• Title/Summary/Keyword: fine grain technique

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A New Method of HTS Material Synthesis by Combination of MCA and SHS

  • Korobova, N.;Soh, Dea-Wha
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07b
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    • pp.1270-1273
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    • 2004
  • The combination of methane-chemical activation and Self-propagating High-temperature synthesis (SHS) has widened the possibilities for both methods. For YBCO systems the investigation showed that a short-term mechano-chemical activation of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors of YBCO composition with a grain size d < $1{\mu}m$ is developed. The specific feature of the technique is formation of the $YBa_2Cu_3O_{7-x}$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors (HTS) are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples investigated.

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Parallelizing Imperfectly Nested Loops

  • Kim, Ki-Chang
    • Journal of Electrical Engineering and information Science
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    • v.1 no.1
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    • pp.140-150
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    • 1996
  • Loops are some of the richest program constructs where parallelism is available. Exploiting fine-grain parallelizm out these constructs is particularly important in light of the growing popularity of superscalar and VLIW machines. This paper explains how the fine-grain parallelization techniques can be generalized to handle nested loops. Our technique integrates nested loop parallelization techniques at the fine-grain level, thus exposing more fine-grain parallelism, and is flexible enough to handle non-perfectly nested loops. Examples and some experimental results are presented to illustrate our approach.

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Combination of Mechano-chemical Activation and SHS for HTS Material Synthesis

  • N. Korobova;Deawha Soh
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2004.05a
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    • pp.96-99
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    • 2004
  • The combination of mechano-chemical activation and Self-propagating High-temperature Synthesis (SHS) has widened the possibilities for both methods. For YBCO systems the investigation showed that a short-term mechano-chemical activation of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors of YBCO composition with a grain size d <1 ${\mu}{\textrm}{m}$ is developed. The specific feature of the technique is formation of the YBa$_2$Cu$_3$O$_{7-{\delta}}$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors (HTS) are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples.fine samples.

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Combination of MCA and SHS for Material Synthesis

  • Soh, Dea-Wha;N., Korobova
    • Journal of the Speleological Society of Korea
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    • no.78
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    • pp.1-8
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    • 2007
  • The combination of mechano-chemical activation (MCA)and Self-propagating High-temperature Synthesis (SHS) has widened the technical possibilities for both methods. For YBCO systems the investigation showed that a short-term MCA of initial powders before SHS leads to single-phase and ultra-fine products. A new technique for preparation ultra-fine high-temperature superconductors (HTS) of YBCO composition with a grain size d <1m is developed using combination of MCA and SHS. The specific feature of the technique is formation of the $YBa_2Cu_3O_7-$ crystalline lattice directly from an X-ray amorphous state arising as a result of mechanical activation of the original oxide mixture. The technique allows the stage of formation of any intermediate reaction products to be ruled out. X-ray and magnetic studies of ultra-fine high temperature superconductors are carried out. Dimension effects associated with the microstructure peculiarities are revealed. A considerable enhancement of inter-grain critical currents is found to take place in the ultra-fine samples.

Effect of grain refinement on the performance of AZ80 Mg alloys during wear and corrosion

  • Naik, Gajanan M;Gote, Gopal D.;Narendranath, S;Kumar, S.S. Satheesh
    • Advances in materials Research
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    • v.7 no.2
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    • pp.105-118
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    • 2018
  • Magnesium and its alloys are attracted towards all engineering applications like automotive, marine, aerospace etc. due to its inherent high strength to weight ratio. But, extensive use of Mg alloys is limited to the current scenario because of low wear and corrosion resistance behavior. However, equal channel angular press is one of the severe plastic deformation technique which has been effective method to improve the wear and corrosion resistance by achieving fine grain structure. In this study, the effect of grain refinement on wear and corrosion resistance of AZ80 Mg alloys were investigated. The wear behavior of the coarse and fine-grained Mg alloys was examined through $L_9$ orthogonal array experiments in order to comprehend the wear behavior under varies control parameters. It was shown that ECAPed alloy increased the wear and corrosion resistance of the Mg alloy through the formation of fine grain and uniform distribution of secondary ${\beta}-phase$. Also, the performance of AZ80 Mg alloy for these changeswas discussed through SEM morphology.

Age determination of bricks related to Muryong Royal Tomb of the Baekje Kingdom using subtraction method (감쇄기법(subtraction method)을 이용한 백제 무령왕릉 관련 전(塼)의 연대결정)

  • Kim, Myung-Jin;Song, Ki-Woung;Lee, Chan-Hee;Jang, Sung-Yoon;Takashima, Isao;Hong, Duk-Geun
    • Analytical Science and Technology
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    • v.20 no.6
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    • pp.508-515
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    • 2007
  • Age determination was carried out with the bricks relating to Muryong Royal Tomb of the Baekje Kingdom, for which there is no information on the external gamma dose rate, by using the subtraction method of luminescence dating. In the subtraction method, each paleodose for fine grain and for quartz inclusion is required for the sample to be dated. In this study, the paleodose for the fine grain was estimated by thermoluminescence measurement and the paleodose for the quartz inclusion was determined using optically stimulated luminescence. The resultant ages among the bricks showed good agreement with standard deviation of 6 % error. Finally the bricks relating to Muryong Royal Tomb were evaluated as AD $530{\pm}50yrs$($1{\sigma}$ SD).

Computer Simulation for Microstructure Development in Porous Sintered Compacts (다공질 소결체의 조직형성에 관한 컴퓨터 시뮬레이션)

  • Shin, Soon-Ki;Matsubara, Hideaki
    • Journal of the Korean Ceramic Society
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    • v.43 no.4 s.287
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    • pp.213-219
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    • 2006
  • A Monte Carlo simulation based on Potts model in a three dimensional lattice was studied to analyze and design microstructures in porous sintered compacts such as porosity, pore size, grain (particle) size and contiguity of grains. The effect of surface energy of particles and the content of additional fine particles to coarse particles on microstructure development were examined to obtain fundamentals for material design in porous materials. It has been found that the larger surface energy enhances sintering (necking) of particles and increases contiguity and surface energy does not change pore size and grain size. The addition of fine particles also enhances sintering of particles and increases contiguity, but it has an effect on increment of pore size and grain size. Such a simulation technique can give us important information or wisdom for design of porous materials, e.g., material system with high surface energy and fine particle audition are available for higher strength and larger porosity in porous sintered compacts with applications in an automobile.

Determination of Mechanical Properties of Equal Channel Angular Pressed Aluminum Alloys in Nano-surface Region (나노표면 영역에서의 ECAP 변형된 알루미늄합금의 기계적 물성변화 측정)

  • An, SeongBin;Kim, ChungSeok
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.3
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    • pp.113-117
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    • 2019
  • The effects of severe plastic deformation and heat treatment on the mechanical properties of Al 5052 and 6005 alloys were investigated using the metallurgical technique and nano-indentation technique in nano-surface region. Equal channel angular pressing (ECAP) was used to apply severe plastic deformation to the aluminum alloys in order to obtain fine grain sized materials. The elastic modulus was measured and interpreted in relation to the metallurgical observation. The elastic modulus increased after ECAP process due to evolution of the fine grains. However, the elastic modulus decreased after heat treatment due to generation of coarsened precipitates on the grain boundaries.

Grain orientation distribution of the ZrB $_{2 }$ - ZrCcomposite sintered by the different sintering technique (소결방법에 따른 ZrB $_{2 }$ - ZrC 복합체에서의 결정립 방위 분포의 변화)

  • ;Y. Yasutomi;Y. Takigawa;H. Yanagida
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.2
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    • pp.152-158
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    • 2000
  • The crystallographic grain orientation of {{{{ { ZrB}_{2 } }}}}-ZrC composite sintered by pressureless a sintering(PLS) and spark plasma sintering (SPS) was analysed by the SEM-EBSP technique. In the case of PLS, (160) plane of {{{{ { ZrB}_{2 } }}}} was oriented to ND direction, (101) and (111) plane of ZrC were oriented to ND direction. In the case of SPS, (0001) plane of {{{{ { ZrB}_{2 } }}}} was strongly oriented to ND direction. Only (001) plane of ZrC was oriented to ND direction. The PLS specimen had weakly oriented grain structure and interface between {{{{ { ZrB}_{2 } }}}} and ZrC was found to be more stable than that of SPS but the SPS specimen had a preferentially oriented grain structure.

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Nanostructure Ceramics of Silicon Nitride Produced by Spark Plasma Sintering

  • Hojo, Junichi;Hotta, Mikinori
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.323-324
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    • 2006
  • The nanostructure control of $Si_3N_4$ ceramics can be achieved by using fine starting powder and retardation of grain growth. The spark plasma sintering technique is useful to retard the grain growth by rapid heating. In the present work, the change of microstructure was investigated with emphasis on the particle size of starting powder, the amount of sintering additive and the heating schedule. The rapid heating by spark plasma sintering gave the fine microstructure consisting of equiaxed grains with the same size as starting particles. The spark plasma sintering of $Si_3N_4$ fine powder was effective to control the microstrucutre on nano-meter level.

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