacturer's directions, three glass ionomer cements were bonded to exposed dentin surfaces of the tooth crown and cured. Crowns and glass ionomers were trimmed after 24hrs and sectioned horizontally and vertically with diamond saw. The interface of glass ionomer cements and dentin was examined under SEM. The results were as follows : 1. Good adatation between glass ionomer cement and dentin on the horizontal section was showed in control and experimental group 1, but the gap of $20{\mu}m$, which was observed distinct separation between glass ionomer cement and dentin, was showed in experimental group 2. 2. Good adatation between glass ionomer cements and dentin on the vertical section was showed in control and experimental group 1, but the gap of 80-$100{\mu}m$ was showed in experimental group 2. 3. Cohesive fracture within glass ionomer cements in control and experimental group 1 was showed, but no cohesive fracture was showed in experimental group 2.

• Macromolecular Research
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• v.16 no.5
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• pp.411-417
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• 2008

The surfaces of henequen fibers, which can be obtained from the leaves of agave plants, were treated with two different media, tap water and sodium hydroxide, that underwent both soaking and ultrasonic methods for the fiber surface treatment. Various biocomposites were fabricated with untreated and treated, chopped henequen fibers and polypropylene using a compression molding method. The result is discussed in terms of interfacial shear strength, flexural properties, dynamic mechanical properties, and fracture surface observations of the biocomposites. The soaking (static method) and ultrasonic (dynamic method) treatments with tap water and sodium hydroxide at different concentrations and treatment times significantly influenced the interfacial, flexural and dynamic mechanical properties of henequen/polypropylene biocomposites. The alkali treatment was more effective than the water treatment in improving the interfacial and mechanical properties of randomly oriented, chopped henequen/PP bio-composites. In addition, the application of the ultrasonic method to each treatment was relatively more effective in increasing the properties than the soaking method, depending on the treatment medium and condition. The greatest improvement in the properties studied was achieved by ultrasonic alkalization of natural fibers, which was in agreement with the other results of interfacial shear strength, flexural strength and modulus, storage modulus, and fracture surfaces.

• Restorative Dentistry and Endodontics
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• v.16 no.2
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• pp.126-142
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• 1991

The purpose of this study was to evaluate the effect of various dentin surface treatments on shear bond strength, microhardness and fracture mode before and after thermocycling. Recently extracted 75 human molars were used. The teeth were sagittal sectioned faciolingually to obtain 150 specimens. They were randomly divided into six groups. Mesial and distal dentinal surfaces of specimens were exposed by grinding and treated respectively with GC-DENTIN CONDITIONER. 10-3 solution of 4-Meta, Cleansar and Primer of GLUMA, Scotchprep of Scotchbond 2, DENTIN CONDITIONER and PRIMER A, B of ALL BOND according to the manufacturers directions. Specimens of one group were not treated. Adhesive agent of Scotchbond 2, were applied and cured on the treated dentin surfaces. After P-50 were cured on them, specimens were stored in 31c water for 24 hours before shear bond strength measurement Shear bond strength was measured in 10 specimens of each group. 10 specimens of each group were thermocycled in $20^{\circ}C$, $60^{\circ}C$,$20^{\circ}C$, $4^{\circ}C$, $20^{\circ}C$ water in order, for 30 seconds respectively, 100 times a day for 7 days. After thermocycling shear bond strength was measured. Microhardness was checked on treated dentin surface and fractured dentin surface in 10 specimens respectievly. Francture modes were observed with SEM The following results were obtained. 1. Before thermocycling. shear bond strengths in the specimens treated with DENTIN CONDITIONER and PRIMER A, B of ALL BOND were significantly higher than those in other specimens(P<0.01). 2. After thermocycling. shear bond strengths in the specimens treated with Cleanser and Primer of GLUMA, Scotchprep of Scotchbond 2 and DENTIN CONDITIONER and PRIMER A, B of AIL BOND were significantly higher than those in specimens not: treated, treated with GC-DENTIN CONDITIONER and 10-3 solution of 4-Meta(P<0.01). Shear bond strengths in the specimens treated with GC-DENTIN CONDITIONER and PRIMER A, B of ALL BOND were significantly higher than those in other specimens except those treated with Scotchprep of Srotchbond 2(P<0.01). 3. Shear bond strengths after thermocycling were reduced in the specimens not treated, treated with GC-DENTIN CONDITIONER and 10-3 solution of 4-Meta and were increased in the specimens treated with Cleanser and Primer of GLUMA, Scotchprep of Scotchbond 2, without significance, compared with those before thermocycling. In the specimens treated with DENTIN CONDITIONER and PRIMER A, B of ALL BOND, shear bond strengths after thermocycling were significantly increased, compared with those before thermocycling(P<0.01). 4. Microhardnesses in the fractured surfaces after shear bond strength measurement were significantly increased in the specimens treated with 10-3 solution of 4-Meta and significantly decreased in the specimens treated with DENTIN CONDITIONER and PRIMER A, B of ALL BOND, compared with those in the treated dentin surfaces(P<0.01). 5. In the specimens treated with Cleanser and Primer of GLUMA, Scotchprep of Scotchbond 2 and DENTIN CONDITIONER and PRIMER A, B of ALL BOND, cohesive fracture modes were observed more than adhesive fracture modes.