• 한국염색가공학회지
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• 제28권4호
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• pp.231-238
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• 2016

We investigated the evolution of crystal formation as a function of drawing ratio in poly(1,4-diaminobutane-co-adipic acid-co-${\varepsilon}$-caprolactam-co-diethylenetriamine)(nylon 466T) copolymer formed by four monomers, i.e 1,4-diaminobutane, adipic acid, ${\varepsilon}$-caprolactam, diethylenetriamine(DETA), using synchrotron X-ray scattering measurement. In case of pristine(as spun) nylon 466T fiber, it was consisted with unoriented nylon $6{\alpha}$ and unoriented nylon $46{\alpha}$ phases. As increase the drawing ratio, unoriented nylon $6{\alpha}$ was transformed to oriented ${\gamma}$ phase, while unoriented nylon $46{\alpha}$ changed to oriented $46{\alpha}$ phase. The effect of the addition of DETA was not observed in the pristine fibers. However, DETA affected to restrict the formation of crystals at the maximum drawing condition, and as a result it had a role to increase the moisture regain.

• 한국세라믹학회지
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• 제32권1호
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• pp.17-24
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• 1995

The TEA complex polymeric sol was prepared by the alkoxide sol-gel method. The purpsoe of this experiment was to vefity the particle shape in the sol from the investigation of the rheological properties. TEA retarded hydrolysis rate by the reaction with alkoxide enough to make a stable transparent sol in the wide range of composition. From the results of the viscosity change with time, the optimum mole ratio for spinning was selected as 0.5 mole of TEA, 3 mole of H2O and the optimum viscosity was 104 cPs. The rheological behavior of the sol showed that the particle shape in the sol was linear, which was adequate for fiber drawing.

• 반도체디스플레이기술학회지
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• 제18권3호
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• pp.12-18
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• 2019

The protective double layer polymer coatings on silica optical fibers are realized by wet-on-wet liquid coating process and they play an important role in final quality of mass produced optical fibers. This numerical study aims to analyze the effects of secondary coating die design parameters by employing two dimensional axisymmetric model of coating cup and coating die geometry and computational fluid dynamics simulations which include temperature dependent viscosity of polymer coating liquids and viscous dissipation heating. Under high speed fiber drawing conditions and pressurized coating liquid supply, the effects of converging die angle are investigated in order to appreciate the change of coating liquid flow patterns such as flow recirculation zone near coating die as well as primary and secondary coating layer thicknesses. The auxiliary coating die to converging coating die is also tested and the results find that this concept is advantageous in achieving stable double layer coatings on silica glass fiber.

• 한국재료학회지
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• 제30권6호
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• pp.308-314
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• 2020

A commercial AA1070 alloy for electrical wire is severely deformed by drawing process in which a rod with an initial diameter of 9mm into is reduced to a wire of 2mm diameter. The drawn AA1070 wire is then annealed at various temperatures from 200 to 450 ℃ for 2h. Changes in microstructure, mechanical properties and electrical properties of the specimens with annealing temperature are investigated in detail. The specimen begins partially to recrystallize at 250 ℃; above 300 ℃ it is covered with equiaxed recrystallized grains over all regions. Fiber textures of {110}<111> and {112}<111> components are mainly developed, and {110}<001> texture is partially developed as well. The tensile strength tends to decrease with annealing temperature due to the occurrence of recovery or/and recrystallization. On the other hand, the elongation of the annealed wire increases with the annealing temperature, and reaches a maximum value of 33.3 % at 300 ℃. Electric conductivity of the specimens increases with annealing temperature, and reaches a maximum value of 62.6 %IACS after annealing at 450 ℃. These results are discussed in comparison with those for the other aluminum alloy.

• 한국세라믹학회지
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• 제39권12호
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• pp.1158-1163
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• 2002

2차 비선형 광특성을 유도하기 위한 UV 폴링용 Ge와 B가 첨가된 광민감성 광섬유를 제조하였다. 248 nm KrF 엑시머 레이저 조사에 의하여 수소처리 없이 장주기 격자를 형성할 수 있었다. 116 mJ/$cm^2$의 펄스 에너지와 10 Hz의 조사 빈도로 1분간 광민감성 광섬유에 레이저를 조사할 경우 -4 dB의 큰 band rejection 특성을 얻을 수 있었다. 제조된 광섬유의 광민감성은 장주기 격자쌍 방법을 이용하여 측정하였으며, 8.67 kJ/$cm^2$의 fluence로 KrF 엑시머 레이저를 조사할 경우 3.3${\times}10^{-3}$의 큰 코어 굴절률 변화를 얻었다. 또한 UV 폴링 시에 광섬유 코어에 고전압을 쉽게 인가할 수 있는 H자 형상의 광섬유를 인출조건의 최적호를 통하여 제조하였다.

• Fibers and Polymers
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• 제7권4호
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• pp.420-423
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• 2006

Spandex has been successfully applied on modified worsted spinning system to produce spandex core spun yam. However it's difficult to produce wool/spandex core-spun yam on woolen spinning system with the same modified device because the drafting device of the two systems is quite different. A new method is introduced to apply spandex on woolen spinning system in this paper. Core-spun yam produced in this way has good appearance and quality by comparing with normal yam. A series of experiments were carried out to study the influence of spandex drafting ratio and yam twist factor on tensile' properties and elasticity of core-spun yams. The results indicate that core-spun yam with spandex drawing ratio of 2.5 and twist factor of 13.63 has highest value of tenacity and breaking elongation.

• 한국공작기계학회논문집
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• 제17권2호
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• pp.77-82
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• 2008

Rubbing-roller is used for manufacturing liquid crystal display, and static displacement of the rubbing-roller becomes bigger as length of the rubbing roller made of aluminum is getting longer. Therefore, material of the rubbing-roller is changed from aluminum to CFRP(Carbon Fiber Reinforced plastic). Recently thermal spraying is applied to manufacturing process of long rubbing-roller. The thermal spraying has disadvantages such as increment of manufacturing time and fraction defective caused by density of stainless steel particle. In this study, fitting process by drawing was suggested and FEM analysis with Tsai-Wu failure theory and fitting experiments are carried out to find adequate shrink allowance. The suggested shrink allowance gives proper adhesive force, and CFRP failure is not occurred. Furthermore, the fitting process is applied to long rubbing-roller and availability of the fitting process is studied by measurement of roundness, straightness and shear strength.

• 한국재료학회지
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• 제15권1호
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• pp.37-41
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• 2005

Stainless steel fibers with a diameter of $17\;{\mu}m$ and 630 nm were produced from stainless steel wires by the drawing/annealing/exfolitation process. The suitable sheath material to draw the core stainless steel wires to fibers was the Cu coating. The low melting metal of Zn was not a suitable sheath coating. Also, an attempt was made to produce $20\;{\mu}m{\Phi}Ti$ fibers from the core titanium wires. The main obstacles in producing Ti fibers were their resistance to deformation owing to the Ti's hop structure, and high reactivity of Ti with the exfolitation solution.

• 한국염색가공학회지
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• 제35권3호
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• pp.169-178
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• 2023

The extended use of polyester nowadays has increased the amount of waste polyester (PET) released into the environment. Although these materials don't directly harm living things or the ecosystem, their inability to biodegrade remains one of the major global threats, driving up the amount of solid waste made up of PET. Environmental concerns have approved an increasing interest in recycled PET however the production of recycled PET with sufficient mechanical properties is still a challenge. Recycled Polyester (rPET) yarns are inexpensive and have the potential to acquire better mechanical characteristics through physical treatments, particularly by using technically simple method like uniaxial drawing. This study inspected the drawn behavior of virgin PET yarns and rPET yarns under various drawing parameters by first analyzing the initial material characteristics of both yarn. The impact of stretching on mechanical and morphological properties was also investigated. The results showed that virgin PET has better properties than rPET yarn; however, mechanical properties resembling virgin PET are achieved after optimizing the draw ratio.

• 한국세라믹학회지
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• 제29권7호
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• pp.544-550
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• 1992

Zirconia gel fibers could be made by drawing from polyester sol containing zirconyl oxychloride during the reaction between ethylen glycol and citric acid. In this case, the critical mole ratio of zirconyl oxychloride to citric acid was about 4 and by adding CaCl2 and calcining the gel fiber in the air, cubic stabilized zirconia fibers having much micropores at surface could be obtained.