• Title/Summary/Keyword: fracture surfaces

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Cure Behaviors and Fracture Toughness of PEl/Difunctional Epoxy Blends (PEI/DGEBA 블랜드계의 열적특성 및 파괴인성)

  • Park, Soo-Jin;Jin, Sung-Yeol;Kaang, Shinyoung
    • Journal of Adhesion and Interface
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    • v.4 no.3
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    • pp.33-40
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    • 2003
  • In this work, diglycidyl ether of bisphenol A (DGEBA)/polyetherimide (PEI) blends were cured using 4,4-diaminodiphenyl methane (DDM). And the effects of addition of different PEI contents to neat DGEBA were investigated in the thermal properties and fracture toughness of the blends. The contents of contents of containing PEI were varied in 0, 2.5, 5, 7.5, and 10 phr. The cure activation energies ($E_a$) of the cured specimens were determined by Kissinger equation and the mechanical interfacial properties of the specimens were performed by critical stress intensity factor ($K_{IC}$). Also their surfaces were examined by using a scanning electron microscope (SEM) and the surface energetics of blends was determined by contact angles. As a result, $E_a$ and $K_{IC}$ showed maximum values in the 7.5 phr PEI. This result was interpreted in the increment of the network structure of DGEBA/PEI blends. Also, the surface energetics of the DGEBA/PEI blends showed a similar behavior with the results of $K_{IC}$. This was probably due to the improving of specific or polor component of the surface free energy of DGEBA/PEI blends, resulting in increasing the hydrogen bonding of the hydroxyl and imide groups of the blends.

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An Experimental Study on the Fracture and Shear Bonding Strength of Resin-modified Glass lonomer Cements (Resin-modified glass ionomer cements의 파절 및 저단결합강도에 관한 실험적 연구)

  • Kim, Jae-Gon;Yang, Cheol-Hee;An, Soo-Hyeon;Rho, Yong-Kwan;Baik, Byeong-Ju
    • Journal of the korean academy of Pediatric Dentistry
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    • v.25 no.1
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    • pp.234-248
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    • 1998
  • The purpose of this study was to compare the fracture and shear bonding strength of resin-modified glass ionomer cements with composite resin and conventional glass ionomer cement Three kinds of restorative materials including a composite resin (Z 100), a conventional glass ionomer cement(Fuji II), and resin- modified glass ionomer cements(Fuji II LC, Vitremer, Dyract and Compoglass) were investigated in this study. For measurement of fracture and shear bonding strength, disk samples of the materials were prepared and cylindrical samples of the materials were bonded the flat enamel and dentin surfaces according to manufactuer's instructions. All specimen were determinated by using an Instron testing machine with a crosshead speed of 1 mm/min. Then, each treated enamel and dentin surface was observed by SEM. The following results were obtained. 1. The bi-axial flexural strength of Z 100 was highest, and Fuji n LC, Vitremer, Dyract and Compoglass were significantly higher than Fuji n (P<0.05). 2. The shear bonding strength of Z 100 on the enamel and dentin surface was higher than other experimental groups except Fuji II LC(P<0.05). Fuji II LC was significantly higher than Fuji II (P<0.05), but in the case of Vitremer, Dyract and Compoglass were similar to Fuji II (P>0.05). 3. The shear bonding strength of Z 100 and Fuji II LC on the enamel surface were highly increased as compared with dentin surface (P<0.05), but in the case of Fuji II, Vitremer, Dyract and Compoglass were not different between enamel and dentin(P>0.05). 4. In the Z 100 and Fuji II LC, obvious etched enamel surface and exposed dentinal tubules according to remove of smear layer and smear plug were observed.

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Green Composites. II. Environment-friendly, Biodegradable Composites Using Ramie Fibers and Soy Protein Concentrate (SPC) Resin

  • Nam Sung-Hyun;Netravali Anil N.
    • Fibers and Polymers
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    • v.7 no.4
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    • pp.380-388
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    • 2006
  • Fully biodegradable and environment-friendly green composite specimens were made using ramie fibers and soy protein concentrate (SPC) resin. SPC was used as continuous phase resin in green composites. The SPC resin was plasticized with glycerin. Precuring and curing processes for the resin were optimized to obtain required mechanical properties. Unidirectional green composites were prepared by combining 65% (on weight basis) ramie fibers and SPC resin. The tensile strength and Young's modulus of these composites were significantly higher compared to those of pure SPC resin. Tensile and flexural properties of the composite in the longitudinal direction were moderate and found to be significantly higher than those of three common wood varieties. In the transverse direction, however, their properties were comparable with those of wood specimens. Scanning electron microscope (SEM) micrographs of the tensile fracture surfaces of the green composite indicated good interfacial bonding between ramie fibers and SPC resin. Theoretical values for tensile strength and Young's modulus, calculated using simple rule of mixture were higher than the experimentally obtained values. The main reasons for this discrepancy are loss of fiber alignment, voids and fiber compression due to resin shrinking during curing.

A local-global scheme for tracking crack path in three-dimensional solids

  • Manzoli, O.L.;Claro, G.K.S.;Rodrigues, E.A.;Lopes, J.A. Jr.
    • Computers and Concrete
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    • v.12 no.3
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    • pp.261-283
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    • 2013
  • This paper aims to contribute to the three-dimensional generalization of numerical prediction of crack propagation through the formulation of finite elements with embedded discontinuities. The analysis of crack propagation in two-dimensional problems yields lines of discontinuity that can be tracked in a relatively simple way through the sequential construction of straight line segments oriented according to the direction of failure within each finite element in the solid. In three-dimensional analysis, the construction of the discontinuity path is more complex because it requires the creation of plane surfaces within each element, which must be continuous between the elements. In the method proposed by Chaves (2003) the crack is determined by solving a problem analogous to the heat conduction problem, established from local failure orientations, based on the stress state of the mechanical problem. To minimize the computational effort, in this paper a new strategy is proposed whereby the analysis for tracking the discontinuity path is restricted to the domain formed by some elements near the crack surface that develops along the loading process. The proposed methodology is validated by performing three-dimensional analyses of basic problems of experimental fractures and comparing their results with those reported in the literature.

Elastic-plastic Analysis of a 3-Dimensional Inner Crack Using Finite Element Alternating Method (유한요소 교호법을 이용한 삼차원 내부 균열의 탄소성 해석)

  • Park, Jai-Hak;Park, Sang-Yun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.10
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    • pp.1009-1016
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    • 2007
  • Finite element alternating method has been suggested and used effectively to obtain the fracture parameters in assessing the integrity of cracked structures. The method obtains the solution from alternating independently between the FEM solution for an uncracked body and the crack solution in an infinite body. In the paper, the finite element alternating method is extended in order to obtain the elastic-plastic stress fields of a three dimensional inner crack. The three dimensional crack solutions for an infinite body were obtained using symmetric Galerkin boundary element method. As an example of a three dimensional inner crack, a penny-shaped crack in a finite body was analyzed and the obtained elastc-plastic stress fields were compared with the solution obtained from the finite element analysis with fine mesh. It is noted that in the region ahead of the crack front the stress values from FEAM are close to the values from FEM. But large discrepancy between two values is observed near the crack surfaces.

Study on grindability of ferrite (페라이트의 연삭성에 관한 연구)

  • Kim, Seong-Cheong;Lee, Jae-U
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.9
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    • pp.1507-1519
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    • 1997
  • This paper aims to clarify the effects of grinding conditions on bending strength in surface grinding of various ferrites with the resin bond diamond wheel. The main conclusions obtained were as follows. At a constant material removal rate, the strength improves with increased wheel depth of cut and decreased workpiece speed. It is desirable to grind at higher peripheral wheel speed and under the critical workpiece speed presented in this paper. Grinding the ferrite of higher brittleness, the wheel depth of cut limited to hold 50% of their inherent strength becomes lower. The effect of various grinding conditions on bending strength becomes more larger in the order of Sr, Mn-Zn and Cu-Ni-Zn. When using the diamond grain of the lower toughness, the bending strength becomes higher, and the wheel wear occurs faster. Considering both bending strength and wheel wear rate, the best concentration of wheel is 100. The ground surfaces exhibit that the fracture process during grinding becomes more brittle in the order of Sr, Mn-Zn and Cu-Ni-Zn.

Characteristics of Fatigue Crack Propagation and Changes in Strain Induced Martensite α' of STS 304 Stainless Steel (LNG 304 스테인레스강의 피로균열전파특성과 변형유발 마르텐사이트 함량의 변화)

  • Kim, Song-Hee;Pak, Hyung-Rae;Lee, Hyun-Seung
    • Journal of Industrial Technology
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    • v.21 no.B
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    • pp.341-348
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    • 2001
  • The effect of initial ${\alpha}^{\prime}$ in STS 304 Stainless Steel on fatigue resistance, and fatigue crack propagation behavior was studied with using C-T specimens. Higher ${\Delta}K_{th}$ was observed in the specimens with the content of 0% initial ${\alpha}^{\prime}$ than in the contents of 2% and 33% initial ${\alpha}^{\prime}$. The difference of da/dN at the same level of ${\Delta}K$ was distinctive in low and intermediate level of ${\Delta}K$ however became less different as the level of ${\Delta}K$ increased. It is because the formation of strain induced martensite occurred readily in lower ${\alpha}^{\prime}$ at the vicinity of the fatigue crack tip, which causes compressive residual stresses resulting in the enhancement of crack closure. In general fatigue cracks propagated transgranular mode and many segments of ridges were observed on the fracture surfaces. At the higher contents of initial ${\alpha}^{\prime}$ appeared the smaller size of ridge segments. Slips in austenite were blocked more frequently by the martensite colonies formed in austenite.

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Wear assessment of the WC/Co cemented carbidetricone drillbits in an open pit mine

  • Saeidi, Omid;Elyasi, Ayub;Torabi, Seyed Rahman
    • Geomechanics and Engineering
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    • v.8 no.4
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    • pp.477-493
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    • 2015
  • In rock drilling, the most important characteristic to clarify is the wear of the drill bits. The reason that the rock drill bits fail with time is wear. In dry sliding contact adhesive wear deteriorates the materials in contact, quickly, and is the result of shear fracture in the momentary contact joins between the surfaces. This paper aims at presenting an overview of the assessment of WC/Co cemented carbide (CC) tricone bit in rotary drilling. To study wear of these bits, two approaches have been used in this research. Firstly, the new bits were weighted before they mounted on the drill rigs and also after completion their useful life to obtain bit weight loss percentage. The characteristics of the rock types drilled by using such this bit were measured, simultaneously. Alternatively, to measure contact wear, namely, matrix wear a micrometer has been used with a resolution of 0.02 mm at different direction on the tricone bits. Equivalent quartz content (EQC), net quartz content (QC), muscovite content (Mu), coarseness index (CI) of drill cuttings and compressive strength of rocks (UCS) were obtained along with thin sections to investigate mineralogical properties in detail. The correlation between effective parameters and bit wear were obtained as result of this study. It was observed that UCS shows no significant correlation with bit wear. By increasing CI and cutting size of rocks wear of bit increases.

The effect of retention grooves in Acrylic resin tooth denture base bond (합성수지 인공치와 열중합의치상 Resin의 결합시 인공치에 형성하는 유지공의 효과에 관한 연구)

  • Kim, Bu-Sob
    • Journal of Technologic Dentistry
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    • v.9 no.1
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    • pp.51-55
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    • 1987
  • One of the primary advantages of acrylic resin teeth is their ability to bond chemically to the denture base resins. Fracture od acrylic resin teeth from a maxillary denture, however, is not uncommon. Bonding failures have been attributed to faulty boil-out procedures that fail to eliminate all traces of wax from the ridge lap surfaces of the teeth and to contamination of the ridge lap surface by careless application of tinfoil substitute. Attempts to increase the strength of the bond between acrylic resin teeth and heat-cured denture base resin include grinding the glossy ridge lap surface (in fluid system), painting the ridgelap surface of the teeth with monomer-polymer solution, and cutting retention grooves in the ridge lap surface of the teeth. This latter method has been tested by applying a tensile force in a labial direction to the incisal part of the lingual surface of the acrylic resin teeth. A progressive shear compressive load was applied at an angle to the lingual surface of acrylic resin teeth bonded to denture base acrylic resin. No statistically singificant advantage was derived by preparing retention grooves of different shapes in the ridgelap surface of the denture teeth.

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Sliding Wear Behavior of Plasma Sprayed Zirconia Coatingagainst Silicon Carbide Ceramic Ball

  • Le Thuong Hien;Chae Young-Hun;Kim Seock Sam;Kim Bupmin;Yoon Sang-bo
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2004.11a
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    • pp.66-74
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    • 2004
  • The sliding wear behavior of $ZrO_2-22wt\%MgO\;(MZ)\;and\;ZrO_2-8wt\%Y_2O_3\;(YZ)$ deposited on a casting aluminum alloy with bond layer (NiCrCoAlY) by plasma spray against an SiC ball was investigated under dry test conditions at room temperature. At all load conditions, the wear mechanisms of the MZ and the YZ coatings were almost the same. The wear mechanisms involved the forming of a smooth film by material transferred on the sliding surface and pullout. The wear rate of the MZ coating was less than that of the YZ coating. With an increase normal load the wear rate of the studied coatings increased. The SEM was used to examine the sliding surfaces and elucidate likely wear mechanisms. The EDX analysis of the worn surface indicated that material transfer was occurred from the SiC ball to the disk. It was suggested that the material transfer played an important role in the wear performance.

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