• Title/Summary/Keyword: eutectic

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Microstructure investigation of iron artifacts excavated from Kkonmoe relic located in Suwon-si (수원시 꽃뫼 유적 출토 철제유물의 미세조직 분석)

  • Yu, Jae-Eun;Go, Hyeong-Sun;Lee, Jae-Sung
    • 보존과학연구
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    • s.23
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    • pp.131-147
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    • 2002
  • Kkonmoe relic located in Jangan-gu, Suwon-si, Gyeonggi-do Provinceis an example of the wide chronology from the Three Kingdoms Period to Joseon Dynasty. Examinations on a forged iron ax, a cast iron ax and an iron sickle excavated from this relic revealed the microstructure structure of the metal and the manufacturing technologies. Microstructure investigation was carried out with a metallurgical microscope and a Vickers hardness tester was used to measure the hardness of the micro structures. The test results show that the forged iron ax has a ferrite and pearlitestructure. It is made of low carbon steel and then carbonized to increase carbon content. After carbonization, the surface grains are reworked and the surface decarbonized. In case of the iron sickle, it is forged from low carbon steel, then carbonized and hardened, to increase overall strength. The sickle blade is carbonized and quenched after forging, resulting in afirm, solid blade. Heat treatment to remove brittleness is not applied to the cast ironartifact, which is manufactured by solidifing hypo-eutectic cast iron with a3-4% carbon content and white cast iron. All artifacts are produced from steel and subjected to a carbonization process. To increase hardness of the blade, additional heat treatment is applied.

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Correlation between rare earth elements in the chemical interactions of HT9 cladding

  • Lee, Eun Byul;Lee, Byoung Oon;Shim, Woo-Yong;Kim, Jun Hwan
    • Nuclear Engineering and Technology
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    • v.50 no.6
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    • pp.915-922
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    • 2018
  • Metallic fuel has been considered for sodium-cooled fast reactors because it can maximize the uranium resources. It generates rare earth elements as fission products, where it is reported by aggravating the fuel-cladding chemical interaction at the operating temperature. Rare earth elements form a multicomponent alloy (Ce-Nd-Pr-La-Sm-etc.) during reactor operation, where it shows a higher reaction thickness than a single element. Experiments have been carried out by simplifying multicomponent alloys for mono or binary systems because complex alloys have difficulty in the analysis. In previous experiments, xCe-yNd was fabricated with two elements, Ce and Nd, which have a major effect on the fuel-cladding chemical interaction, and the thickness of the reaction layer reached maximum when the rare earth elements ratio was 1:1. The objective of this study is to evaluate the effect and relationship of rare earth elements on such synergistic behavior. Single and binary rare earth model alloys were prepared by selecting five rare earth elements (Ce, Nd, Pr, La, and Sm). In the single system, Nd and Pr behaviors were close to diffusion, and Ce showed a eutectic reaction. In the binary system, Ce and Sm further increased the reaction layer, and La showed a non-synergy effect.

Compression D/B for Liquid Segregation Control in Semi-Solid Forming Process and Its Application (반용융 성형공정에 있어서 액상편석제어를 위한 압축 D/B 및 응용)

  • 정경득
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.06a
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    • pp.15-32
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    • 1999
  • A relationship between stress and stain is very important to design a die to avoid defects of products during semi-solid forming process. Since the liquid will be of eutectic composition in alloys liquid segregation will result in significant or undesirable situation. The materials used in this experiment are A 357. A390, Al2024 alloys that is fabricated by the electro-magnetic stirring process from Pechiney in France. The compression test was performed by induction heating equipment and MTS. In order to prevent the liquid segregation these measured temperature would be useful to control of strain rate during compression test. The liquid segregation is controlled as change of the strain rate and solid fraction during the compression process, The characteristics of flow between solid and liquid phase considering liquid segregation is examined through the above experiments. In the case of medium and high volume fractions of solid the distribution of strain rate is calculated by using compression test data of semi-solid materials (SSM). The thixoforming experiments with the designed die are carried out successfully. The die filling patterns of SSM for variation of die temperature and pressing force have been investigated. The hardness of the thixoformed scroll products is evaluated in terms of the microstructure for each position.

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A Study on the Production of a Compressor Piston for an Automobile Air-Conditioner using Aluminum casting/Forging (알루미늄 주조/단조 공정을 이용한 자동차용 에어컨 컴프레서 피스톤의 생산에 관한 연구)

  • Lee, Sung-Mo;Wang, Shin-Il;Kim, Hyo-Ryang;Bae, Won-Byong
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.8
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    • pp.53-59
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    • 2000
  • In this study aluminum casting experiments are carried out to reduce the grain size of a cast preform and to spheriodize its dendritic structure by adding Ti+B and Zr and to modify flaked eutectic silicon by adding Sr, And a finite element simulation is performed to determine an optimal configuration of the cast preform to be used in forging of a compressor piston for an automobile air-conditioner. When 0.15% Ti+B Zr and 0.05% Sr are added respectively into the molten aluminum alloy the finest grain in casting of the preform is obtained. It is confirmed that the optimal configuration of the cast preform predicted by FEM simulation is very useful for forging the compressor piston. After forging the cast preform of the compressor piston. the microstructure and the hardness of the cast preform is compared with those of the cast/forged product.

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Effects of Alloying Elements on the Damping Capacities and Mechanical Properties in 3.9%C Gray Cast Iron (3.9%C 회주철의 진동감쇠능 및 기계적 성질에 미치는 합금원소 첨가의 영향)

  • Kim, J.C.;Son, Y.C.;Han, D.W.;Baik, S.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.1
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    • pp.47-54
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    • 1997
  • Flake graphite cast irons with the high damping capacity have been used for the control of vibration and noise occuring in the members of various mechanical structures under vibrating conditions. However, the damping capacity which is morphological characteristics of graphite is one of the important factors in reducing the vibration and noise, but hardly any work has deal with this problem. Therefore, the authors have examined the damping capacity of various cast irons with alloying elements and studied the influences of the matrix, mechanical properties and morphological characteristics of graphite. The main results obtained are as follows: Effects of Ni on the damping capacities and mechanical properties are investigated in 3.9%C-0.3% Cu gray cast iron. At 0.2% Ni content, specific damping capacity showed the maximum value, and decreased with further increase in Ni content, Graphite continuity also showed same behavior. This indicates that the specific damping capacity has a close relation with graphite continuity. On the other hand, the damping capacity in pearlite matrix showed superior to that in ferrite. In contrast, with increasing the Ni content, both tensile strength and hardness increased due to the decrease of graphite length and eutectic cell size.

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Microstructural Feature of Discontinuous Precipitates Formed by Furnace Cooling in AZ91 Magnesium Alloy (AZ91 마그네슘 합금에서 노냉으로 생성된 불연속 석출물의 미세조직 특징)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.5
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    • pp.231-236
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    • 2018
  • The purpose of this study was to investigate the microstructural characteristics and hardness distribution of AZ91 magnesium alloy furnace-cooled to room temperature after solution treatment, and to compare the results with those of as-cast condition. The as-cast alloy showed a partially divorced eutectic ${\beta}(Mg_{17}Al_{12})$ phase and discontinuous precipitates (DPs) with a lamellar morphology, while only DPs were observed in the furnace-cooled alloy. The DPs in the furnace-cooled AZ91 alloy had various apparent interlamellar spacings, which would be ascribed to the different transformation temperatures during the furnace cooling. The average hardness for the furnace-cooled alloy is similar to that for the as-cast alloy. It is interesting to note that the hardness values of the furnace-cooled alloy were distributed over a narrower range than those of the as-cast alloy. This is likely to be caused by the relatively more homogeneous microstructure of the furnace-cooled alloy in comparison with the ascast one.

Effects of EMLA Cream in Intradermal Skin Test of Ampicillin Sodium Antibiotics (EMLA 크림이 ampicillin sodium 항생제 피내반응검사에 미치는 효과)

  • Kim, Jin;Kang, Hee-Young
    • Journal of Korean Academy of Fundamentals of Nursing
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    • v.18 no.1
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    • pp.46-53
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    • 2011
  • Purpose: The purpose of this study was to identify the effects of EMLA cream (eutectic mixture of local anesthetics, lidocaine and prilocaine) on pain during ampicillin sodium intradermal (ID) skin test, and also to assess skin reaction after the skin test. Methods: Forty-three nurse-volunteers had skin tests with 0.01ml-0.05ml ampicillin sodium antibiotics. Skin tests were done on each forearm to compare the pain level of the skin test site after application of EMLA cream with the pain level when no EMLA cream was applied. EMLA cream was applied at the ID skin test site with an occlusive dressing for one hour. Pain was evaluated using a visual analogue scale and pain sensation using the short form McGill Pain Questionnaire. The transverse diameter of the wheal and redness was read right after and at 15 minutes after the skin test. The results were compared using independent t-tests. Results: Pain score and sensation with EMLA cream treatment were significantly lower than when EMLA cream was not applied. There was no difference in skin reactions; reading of the skin test was not affected by EMLA cream. Conclusions: EMLA cream was found to be an effective local anesthetic to relieve the pain of clients having ampicillin sodium antibiotics ID skin tests.

Effect of TiC and AlN on the Wear Behavior and Mechanical Properties of Hypereutectic Al-Si Alloys (과공정 Al-Si 합금의 마모 거동과 기계적 성질에 미치는 TiC와 AlN의 영향)

  • Ju, Seung Hwan;Choi, Jin Myung;Kim, Yong Jin;Park, Ik Min;Park, Yong Ho
    • Korean Journal of Metals and Materials
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    • v.48 no.11
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    • pp.1003-1008
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    • 2010
  • In this study, the effect of the reinforcement on the wear behaviour and mechanical properties of hypereutectic Al-Si alloys was investigated. The Gas atomized hypereutectic Al-20Si alloy powders were mixed with 1, 3, and 5 wt.% AlN and TiC ceramic particles and consolidated by hotpress. The Al-20Si powder has both finely dispersed primary Si phases and eutectic structures. The Al-20Si-AlN, TiC composites showed that the reinforcements were distributed along the boundary of the Al-20Si alloy. The UTS increased with increasing the AlN, TiC contents. At a lower load, with an increasing weight fraction of reinforcements, the wear rate decreased in both composites and the wear mechanism was adhesive wear. At a higher load, the shape of the debris changes the mechanism of the AlN composites to abrasive-adhesion wear and this resulted in an increase of the wear rate.

Mechanically Workable High-strength Cu-Zr Composite (소성가공이 가능한 고강도 Cu-Zr 복합재료)

  • Shin, Sang-Soo;Lim, Kyung-Mook;Kim, Eok-Soo;Lee, Jae-Chul
    • Korean Journal of Metals and Materials
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    • v.50 no.4
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    • pp.293-299
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    • 2012
  • Ultrafine-grained or nanostructured alloys usually lack the strain hardening capability needed to sustain uniform tensile deformation under high stresses. To circumvent this problem, we fabricated the Cu-based composite reinforced with the 3-dimensionally interconnected $Cu_5Zr$ phase using the combined technique of rapid quenching and subsequent hot-rolling. The alloy exhibited a tensile ductility of ~2.5% together with a strength of 1.57 GPa, which exceeds the values of most commercially available Cu-Be alloys. In this study, we elucidated the structural origin of the high strength and tensile ductility of the developed alloy by examining the thermal stability of the $Cu_5Zr$ reinforcing phase and the energy (work) absorption capability of the Cu matrix.

Damping Capacities of Mg-Al alloy with As-Cast and Discontinuous Precipitates Microstructures (주조 및 불연속 석출물 미세조직을 가지는 Mg-Al 합금의 진동감쇠능)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.5
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    • pp.218-225
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    • 2021
  • In this study, damping capacities were comparatively investigated for Mg-9%Al alloy with as-cast (AC) and fully discontinuous precipitates (DPs) microstructures, respectively. The DPs microstructure was obtained by solution treatment at 678 K for 24 h, followed by furnace cooling to RT. The AC microstructure was typically characterized by partially divorced eutectic β(Mg17Al12) phase particles distributed along the α-(Mg) matrix cell boundaries. The DPs microstructure showed lamellar morphology consisting of α and β thin layers with various interlamellar spacings. The DPs microstructure had better damping capacity than the AC microstructure in the strain-amplitude independent region, while in the strain-amplitude dependent region, the damping behavior was reversed. In view of the microstructural features of AC and DPs, the lower concentration of Al in the α-(Mg) phase for the DPs microstructure and the lower β phase number density for the AC microstructure would be responsible for the higher damping capacities in the strain-amplitude independent and strain-amplitude dependent regions, respectively.