• Title/Summary/Keyword: finer grain size

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The effects of starting precursor conditions on the phase formation and transport properties of Bi-2223/Ag tapes

  • Chunhai Jiang;Jaimoo Yoo;Jaewoong Ko;Kim, Haidoo;Hyungsik Chung
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2002.02a
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    • pp.343-345
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    • 2002
  • The influence of starting precursor powders on the phase formation and transport properties of Bi-2223/Ag tapes has been studied. The experimental results show that the average particle size of precursors as fine as 1.64 ${\mu}{\textrm}{m}$ and 1.51 ${\mu}{\textrm}{m}$ can still increase the transport properties. The J$_{c}$-B behavior is also enhanced in tapes fabricated with powders in finer particle sizes. However, at higher magnetic fields, J$_{c}$ of tape started from the powder with the finest particles drops rapidly at the direction of H//c, which is possibly attributed to the small grain sizes and weak flux pinning ability that due to the short induction period at the initial stage of phase formation as the result of fine particles in precursor powder.der.

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A Study on the Moisture Adsorption and Permeability Characteristics of Weathered Granite Soils (화강토의 풍화도가 수분흡착 및 침투성에 미치는 영향)

  • 이대훈;도덕현
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.26 no.3
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    • pp.81-89
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    • 1984
  • To examine the moisture adsorption and permeability characteristics, weathered granite soils of different degrees of weathering, cultivated upland soils and sands of Han-river were sampled. The results are as follows: 1. In case that the mother rock was same, the pF values under same moisture content decreased according as the grain size of soil became finer by the weathering process. 2. In case that the mother rock was different, the pF value varied by the behavior of clay minerals, and the cultivated upland soils showed more sensitive reaction than sands and fresh granite soils. 3. The pF value changed by the difference of primary moisture content and also influenced by soil structure, testing method and etc. 4. The pF value and compaction curve had close relation, however under same moisture content, the pF value decreased by the increment of density. 5. The permeability depend on the available void ratio between the soil particles according to the degree of weathering, and the pF value of available void water between the soil particles which related directly to permeability was about 3.3 except the void water holded in the soil particles. 6. As the above, the pF value and permeability were differentiated by degree of weathering, primary moisture content, density and etc. Therefore it is considered unreasonable to define uniformly by soil texture.

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Effect of Starting Crystallographic Phase on the Mechanical Properties of Hot-Pressed SiC Ceramics (초기분말의 결정상이 $Al_2O_3$를 소결 조제로한 고온가압 SiC 세라믹스의 기계적 특성에 미치는 영향)

  • 정동익;강을손;최원봉;백용기
    • Journal of the Korean Ceramic Society
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    • v.29 no.3
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    • pp.232-240
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    • 1992
  • Densification behavior, microstructural evolution, and mechanical properties of hot-pressed specimens using $\beta$-SiC and $\alpha$-SiC powder with Al2O3 additive were studied. Beta-SiC powder was fully densified as 205$0^{\circ}C$, but $\alpha$-SiC powder was at 210$0^{\circ}C$. The maximum flexural strength and the fracture toughness of the specimen hot-pressed using $\beta$-SiC powder were 681 MPa and 6.7 MPa{{{{ SQRT {m } }}, and thosevalues of specimen hot-pressed using $\alpha$-SiC powder were 452 MPa and 4.7 MPa{{{{ SQRT {m } }}, respectively. The strength superiority of specimen hot-pressed using $\beta$-SiC powder was due to the finer grain size, and higher density. The higher toughness of specimen hot-pressed using $\beta$-SiC powder than $\alpha$-SiC powder than $\alpha$-SiC powder was due to the crack deflection mechanism arised from the difference of thermal expansion coefficient between $\alpha$ and $\beta$-SiC phases which were co-existed in the sintered body.

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Effect of Crack Closure on the Fatigue Crack Growth Behavior of Forged AI7050-T7452 (AI7050-T7452 단조재의 피로균열성장에 대한 균열닫힘의 영향)

  • Lee, W.S.;Park, J.Y.;Lee, H.W.
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.7
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    • pp.82-90
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    • 1997
  • When a structure is made by the process of forging, it has the different mechanical properties from those it has before the process. This study is based on the crack closure phenomenon of the crack growth behavior of forged AI7050-T7452. The specimens were prepared in three kinds of forging ratio in order to find out the effects of crack closure on the forged material and compare the crack growth behavior with not-forged aluminum. COD method and strain gage method were used in measuring the crack closure stress and the results from those methods were compared each other. FEM analysis was applied to verify the effective stress intensity factor range by the superposition of the crack closure load to the crack tip. In the result of this study, the crack closure stress decreased with increasing the forging ratio due to the finer grain size and the brittle manner.

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A Study on Heat Transfer in Sand Molds (사형(砂型)의 열전달(熱傳達)에 관(關)한 연구(硏究))

  • Lee, Jong-Nam;Kim, Kwang-Bea
    • Journal of Korea Foundry Society
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    • v.2 no.1
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    • pp.2-11
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    • 1982
  • In order to investigate the relationship between the thermal characteristics of the various molds as green sand mold, dry sand mold, $CO_2$ mold and shell mold, and the solidification characteristics of molten metal, the thermal analysis of rarious molds and melt were performed. The structure of Al-Castings was a/so observed. Results obtained in this experiment were as follows : 1) The heating rate of the molds was increased in the order of green sand mold, $CO_2$ mold, dry sand mold and shell mold, On the other hand the solidification time of the melts was shortened in the order of dry sand mold castings, $CO_2$ mold castings, green sand mold castings and shell mold castings. 2) The arrest temperature period in the heating curve of the green sand mold was resulted from the eraporation of moisture contained in mold, which was transfered to the outer side of the mold. 3) The temperature fluctuation of the melt in the shell mold was considered to be resulted from the combution heat of resin contained in the mold. 4) The amounts of heat absorption of the molds were increased in the order of dry sand mold, $CO_2$ mold, green sand mold and shell mold. 5) The higher the solidification rate was, the longer was its shrinkage pipe and the finer its grain size.

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Study of the Cheonripo Intertidal Beach Sands and Coastal Dune Sands, Cheonripo, the West Coast of Korea (한국 서해 천리포 사질 조간대 해빈층과 해안 사구층의 연구)

  • 박용안;최경식
    • The Korean Journal of Quaternary Research
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    • v.7 no.1
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    • pp.93-101
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    • 1993
  • A sedimentation study of the Cheonripo intertidal beach sands and its related coastal dune sands, Cheonripo, Seosan Gun, Choongcheong Namdo, Korea has been carried out based on a series of several summer time field surveys. Each subenvironment in the Cheonripo coastal zone, that is, intertidal sand beach and coastal sand dune, could be differenciated in terms of textural parameters. The coastal dune sands are finer than the intertidal beach sands in mean grain size, and the sorting of dune sands is relatively poorer than that of intertidal beach sands. However, the skewness of intertidal beach and dune sands is commonly positive. Such textural parameters are characteristically differentiated on scatter diagrams. A series of megaripple bedform observations for 6 tidal cycle periods(August 13, 14 and 15, 1990) are interpreted to find out migration pattern of bedforms and its related sand migration. Such migration natures are shown on the tables and figures.

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Structural Analyses and Properties of $Ti_{1-x}Al_xN$ Films Deposited by PACVD Using a $TiCl_4/AlCl_3/N_2/Ar/H_2$ Gas Mixture ($TiCl_4/AlCl_3/N_2/Ar/H_2$ 반응계를 사용하는 플라즈마화학증착법에 의한 $Ti_{1-x}Al_xN$ 박막의 구조분석 및 물성)

  • 김광호;이성호
    • Journal of the Korean Ceramic Society
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    • v.32 no.7
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    • pp.809-816
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    • 1995
  • Ti1-xAlxN films were successfully deposited on high speed steel and silicon wafer by plasma-assisted chemical vapor deposition using a TiCl4/AlCl3/N2/Ar/H2 gas mixture. Plasma process enabled N2 gas to nitride AlCl3, which is not possible in sense of thermodynamics. XPS analyses revealed that the deposited layer contained Al-N bond as well as Ti-N bond. Ti1-xAlxN films were polycrystalline and had single phase, B1-NaCl structure of TiN. Interplanar distance, d200, of (200) crystal plane of Ti1-xAlxN was, however, decreased with Al content, x. Al incorporation into TiN caused the grain size to be finer and changed strong (200) preferred orientation of TiN to random oriented microstructure. Those microstructural changes with Al addition resulted in the increase of micro-hardness of Ti1-xAlxN film up to 2800Kg/$\textrm{mm}^2$ compared with 1400Kg/$\textrm{mm}^2$ of TiN.

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Effect of Mo Addition on the Sinterability and Mechanical Properties of TiB$_2$-Fe Cermets (TiB$_2$-Fe 서메트의 소결성 및 기계적성질에 미치는 Mo첨가의 영향)

  • 최덕순
    • Journal of the Korean Ceramic Society
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    • v.36 no.5
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    • pp.471-477
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    • 1999
  • Fe and Fe-Mo binder were used to produce TiB2 based cermet by a pressureless sintering. The densification behaviour of TiB2-Fe-Mo cermet during liquid-phase sintering in argon was studied in relation to binder phase charactertics. The effects of Mo addition and sintering condition on the sintering behaviour and mechanical properties were also investigated. TiB2-based cermets with Fe-Mo binder composition showed a better sinterability than the cermets with only Fe binder. In TiB2-Fe-Mo cermet higher densities in the wide temperature range were obtained and also fully densified sintered cermet were obtained at 1873K The enhancement in the densification phenomenon of TiB2-Fe-Mo system can be explained by improved liquid phase wettability associated with the roles of Mo components as solute atoms. When Fe-Mo binders were used cermets with a finer grain size and enhanced mechanical properties wereproduced and new phases such as Fe2B and Mo2FeB2 were observed in the sintered cermet. The highest bending strength was obtained from the 20vol% Fe-Mo cermet and these hardness-fracture toughness combination in the wide binder compositions is better than that of TiB2-Fe cermet. In order to improve mechanical properties microstructure control with high purity powders is desirable because high purity powders prevent the formation of Fe2B and Mo2FeB2 phase which comsume the ductile binder phase.

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Effect of Microstructure on the Corrosion Resistance of Nd-Fe-B Permanent Magnets

  • Li, Jiajie;Li, Wei;Li, Anhua;Zhao, Rui;Lai, Bin;Zhu, Minggang
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.304-307
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    • 2011
  • High performance Nd-Fe-B magnets can be manufactured by both sintering and hot deformation. The corrosion behaviors of the magnets prepared by the two processes were compared. Effect of microstructure on the corrosion resistance of Nd-Fe-B magnets was also investigated. A neutral salt spray test (NSS) was performed for the different-processed magnets. The weight losses of the samples after the corrosion test were measured. The corrosion microstructures were observed using a scanning electron microscope. It shows that the corrosion resistance of hot deformed magnets is much better than that of the sintered ones because the grain size and the distribution of Nd-rich phases of the hot deformed magnets are much finer and more uniform than those of the sintered ones. The different microstructure between the sintered and the hot deformed magnets causes the different corrosion behavior.

The Electromagnetic Wave Absorption Characteristics of Cu-Ni-Zn Ferrite by Thermal Decomposition of Organic Acid Salt (유기산염 열분해법에 의한 Cu-Ni-Zn 페라이트의 전자파 흡수 특성)

  • 정재우;이완재
    • Journal of the Korean Magnetics Society
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    • v.5 no.6
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    • pp.947-951
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    • 1995
  • The electromagnetic interference is prevented by the high magnetic loss of the ferrite. The absorbing property of electromagnetic wave could be improved by the ferrite that has a finer and more uniform microstructure. The thermal decomposition of organic acid salt provided the uniform composition and fine powder. The absorbing properties of electromagnetic wave were evaluated by the relative complex permeability, permittivity, and the attenuation which is calculated from the results of network analyzer. The permeability and permittivity were increased with increase of the density and with decrease of the grain size. The matching thickness could be reduced with increasing sintered temperature. The attenuation of the Cu-Ni-Zn ferrite showed over 20dB when the matching thickness and the matching frequency range were 6.75mm and from 160MHz to 640MHz, respectively.

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