• Carbon letters
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• 제12권1호
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• pp.26-30
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• 2011

For polyacrylonitrile (PAN) based carbon fiber (CF) process, we developed a lab scale wet spinning line and a continuous tailor-made stabilization system with ten columns for controlling temperature profile. PAN precursor was spun with a different spinning rate. PAN spun fibers were stabilized with a total duration of 45 to 110 min at a given temperature profile. Furthermore, a stabilization temperature profile was varied with the last column temperature from 230 to $275^{\circ}C$. Stabilized fibers were carbonized in nitrogen atmosphere at $1200^{\circ}C$ in a furnace. Morphologies of spun and CFs were observed using optical and scanning electron microscopy, respectively. Tensile properties of resulting CFs were measured. The results revealed that process conditions such as spinning rate, stabilization time, and temperature profile affect microstructure and tensile properties of CFs significantly.

• 한국염색가공학회지
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• 제35권4호
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• pp.239-245
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• 2023

Cellulose is an abundant biodegradable material in nature with excellent properties, but due to its poor processability, it has been widely studied for processing through modification. Cellulose acetate propionate (CAP) is a cellulose derivative in which the hydroxyl group of cellulose is replaced by acetyl and propionyl groups. CAP has several advantages, such as excellent solubility, structural stability, light and weather resistance, and good transparency. Porous nanofibers with excellent specific surface area, which can be applied in various fields, can be easily formed by the phase separation method using highly volatile solvents. High speed centrifugal spinning is a nano/micro fiber preparation method with advantages such as fast spinning and easy alignment control. In this study, a CAP/polybutylene succinate (PBS) spinning solution with chloroform as solvent was prepared to prepare porous microfibers and the fiber morphology was examined as a function of the disk rotation speed in an high speed centrifugal spinning device.

• 한국세라믹학회지
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• 제42권8호
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• pp.593-598
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• 2005

Polycarbosilane was synthesized by the Kumada rearrangement of polydimethylsilane in the presence of zeolite (ZSM-5) as a catalyst at $350^{\circ}C$. The prepared polycarbosilane had very low molecular weight ($M_w=500$), so that it was not suitable to fabricate SiC fiber by melt spinning. Further polymerization of PCS was conducted around $400^{\circ}C$ to obtain spinnable polycarbosilane. After polymerization, the polycarbosilanes were isolated by distillation according to the molecular weight distributions. The PCS with a controlled molecular weight distribution was spun into continuous polycarbosilane green fibers. The PCS green fiber was successfully transformed into silicon oxycarbide fiber. The room temperature strength of the SiC fiber was around 1.5 - 1.8 GPa. The oxidation behavior and the tensile strength after oxidation were also evaluated.

• 한국의류학회지
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• 제30권4호
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• pp.607-614
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• 2006

This study was carried out to suggest the optimal spinning process condition which provides a proper range of tenacity and biodegradability as textile fibers. The effects of the melt spinning speed and heat treatment on the mechanical property and biodegradability of polylactic acid fiber were investigated. Polylactic acid(PLA) was spun in a high spinning speed of $2000{\sim}4000m/min$. Each specimen was heat-treated at $100^{\circ}C$ during 30min. Mechanical properties such as breaking stress and the degree of crystallinity were evaluated using WAXS. Biodegradability was estimated from the decrease of breaking stress, weight loss, and the degree of crystallinity after soil burial. Experimental results revealed that heat treated specimens showed higher breaking stress than untreated specimens, but the increase was not so high as was expected from the remarkable change of crystallinity by heat treatment. It was concluded that breaking stress was more influenced by spinning speed than heat treatment. In the soil burial test, however biodegradability calculated from weight loss was more influenced by heat treatment than spinning speed.

• 대한화학회지
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• 제57권2호
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• pp.289-294
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• 2013

• 정보처리학회논문지:소프트웨어 및 데이터공학
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• 제11권12호
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• pp.489-498
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• 2022

최근 노동 집약적인 성격의 섬유 산업에서는 인공지능을 통해 섬유 방사 공정에 들어가는 비용을 줄이고 품질을 최적화하려고 시도 하고 있다. 그러나 섬유 방사 공정은 데이터 수집에 필요한 비용이 크고 체계적인 데이터 수집 및 처리 시스템이 부족하여 축적된 데이터양이 적다. 또 방사 목적에 따라 특정한 변수에만 변화를 준 데이터만을 우선으로 수집하여 데이터 불균형이 발생하며, 물성 측정 환경의 차이로 인해 동일 방사 조건에서 수집된 샘플 간에도 오차가 존재한다. 이러한 데이터 특성들을 고려하지 않고 인공지능 모델에 활용할 경우 과적합과 성능 저하 등의 문제가 발생할 수 있다. 따라서 본 논문에서는 방사 공정 데이터 특성을 고려한 이상치 처리 기법과 데이터 증강 기법을 제안한다. 그리고 이를 기존 이상치 처리 기법 및 데이터 증강 기법과 비교하여 제안한 기법이 방사 공정 데이터에 더 적합함을 보인다. 또 원본 데이터와 제안한 기법들로 처리된 데이터를 다양한 모델에 적용하여 비교함을 통해 제안한 기법들을 사용한 모델들이 그렇지 않은 모델들에 비해 인장 강신도 예측 모델의 성능이 개선됨을 보인다.

• 한국항해학회지
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• 제18권4호
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• pp.171-178
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• 1994

Fiber optic gyroscopes must be a promising technology that can replace conventional mechanical ones based on the principle of inertia of spinning masses. The advantages of fiber optic gyroscopes over mechanical ones include low cost, light weight, compact size and fast turn-on time. We will apply them to fiber optic gyrocompass for ships. Fiber optic gyrocompass for ships requires the north-seeking accuracy of $15^{\circ}$/hr, earth rotation rate, or better. This article introduces the fiber optic gyroscope as rotation sensor in the fiber optic gyrocompass system for ships that is planed to develop in our laboratory.

• Journal of Plant Biotechnology
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• 제49권3호
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• pp.257-270
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• 2022

The aim of this work was to prepare a new biodegradable polyhydroxybutyrate (PHB) submicron fiber mat loaded with hypericin-rich Hypericum perforatum raw extract by centrifugal spinning technology, an alternative approach to the traditional method of electrospinning to fabricate nanofibers or microfibers from solutions at high speed and low cost. Hypericins in methanol/acetone extract of H. perforatum were determined by UHPLC-MS/MS and HPLC/PDA. Submicron fiber mats composed of pure PHB or PHB enriched with H. perforatum extract were prepared using a pilot plant demonstrator for the centrifugal spinning technology and characterized by SEM. Singlet oxygen production was quantified by the 1,3-diphenylisobenzofuran (DPIBF) method in hexane. The results proved a significant production of singlet oxygen by the prepared submicron fiber mat. We also found a significant antibacterial activity against the bacterial strain Escherichia coli CCM 5417 by a method in accordance with JIS Z 2801/ISO 22196 standards. The H. perforatum extract-enriched PHB submicron fiber mats showed potential for the development of self-cleaning and antimicrobial air filters.

• Fibers and Polymers
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• 제7권4호
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• pp.432-435
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• 2006

High Modulus and high tenacity polypropylene fibers have been prepared by drawing on a gradient heater. Results show that fiber properties are significantly affected by temperature profiles of final stage drawing on a gradient heater. The gradient drawn filaments showed superior mechanical properties when compared to filaments drawn over a constant temperature heater. Fibers with initial modulus of 16.4 GPa and tenacity of 670 MPa have been manufactured in the process. The nature of the gradient drawing had a significant effect on end properties. The superior mechanical properties are attributed to the high crystal perfection and crystallinity and low void fractions obtained at high draw ratios when drawn over a gradient heater.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2006년도 추계학술대회
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• pp.471-473
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• 2006

An object of the present study is to provide a hollow fiber membrane humidifier capable of improving the humidification efficiency while lowering the pressure loss, and is suitably usable for PEMFC(Polymer Electrolyte Membrane Fuel Cell). The performance of PEMFC is decisively dependent on the humidity of the electrolyte membrane(fluorinated membrane) and a humidifier plays an important role in moisturizing electrolyte membrane. Especially this humidifier is adaptable for lower price to promote the commercialization of fuel cell vehicles and is passive type to be power free and to be volumetrically optimized. In this research, we propose the substitutes for the expensive fluorinated materials and the optimum dry-jet wet spinning conditions of hollow fiber membrane to get the fuel cell humidifier. In addition to that we established the standard method of evaluating the moisturizing performance of the humidifier of various materials.