• Title/Summary/Keyword: epoxy type resin

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A Study on Detection of Elastic Wave Using Patch Type Piezo-Polymer Sensor (부착형 고분자 압전센서를 이용한 탄성파 검출 연구)

  • Kim, Ki-Bok;Yoon, Dong-Jin;Kueon, Jae-Hwa;Lee, Young-Seop
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.3
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    • pp.268-274
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    • 2004
  • Patch type piezo-polymer sensors for smart structures were experimented to detect elastic wave. The pencil lead braking test was performed to analyze the characteristics of patch-type piezo-polymer sensors such as polyvinyliden fluoride (PVDF) and polyvinylidene fluoride trifluorethylene (P(VDF-TrFE)) for several test specimens with various elastic wave velocities and acoustical impedances. The characteristics of the patch-type piezo-polymer sensor were compared with the commercial PZT acoustic emission (AE) sensor. The vacuum grease and epoxy resin were used as a couplant for the acoustic impedance matching between the sensor and specimen. The peak amplitude of elastic wave increased as the diameter of piezo-film and acoustical impedance of the specimen increased. The frequency detection range of the piezo-film sensors decreased with increasing diameter of the piezo-film sensor. The P(VDF-TrFE) sensor was more sensitive than the PVDF sensor.

EVALUATION OF THE INTERFACES BETWEEN IMPLANTS AND REGENERATED BONE USING BONE MORPHOGENETIC PROTEIN AND DEMINERALIZED FREEZE-DRIED BONE (임플란트 매식시 골형성단백질 및 탈회동종골 사용에 따른 골재생 및 계면에 대한 연구)

  • Kang, Sang-Gyu;Lee, Jong-Ho;Kim, Myung-Jin
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.26 no.1
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    • pp.24-39
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    • 2000
  • Various methods and graft materials have been used to fill in the defect adjacent to the implants and considered as clinically acceptable. But it is not clear whether the regenerated bone increases the implant-bone contact and supports the implant. The purpose of this study is to evaluate regenerated bone surrounding implants using bone morphogenetic protein(BMP) and demineralized freeze-dried bone(DFDB), and the interfaces between implants and regenerated bone. bBMP was extracted and partially purified from the bovine bone matrix using heparine chromatography. Demineralized freeze-dried bone was made from the dog. Inactive insoluble collagenous bone matrix(IBM) of dog was used as carrier of bBMP. Interfaces of titanium coated epoxy resin implants were processed for demineralized section for transmission electron microscopy(TEM) and those of screw type implants were for nondemineralized section for light and fluoromicroscopic examination. Implants were inserted in the inferior border of mandible of adult dogs and artificial bony defects($3{\times}3{\times}4mm$) were made at the mesial and distal side of implants. Defects were filled with BMP(BMP group) and DFDB(DFDB group). For the fluoromicroscopic examination, the fluorescent dyes(oxytetracycline, calcein green, alizarin red) were injected 2, 4, 6, 8, 12 weeks after implantation. The experimental animals were sacrificed at the 6th and the 12th week and their mandible were extirpated and processed for examination with light microscopy, fluoromicroscopy and TEM. The obtained results were as follows : 1. By the light microscopic findings, the defects were filled with woven bone at the 6th week and compact bone at the 12th week, and the osseointegrations were seen in both groups. There was no histological difference between them. 2. On the basis of the histomorphometric analysis, BMP group(6th week: 40.25%, 12th week: 56.04%) had higher bony contact ratio than DFDB group(38.37%, 42.63%). There was significant difference between two groups at the 12th week(p<0.05). 3. The amount of bone formation in BMP group was more prominent than in DFDB group. Significant difference was noted among two groups at the 6th and the 8th week(p<0.05). 4. By the transmission electron microscopic findings, $0.4-2{\mu}m$ soft tissue layer was found in adjacent to the interfaces and over the collagen fibrils of bone at the 6th week. However, about 100nm amorphous layer was noted at the interface or collagen fibrils directly extended to the titanium surface at the 12th week. There was no significant difference between two groups. 5. These results suggest that BMP and DFDB can be used as good graft materials in the regeneration of bone adjacent to implant, and BMP is more valuable as a bone inducer than DFDB.

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Evaluation of Consolidation Properties in Soft Soils Using Elastic and Electromagnetic Waves (전단파와 전자기파를 이용한 연약 지반의 실내 압밀 특성 평가)

  • Lee, Chang-Ho;Yoon, Hyung-Koo;Kim, Joon-Han;Lee, Jong-Sub
    • Journal of the Korean Geotechnical Society
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    • v.24 no.8
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    • pp.25-34
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    • 2008
  • A new hybrid oedometer cell is designed and manufactured to investigate a behavior of soft soils by using elastic and electromagnetic waves during consolidation test. Bender elements, which generate and detect shear waves, are placed in the top cap and the bottom plate and mounted on the oedometer wall. Double wedge type electrical resistance probe, which measures local void ratio change, is positioned onto the top cap of the oedometer cell. The bender elements and the electrical resistance probe are anchored into a nylon set screw with epoxy resin. The nylon set screw with epoxy resin minimizes directly transmited elastic waves through the oedometer cell due to impedence mismatch and allows for easy replacement of defected bender elements and electrical resistance probe. Primary consolidation time can be estimated from the slope of electrical resistance versus log time curve and the evolution of shear wave velocity. The shear wave velocity can be used to assess inherent anisotropy when disturbance effects are minimized because particle alignment affects the shear wave velocity. The void ratios evaluated by the electrical resistance probe are similar to those by the settlement during consolidation. This study suggests that the shear wave velocity and the electrical resistance can provide complementary imformations to understand consolidation characteristics such as primary consolidation, anisotropy, and void ratio.

A Study on the Measurement of Changes by Light Source in the Restoration Materials of the 10-story Gyeongcheonsa Stone Pagoda (광원에 의한 경천사지 십층석탑 복원재 변화도 측정 조사 연구)

  • Ryu Jaehyoung;Yang Seokjin;Ha Sunhee;Kim Taeha
    • Conservation Science in Museum
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    • v.29
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    • pp.81-98
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    • 2023
  • This study was conducted to examine the effect of the light source for the media facade of the 10-story Gyeongcheonsa Stone Pagoda on the pagoda's restoration materials. To restore the pagoda, two types of epoxy resin-L-30, Araldite (AW106, and HV953U)-were used, and the photostability of the restoration materials and the acceptable lighting irradiation time were estimated through accelerated aging experiments of the restoration specimens. Six types of specimens were used in this process: a specimen painted with blue and yellow pigments for each resin type, and an unpainted specimen. Among them, the ΔE of the unpainted specimens (BA) of Araldite AW106 and HV953U was the highest of 4.66, and the acceptable light irradiation time was about 130,000 hours if the change rate of ΔE is limited to about 1. It was confirmed that the BA specimens were losing their characteristics due to light, as their reflectance and transmittance increased and the absorbance decreased, making them more transparent than their original color. It was found that the painted specimens had a low change rate of ΔE, with insignificant changes in their reflectance, transmittance and absorbance. Therefore, the use of pigments with high photostability provides more restoration materials options.

Thermal effects on nonlinear dynamic characteristics of polymer-CNT-fiber multiscale nanocomposite structures

  • Ebrahimi, Farzad;Habibi, Sajjad
    • Structural Engineering and Mechanics
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    • v.67 no.4
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    • pp.403-415
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    • 2018
  • In the present study, nonlinear dynamic response of polymer-CNT-fiber multiscale nanocomposite plate resting on elastic foundations in thermal environments using the finite element method is performed. In this regard, the governing equations are derived based on Inverse Hyperbolic Shear Deformation Theory and von $K{\acute{a}}rm{\acute{a}}n$ geometrical nonlinearity. Three type of distribution of temperature through the thickness of the plate namely, uniform linear and nonlinear are considered. The considered element is C1-continuous with 15 DOF at each node. The effective material properties of the multiscale composite are calculated using Halpin-Tsai equations and fiber micromechanics in hierarchy. The carbon nanotubes are assumed to be uniformly distributed and randomly oriented through the epoxy resin matrix. Five types of impulsive loads are considered, namely the step, sudden, triangular, half-sine and exponential pulses. After examining the validity of the present work, the effects of the weight percentage of SWCNTs and MWCNTs, nanotube aspect ratio, volume fraction of fibers, plate aspect, temperature, elastic foundation parameters, distribution of temperature and shape of impulsive load on nonlinear dynamic response of CNT reinforced multi-phase laminated composite plate are studied in details.

Property of Carboxylic Polyester Powder Coatings with Different Hardeners (경화제에 따른 열경화성 분체도료의 물성 비교)

  • Choi, Seung-Ok;Kim, Eun-Mi;Yoo, Jung-Hee;Jeong, Noh-Hee
    • Journal of the Korean Applied Science and Technology
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    • v.28 no.3
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    • pp.351-358
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    • 2011
  • It was researched to be alternative of TGIC type hardener with human hazard element as PT 910 mix powder paint with hardener. Generally PT 910 was compared with TGIC & Epoxy resin of hardener to be used at thermosetting powder paint. We inquired a property of matter for paint through Gel time, glass transition temperature, melting point and a property of matter for film through a property of adhesion, a property of tolerance, softness, gloss, acid-resistant, alkali-resistant, salt water spray-resistant, facilitation climatic. When PT 910 is used of hardener, it was shown the excellent results in gel time, softness, salt water spray-resistant, fracilitation climatic and the similar results in melting point, a property of tolerance, a property of adhesion, gloss, acid-resistant, alkali-resistant, as compared with the powder paint used by TGIC hardener. The glass transition temperature was little low. But there was slightly different results. After the study results, we reached the conclusion that thermosetting powder used by PT 910 is alterative to by TGIC hardener.

Conservation of gilted footware excavated from Bokam-ri, Naju Province (나주 복암리 고분 출토 금동신발 보존처리)

  • Yu, Jae-Eun;Wi, Koang-Chul;You, In-Sook;Shin, Ui-Kyoung
    • 보존과학연구
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    • s.19
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    • pp.23-34
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    • 1998
  • Bokam-ri site was excavated from July 1996 to September 1998 and archaeologically assumed to be grouped with tombs of Mahan period. Among these groups, Tomb No. 3 had built up with stone chamber and found one pair of gilted footware near the jar coffin. This footware was severely corroded and cracked so transfered it gently with soil. Radiography film of this footware showed spike decorations on the bottom and fish-shapped ornament. Gilted footware was consolidated with soil using Paraloid B72 10%~15%solution and cleaned using small tools and microscope. SV427 and HV427 as epoxy resin and Araldite(rapid type) used for joining and restoring. The fore part of gilted footware was connected with nails and folded “L” shape to introduce the bottom material. Tortoise-shell design and flower ornaments appeared on the surface and fish-shaped ornaments, spikes and spangles on the bottom. It was found that 7 spikes and 5 fish-shaped ornaments remained well. Especially, Fish-shaped ornaments were firstly found in the gilted footware and appraised archaeologically important materials.

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Evaluation of the Cryogenic Characteristics of Composite/Aluminum Ring Specimens (복합재/알루미늄 링 시편의 극저온 특성 평가)

  • 김명곤;강상국;김천곤;공철원
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.9
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    • pp.25-32
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    • 2006
  • In this study, the characteristics of filament wound composite/aluminum ring specimens were investigated at cryogenic temperature. The ring specimens were manufactured using carbon fibre and Type B epoxy resin which had been developed for cryogenic use. As a result of measuring thermal strains at -150℃, it was found that compressive thermal stress was induced in composite part on the contrary, tensile thermal stress in aluminum part which was about 32% of yield stress and in turn, caused aluminum to be yielded at lower load level. In addition, Thermal strains which resulted from finite element analysis showed good agreement with those of the experiment. After 6 mechanical loading cycles had been applied to the ring specimen at -150℃, tensile tests were performed at -150℃ using a split disk fixture. As a result, it was shown that composite strength in a liner-composite tank structure which is for the use of cryogenic propellant tank would be decreased by auto-frettage pressure which is applied to it.

Effect of various surface treatment methods of highly translucent zirconia on the shear bond strength with resin cement (고투명도 지르코니아의 다양한 표면처리 방법이 레진시멘트와의 전단결합강도에 미치는 영향)

  • Yu-Seong Kim;Jin-Woo Choi;Hee-Kyung Kim
    • The Journal of Korean Academy of Prosthodontics
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    • v.61 no.3
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    • pp.179-188
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    • 2023
  • Purpose. The purpose of this study was to evaluate the effect of surface treatments on the shear bond strength of two types of zirconia (3-TZP and 5Y-PSZ) with resin cement. Materials and methods. Two different types of zirconia specimens with a fully sintered size of 14.0×14.0×2.0 mm3 were prepared, polished with 400, 600, and 800 grit silicon carbide paper, and buried in epoxy resin. They were classified into four groups each control, sandblasting, primer, and sandblasting & primer. Cylindrical resin adhered to the surface-treated zirconia with resin cement. It was stored in distilled water (37℃) for 24 hours, and a shear bond strength test was performed. The normality of the experimental group was confirmed with the Kolmogorov-Smirnov & Shapiro-Wilk test. The interaction and statistical difference were analyzed using a two-way ANOVA. A post-hoc analysis was performed using Dunnett T3. Results. As a result of two-way ANOVA, there was no significant difference in shear bonding strength between zirconia types (P > .05), but there was a significant correlation in the sandblasting, primer, and alumina sandblasting & primer group (P < .05). Dunnett T3 post-test showed that, regardless of the type of zirconia, shear bonding strength was sandblasting & primer > Primer > sandblasting > control group (P < .05). Conclusion. There was no difference in shear bond strength between the types of zirconia. The highest shear bond strength was shown when the mechanical and chemical treatments of the zirconia surface was performed simultaneously.

Fabrication and Evaluation of Heat Transfer Property of 50 Watts Rated LED Array Module Using Chip-on-board Type Ceramic-metal Hybrid Substrate (Chip-on-board 형 세라믹-메탈 하이브리드 기판을 적용한 50와트급 LED 어레이 모듈의 제조 및 방열특성 평가)

  • Heo, Yu Jin;Kim, Hyo Tae
    • Journal of the Microelectronics and Packaging Society
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    • v.25 no.4
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    • pp.149-154
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    • 2018
  • This paper describes the fabrication and heat transfer property of 50 watts rated LED array module where multiple chips are mounted on chip-on-board type ceramic-metal hybrid substrate with high heat dissipation property for high power street and anti-explosive lighting system. The high heat transfer ceramic-metal hybrid substrate was fabricated by conformal coating of thick film glass-ceramic and silver pastes to form insulation and conductor layers, using thick film screen printing method on top of the high thermal conductivity aluminum alloy heat-spreading panel, then co-fired at $515^{\circ}C$. A comparative LED array module with the same configuration using epoxy resin based FR-4 PCB with thermalvia type was also fabricated, then the thermal properties were measured with multichannel temperature sensors and thermal resistance measuring system. As a result, the thermal resistance of the ceramic-metal hybrid substrate in the $4{\times}9$ type LEDs array module exhibited about one third to the value as that of FR-4 substrate, implying that at least triple performance of heat transfer property as that of FR-4 substrate was realized.