• 제목/요약/키워드: epoxy

검색결과 3,689건 처리시간 0.028초

선하중(先荷重)을 받은 RC보의 CFRP-Rod 휨보강 효과에 대한 실험적 연구 (An Experimental Study on the Flexural Behavior of Pre-loaded RC Beams Strengthened with CFRP-Rod)

  • 예상민;천우철;강주원;박성무
    • 한국공간구조학회논문집
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    • 제7권1호
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    • pp.79-85
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    • 2007
  • FRP를 이용한 보강법 중에서도 기존에 일반적으로 행해진 보강법은 Plate 또는 Sheet의 형태로 콘크리트 표면에 부착하여 추가적인 강도를 발현하도록 하는 것이다. 그러나 조기 박락파괴, 부착면의 정리, 보강 단부의 앵커시공, 부착면에 대한 내화처리 등의 어려움이 많다. 이러한 문제점들에 대한 방안으로 막대(Rod) 형태인 CFRP-Rod를 보강모체에 홈을 파고 매립하는 NSMR(Near Surface Mounted Reinforcement)공법이 제안되었고, CFRP-Rod의 보강량, 길이, 간격 등의 변수에 의한 휨보강 능력의 평가에 대한 연구가 이루어져왔다. 그러나 구조물에서 CFRP-Rod의 보강은 어느 정도의 하중이 보강부위에 계속 재하된 상태로 보강이 이루어지게 되므로 본 연구에서는 보강전에 가해지는 선하중(Pre-loading)의 크기를 주요변수로 선하중의 크기에 따른 구조물의 거동 특성을 분석하고자 하였고, 선하중의 크기의 결정은 무보강 시험체의 공칭모멘트와의 비로 결정하였다.

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IN VITRO EVALUATION OF FRACTURE RESISTANCE OF VARIOUS THICKNESS FIBER- REINFORCED COMPOSITE INLAY FPD

  • Yi Yang-Jin;Yoon Dong-Jin;Park Chan-Jin;Cho Lee-Ra
    • 대한치과보철학회지
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    • 제41권6호
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    • pp.762-771
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    • 2003
  • Statement of problem. In dentistry, the minimally prepared inlay resin-bonded fixed partial denture (FPD) made of new ceromer / fiber-reinforced composite (FRC) was recently introduced. However, the appropriate dimensions for the long-term success and subsequent failure strength are still unknown. Purpose. The aim of this study was to investigate the most fracture-resistible thickness combination of the ceromer / FRC using a universal testing machine and an AE analyzer. Material and Methods. A metal jig considering the dimensions of premolars and molars was milled and 56-epoxy resin dies, which had a similar elastic modulus to that of dentin, were duplicated. According to manufacturer's instructions, the FRC beams with various thicknesses (2 to 4 mm) were constructed and veneered with the 1 or 2 mm-thick ceromers. The fabricated FPDs were luted with resin cement on the resin dies and stored at room temperature for 72 hours. AE (acoustic emission) sensors were attached to both ends, the specimens were subjected to a compressive load until fracture at a crosshead speed of 0.5 mm/min. The AE and failure loads were recorded and analyzed statistically. Results. The results showed that the failure strength of the ceromer/FRC inlay FPDs was affected by the total thickness of the connectors rather than the ceromer to FRC ratio or the depth of the pulpal wall. Fracture was initiated from the interface and propagated into the ceromer layer regardless of the change in the ceromer / FRC ratio. Conclusion. Within the limitations of this study, the failure loads showed significant differences only in the case of different connector thicknesses, and no significant differences were found between the same connector thickness groups. The application of AE analysis method in a fiber-reinforced inlay FPD can be used to evaluate the fracture behavior and to analyze the precise fracture point.

치관보철물(齒冠補綴物)의 인접변연부위(隣接邊緣部位)에 작용(作用)하는 Stress에 관(關)한 광탄성학적(光彈性學的) 분석(分析) (Photoelastic Stress Analysis of Proximal Margins in Dental Restorations)

  • 임정규
    • 대한치과보철학회지
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    • 제18권1호
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    • pp.37-47
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    • 1980
  • The purpose of this study was to investigate the stresses in different proximal margins and to measure, quantitatively, the effect of different modifications in the design of preparations on the stresses using two-dimensional photoelasticity. Photoelastic stress analysis is based on the phenomenon, exhibited by most transparent solids, of becoming birefringent, or doubly refracting, when strained. Two birefringent materials were used in this study, PSM-1 and PSM-5 in .standard sheet ($10'{\times}10'{\times}\frac{1}{4}'$ thickness), PSM-1(polyester) was used for constructing the substructure, and PSM-5(epoxy resin) was used in making the restorations to be investigated. Two birefringent materials were used in the construction of composite photoelastic model. Seven variable models were constructed. The peripheral dimensions of all model were constant and the models represent an occlusomesial section of a lower posterior molar. Model 1 represents the knife edge margin (shoulderless), Model 2 represents the chamfer, Model 3 represents a rounded shoulder(no sharp angle between the axial wall and gingival floor), Model 4 represents a flat shoulder (axial wall is a $90^{\circ}$ angle to the gingival wall), Model 5 represents $+15^{\circ}$ angulation, Model 6 has a $-15^{\circ}$ angulation, and Model 7 is the same as Model 4 except that it has a $45^{\circ}$ bevel. Improved artificial stone was used to represent dental cement in luting the composite photoelastic model. Static loading procedures(100 pounds) were used at preplanned sites. The results were as follows; 1. The stresses in the proximal portion of all tested models were compressive in nature when the proximal shoulders were loaded vertically on the same proximal marginal ridge. 2. The round and chamfered preparations were the optimum designs in proximoocclusal restorations. They showed the lowest stress concentration factor, i.e. 2.16 and 2.23, respectively. The knife edged shoulder had the highest value, K=5.39. Round type shoulder geometry experiments reduced the stress concentration factor (S.C.F.) 3. The gingival portion of proximal shoulder geometry was a critical location for stress concentration.

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탄소섬유 복합재료 사각튜브의 압추에너지 흡수 특성

  • 한창환;김근택;이종원;최윤호
    • 항공우주기술
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    • 제1권2호
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    • pp.19-31
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    • 2002
  • 본 연구는 탄소섬유 복합재료 사각튜브의 압축 에너지 흡수 특성을 실험적으로 규명하였으며, 유한요소해석을 통해서 그 특성을 예측하였다. 압축 속도는 0.003mm/sec 와 0.3mm/sec로 하여 사각튜브에 가하였으며, 적층각 별로 실험을 하여 각각에 대한 압축 에너지 흡수 특성인 최대 압축하중과 평균하중을 찾았다. [0/90]₄와 [0/±45/90]₂의 특정 적층각을 가지는 사각튜브에 대해 유한요소해석을 수행하여 최대 압축하중을 예측하였다. 유한요소모델은 좌굴해석을 통해서 나온 형상과 원래 형상을 중첩하였으며, 해석방법은 Tsai-Wu criteria를 사용하였다. 실험으로부터 최대 압축하중은 인 사각튜브에서 나타났고 평균 압축하중은에서 나타났으며, 특정각을 가지는 사각튜브에 대한 최대 압축하중 예측은 실험과 거의 일치하였다.

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연어알에서 분리한 Carotenoprotein의 구조적 특성 (Subunits and Composition of Carotenoprotein from Salmo Salar Eggs)

  • 김재웅;민태진;이태녕
    • 대한화학회지
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    • 제32권4호
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    • pp.377-384
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    • 1988
  • 연어알(Salmo Salar)에서 carotenoprotein을 CM-세룰로스, 50% 황산암모늄 침전, DEAE-세룰로스 및 세파덱스 G-75젤을 사용하여 충분히 정제하였다. 인산염 완충용액(pH 7.0)에서 자외선 흡수극대는 ${\lambda}_{max}$ 409, 540 그리고 580nm이었다. 세파덱스 G-200젤 여과법으로 측정된 분자량은 50, 200rhk 26,000달톤으로 heterogeneous한 두가지 형태였다. 전자는 적자색으로 SDS-PAG 전기영동 결과 분자량이 12,500달톤인 4개의 동일한 subunit로 구성되었고, 상당량의 지질과 만노오스, 갈락토스와 글루코사민을 함유하고 있음을 밝혔다. carotenoprotein의 색소를 추출하여 tlc로 정제한 다음 분배비 시험, 요오드 시험, 에폭시 그룹 시험, 알릴릭 시험, 환원 시험 그리고 아세틸화 시험등의 유기반응과 uv/vis, ir 및 nmr 데이타를 얻어 구조를 결정한 결과 carotenoid는 astaxanthin ester임을 확인하였으며 그 ester는 스테아르산(47.9%)과 팔미트산 (21.4%)이 대부분이었다.

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Effects of early prepubertal exposure to bisphenol A on the onset of puberty, ovarian weights, and estrous cycle in female mice

  • Nah, Won-Heum;Park, Mi-Jung;Gye, Myung-Chan
    • Clinical and Experimental Reproductive Medicine
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    • 제38권2호
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    • pp.75-81
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    • 2011
  • Objective: Bisphenol A (BPA) is a chemical used extensively to manufacture plastics and epoxy resin liners for food and beverage cans. BPA, with properties similar to estrogen, has endocrine-disrupting effects. In the present study, we examined the effects of early prepubertal BPA exposure on the onset of puberty and reproductive parameters such as estrous cycle and reproductive organ weights in female mice. Methods: Female mice were injected subcutaneously at postnatal day (PND) 8 with BPA (0.1, 1, 10, 100 mg/kg) in sesame oil or with sesame oil alone. Body weight was measured from PND 10 to 70. Vaginal opening and estrous cycle were monitored from PND 20 to 29. Animals were sacrificed at PND 25, 30, and 70, and the ovary and uterus weights were measured. Results: Early prepubertal exposure to BPA (10 and 100 mg/kg) significantly decreased body weight from PND 18 to 30. BPA treated mice at testing dose levels showed early opening of the vagina compared to the control group. The number of estrous cycle and days of estrus were significantly decreased in high dose (100 mg/kg) BPA treated mice. The ovary weight at PND 25 and 30 was significantly decreased in all BPA treatment groups. Conclusion: Early prepubertal exposure to BPA accelerated the onset of puberty but decreased reproductive parameters in female mice.

Investigation on interlaminar shear stresses in laminated composite beam under thermal and mechanical loading

  • Murugesan, Nagaraj;Rajamohan, Vasudevan
    • Steel and Composite Structures
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    • 제18권3호
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    • pp.583-601
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    • 2015
  • In the present study, the combined effects of thermal and mechanical loadings on the interlaminar shear stresses of both moderately thin and thick composite laminated beams are numerically analyzed. The finite element modelling of laminated composite beams and analysis of interlaminar stresses are performed using the commercially available software package MSC NASTRAN/PATRAN. The validity of the finite element analysis (FEA) is demonstrated by comparing the experimental test results obtained due to mechanical loadings under the influence of thermal environment with those derived using the present FEA. Various parametric studies are also performed to investigate the effect of thermal loading on interlaminar stresses generated in symmetric, anti-symmetric, asymmetric, unidirectional, cross-ply, and balanced composite laminated beams of different stacking sequences with identical mechanical loadings and various boundary conditions. It is shown that the elevated thermal environment lead to higher interlaminar shear stresses varying with the stacking sequence, length to thickness ratio, ply orientations under identical mechanical loading and boundary conditions of the composite laminated beams. It is realized that the magnitude of the interlaminar stresses along xz plane is always much higher than those of along yz plane irrespective of the ply-orientation, length to thickness ratios and boundary conditions of the composite laminated beams. It is also observed that the effect of thermal environment on the interlaminar shear stresses in carbon-epoxy fiber reinforced composite laminated beams are increasing in the order of symmetric cross-ply laminate, unidirectional laminate, asymmetric cross-ply laminate and anti-symmetric laminate. The interlaminar shear stresses are higher in thinner composite laminated beams compared to that in thicker composite laminated beams under all environmental temperatures irrespective of the laminate stacking sequence, ply-orientation and boundary conditions.

니켈도금된 탄소섬유 강화 에폭시 수지 복합재료의 충격 특성 (Impact Behaviors of Ni-plated Carbon Fibers-reinforced Epoxy Matrix Composites)

  • 박수진;김병주;이종문
    • 폴리머
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    • 제27권1호
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    • pp.52-60
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    • 2003
  • 본 연구에서는 탄소섬유 강화 에폭시 수지 복합재료의 충격 특성 향상을 위해 탄소섬유표면에 전해 및 무전해 니켈도금처리를 하였으며, 이때 각각의 니켈도금법에 따른 충격 특성을 비교 고찰하였다. 도금된 탄소섬유의 표면 특성은 XRD, SEM, 그리고 접촉각 측정을 통해 관찰하였고, 탄소섬유 강화 복합재료의 충격 특성은 Izod형의 충격시험기를 이용하여 분석하였다. 실험결과, 무전해 니켈도금층에는 전해도금층과는 달리 Ni-P 합금이 포함된 것이 XRD를 통하여 확인되었으며, 전해 니켈도금된 탄소섬유가 무전해 니켈도금된 것보다 표면자유에너지가 큰 것이 접촉각 측정을 통해 관찰되었다. 한편, 무전해 니켈도금된 탄소섬유 강화 에폭시 수지 복합재료는 충격강도가 크게 증가하였으나, 전해 니켈도금된 복합재료의 경우는 충격강도가 증가하지 않았다. 이러한 결과는 각각의 도금법에 따른 젖음성의 차이가 탄소섬유 강화 복합재료의 연성을 변화시켜 충격강도 증가에 주요하게 작용되었기 때문으로 사료된다.

한 끝단 형상에 따른 마그네슘 합금과 유리섬유 복합소재 단일겹치기 본드 조인트 거동 분석 (Structural Behavior Evaluation of Mg-GFRP Composite Single-Lap Bonded Joints With Different End Shapes)

  • 김정석;임재용;이우근
    • 한국철도학회논문집
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    • 제17권6호
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    • pp.391-396
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    • 2014
  • 본 연구에서는 마그네슘 합금과 유리섬유/에폭시 복합재로 구성된 단일겹치기 조인트의 접착부재의 끝단 형상에 따른 조인트의 구조거동을 시험적으로 평가하였다. 이를 위해 4가지 서로 다른 끝단부 형상을 갖는 마그네슘 합금-유리섬유/에폭시 복합재 단일겹치기 시편을 제작하였다. 또한, 인장 시험을 통해 각 단일겹치기 조인트의 파단 거동을 평가하였다. 시험결과 끝단형상이 직각인 형상을 갖는 조인트의 파단 강도가 가장 낮았다. 이에 반해, 접착부재가 역방향 테이퍼를 갖는 조인트의 접합강도가 가장 높았고, 이 값은 끝단 형상이 직각인 형상 대비 약 11.1% 증가된 접합강도이다.

IV형 경석고와 경화처리된 IV형 경석고 그리고 폴리우레탄 수지 치형재의 표면경도와 미세구조 특성의 비교 (A comparison of surface hardness and microstructural characteristics between a type IV stone with and without die hardening treatment, and a polyurethane resin die material)

  • 이완선;김지환;김태석;김남식;유진호
    • 대한치과기공학회지
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    • 제34권3호
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    • pp.227-235
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    • 2012
  • Purpose: This study compared the surface hardness (Vickers) and microstructural characteristics between a type IV stone with and without die hardening treatment, a polyurethane die material. Methods: Materials used were a type IV stone(MG Crystal Rock), two die hardeners (Hardening bath, Epox-it), and a polyurethane resin material(Polyluck). Six specimens per group were prepared according to manufacturer's directions. The prepared specimens were tested by means of hardness test, one-way ANOVA analysis, scanning electron microscopic(SEM) observations and energy dispersive spectroscopic(EDS) analysis. Results: In the hardness test and its statistical analysis, there was no significant difference in the surface hardness between a type IV stone and type IV stone with die hardener coating, type IV stone mixed with an epoxy like material instead of water. In contrast, polyurethane resin material exhibited significantly greater surface hardness than other specimen groups (p<0.05). Conclusion: By considering the results of the hardness test, SEM observations and EDS analysis, although the die hardeners on type IV stone did not show remarkable improvement in surface hardness, the die hardener coating on the surface of type IV stone material did show decrease of microporous and improvement of surface defects.