• 제목/요약/키워드: fine grain technique

검색결과 41건 처리시간 0.026초

A New Method of HTS Material Synthesis by Combination of MCA and SHS

  • Korobova, N.;Soh, Dea-Wha
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.2
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    • pp.1270-1273
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    • 2004
  • The combination of methane-chemical activation and Self-propagating High-temperature synthesis (SHS) has widened the possibilities for both methods. For YBCO systems the investigation showed that a short-term mechano-chemical activation of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors of YBCO composition with a grain size d < $1{\mu}m$ is developed. The specific feature of the technique is formation of the $YBa_2Cu_3O_{7-x}$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors (HTS) are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples investigated.

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Parallelizing Imperfectly Nested Loops

  • Kim, Ki-Chang
    • Journal of Electrical Engineering and information Science
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    • 제1권1호
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    • pp.140-150
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    • 1996
  • Loops are some of the richest program constructs where parallelism is available. Exploiting fine-grain parallelizm out these constructs is particularly important in light of the growing popularity of superscalar and VLIW machines. This paper explains how the fine-grain parallelization techniques can be generalized to handle nested loops. Our technique integrates nested loop parallelization techniques at the fine-grain level, thus exposing more fine-grain parallelism, and is flexible enough to handle non-perfectly nested loops. Examples and some experimental results are presented to illustrate our approach.

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Combination of Mechano-chemical Activation and SHS for HTS Material Synthesis

  • N. Korobova;Deawha Soh
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2004년도 SMICS 2004 International Symposium on Maritime and Communication Sciences
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    • pp.96-99
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    • 2004
  • The combination of mechano-chemical activation and Self-propagating High-temperature Synthesis (SHS) has widened the possibilities for both methods. For YBCO systems the investigation showed that a short-term mechano-chemical activation of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors of YBCO composition with a grain size d <1 ${\mu}{\textrm}{m}$ is developed. The specific feature of the technique is formation of the YBa$_2$Cu$_3$O$_{7-{\delta}}$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors (HTS) are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples.fine samples.

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Combination of MCA and SHS for Material Synthesis

  • Soh, Dea-Wha;N., Korobova
    • 동굴
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    • 제78호
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    • pp.1-8
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    • 2007
  • The combination of mechano-chemical activation (MCA)and Self-propagating High-temperature Synthesis (SHS) has widened the technical possibilities for both methods. For YBCO systems the investigation showed that a short-term MCA of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors (HTS) of YBCO composition with a grain size d <1m is developed using combination of MCA and SHS. The specific feature of the technique is formation of the $YBa_2Cu_3O_7-$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples.

Effect of grain refinement on the performance of AZ80 Mg alloys during wear and corrosion

  • Naik, Gajanan M;Gote, Gopal D.;Narendranath, S;Kumar, S.S. Satheesh
    • Advances in materials Research
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    • 제7권2호
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    • pp.105-118
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    • 2018
  • Magnesium and its alloys are attracted towards all engineering applications like automotive, marine, aerospace etc. due to its inherent high strength to weight ratio. But, extensive use of Mg alloys is limited to the current scenario because of low wear and corrosion resistance behavior. However, equal channel angular press is one of the severe plastic deformation technique which has been effective method to improve the wear and corrosion resistance by achieving fine grain structure. In this study, the effect of grain refinement on wear and corrosion resistance of AZ80 Mg alloys were investigated. The wear behavior of the coarse and fine-grained Mg alloys was examined through $L_9$ orthogonal array experiments in order to comprehend the wear behavior under varies control parameters. It was shown that ECAPed alloy increased the wear and corrosion resistance of the Mg alloy through the formation of fine grain and uniform distribution of secondary ${\beta}-phase$. Also, the performance of AZ80 Mg alloy for these changeswas discussed through SEM morphology.

감쇄기법(subtraction method)을 이용한 백제 무령왕릉 관련 전(塼)의 연대결정 (Age determination of bricks related to Muryong Royal Tomb of the Baekje Kingdom using subtraction method)

  • 김명진;송기웅;이찬희;장성윤;;홍덕균
    • 분석과학
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    • 제20권6호
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    • pp.508-515
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    • 2007
  • 감마선량율에 대한 정보를 얻을 수 없는 백제 무령왕릉 출토 전(塼)과 송산리 고분 출토 전, 부여 정동리 가마유구 출토 전에 대한 절대연대를 산출하였다. 연대측정은 전 시료로부터 석영을 추출하여 열 냉광(thermoluminescence)을 미립자법(fine grain technique)에 적용하여 얻은 결과와 광 자극 냉광(optically stimulated luminescence)을 조립자법(quartz inclusion technique)에 적용하여 얻은 결과를 감쇄기법(subtraction method)에 대입하여 수행하였다. 연대측정 결과 각 시료의 연대 오차는 모두 6 % 표준편차 이내로 매우 안정적이었으며, 산출된 연대측정치는 서로 오차범위 내에서 일치하였다. 최종적으로 이 연구를 통하여 결정된 백제 무령왕릉 관련 전의 연대는 AD $530{\pm}50yrs$ ($1{\sigma}$ SD)이었다.

다공질 소결체의 조직형성에 관한 컴퓨터 시뮬레이션 (Computer Simulation for Microstructure Development in Porous Sintered Compacts)

  • 신순기
    • 한국세라믹학회지
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    • 제43권4호
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    • pp.213-219
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    • 2006
  • A Monte Carlo simulation based on Potts model in a three dimensional lattice was studied to analyze and design microstructures in porous sintered compacts such as porosity, pore size, grain (particle) size and contiguity of grains. The effect of surface energy of particles and the content of additional fine particles to coarse particles on microstructure development were examined to obtain fundamentals for material design in porous materials. It has been found that the larger surface energy enhances sintering (necking) of particles and increases contiguity and surface energy does not change pore size and grain size. The addition of fine particles also enhances sintering of particles and increases contiguity, but it has an effect on increment of pore size and grain size. Such a simulation technique can give us important information or wisdom for design of porous materials, e.g., material system with high surface energy and fine particle audition are available for higher strength and larger porosity in porous sintered compacts with applications in an automobile.

나노표면 영역에서의 ECAP 변형된 알루미늄합금의 기계적 물성변화 측정 (Determination of Mechanical Properties of Equal Channel Angular Pressed Aluminum Alloys in Nano-surface Region)

  • 안성빈;김정석
    • 열처리공학회지
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    • 제32권3호
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    • pp.113-117
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    • 2019
  • The effects of severe plastic deformation and heat treatment on the mechanical properties of Al 5052 and 6005 alloys were investigated using the metallurgical technique and nano-indentation technique in nano-surface region. Equal channel angular pressing (ECAP) was used to apply severe plastic deformation to the aluminum alloys in order to obtain fine grain sized materials. The elastic modulus was measured and interpreted in relation to the metallurgical observation. The elastic modulus increased after ECAP process due to evolution of the fine grains. However, the elastic modulus decreased after heat treatment due to generation of coarsened precipitates on the grain boundaries.

소결방법에 따른 ZrB $_{2 }$ - ZrC 복합체에서의 결정립 방위 분포의 변화 (Grain orientation distribution of the ZrB $_{2 }$ - ZrCcomposite sintered by the different sintering technique)

  • 심승환;;;;오근호;심광보
    • 한국결정성장학회지
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    • 제10권2호
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    • pp.152-158
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    • 2000
  • 상압 소결법(PLS, pressureless sintering) 및 방전가열 소결법(SPS, spark plasma sintering)으로 소결한 {{{{ {ZrB }_{2 } - ZrC }}}} 복합체의 미세구조를 SEM-EBSP 법에 의해 결정기하학적으로 분석하였다. PLS법에 의해 소결된 복합체에서 {{{{ { ZrB}_{2 } }}}}의 (1010) 면은ND(시편에 수직인 방향)로 배향되었고, ZrC 경우 (101) 및 (111)면이 ND방향으로 배향되었다. 한편 SPS법에 위해 소결된 {{{{ { ZrB}_{2 } }}}}의 (0001)A면은 ND방향으로 강하게 배향되었다. ZrC인 경우 (001) 면만이 ND방향으로 배향되었다. PLS법에 의한 소결체의 결정립은 특정방위에 대해 약한 배향을 갖으면서, {{{{ { ZrB}_{2 } }}}}와 ZrC상 계면의 구조적 조화가 우수한 반면, SPS법에 의한 소결체의 결정립들은 특정방향으로 강하게 배향되는 경향을 보인다.

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Nanostructure Ceramics of Silicon Nitride Produced by Spark Plasma Sintering

  • Hojo, Junichi;Hotta, Mikinori
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.323-324
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    • 2006
  • The nanostructure control of $Si_3N_4$ ceramics can be achieved by using fine starting powder and retardation of grain growth. The spark plasma sintering technique is useful to retard the grain growth by rapid heating. In the present work, the change of microstructure was investigated with emphasis on the particle size of starting powder, the amount of sintering additive and the heating schedule. The rapid heating by spark plasma sintering gave the fine microstructure consisting of equiaxed grains with the same size as starting particles. The spark plasma sintering of $Si_3N_4$ fine powder was effective to control the microstrucutre on nano-meter level.

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