• 제목/요약/키워드: elemental analysis

검색결과 1,140건 처리시간 0.03초

2-phenyl-N-methyl-l,3-thiazolium Perchlorate 유도체의 합성 및 가수분해 (Synthesis and hydrolysis of 2-phenyl-N-methyl-1,3-thiazolium Perchlorate derivatives.)

  • 한만소;이소영
    • 한국응용과학기술학회지
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    • 제15권2호
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    • pp.93-99
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    • 1998
  • 2-phenyl-N-methyl-1,3-thiazolium perchlorate(PTP)derivatives were synthesized via addition and substitution reactions. PTP was hydrolyzed under aqueous hydrochloride. The structures of the compounds were conformed by N.M.R.,I.R., and elemental analysis.

철도화재 안전관리체계 개선 및 장기전략 수립 방안에 관한 연구 (A study on the establishment of advanced safety management system and long-tenn plan for railway fire safety improvement)

  • 왕종배;김상암;곽상록
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2003년도 추계학술대회 논문집(II)
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    • pp.229-234
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    • 2003
  • In this paper, the elemental components and improving purpose in advanced safety management system are reviewed to cope with a railway fire accident. And a considering procedure(V-cycle) of long-term plan for railway fire safety improvement is proposed. For the purpose of preventing recurrence of accident, items which have to be considered in the course of accident investigation and cause analysis are presented according to the stage of investigation activity.

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실험 항암제 2-Formylpyridine Thiosemicarbazone유도체의 철 및 동착물의 합성 (Synthesis of Iron and Copper Complexes of 2-Formylpyridine Thiosemicarbazone Derivatives, Potential Antitumor Agents)

  • 김종윤;최보길;우순형
    • 약학회지
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    • 제26권3호
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    • pp.181-184
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    • 1982
  • The iron and copper chelates of 4-dimethylamino-2-formylpyridine thiosemicarbazone, one of the amine substituted derivatives at 4-C of 2-formylpyridine thiosemicarbazones which are known as the more improved potential antitumor agents, have been synthesized to make them more effective than the ligand (denoted as HL) itself. Their ligand-to-metal ratios were 2:1 and 1:1 for the iron and copper chelates, and the data along with those of elemental analysis and IR spectroscopy showed that. the compositions are [$FeI_{2}{\times}2H_{2}SO_{4}$ and [CuL($H_{2}Cl$O)], respectively.

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소염진통제에 관한 연구 Arylpropionic acid 류의 합성 및 항부종시험 (Studies on the Synthesis of Arylpropionic Acids and their Antiinflammatory Activity)

  • 채동규
    • 약학회지
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    • 제23권2호
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    • pp.119-124
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    • 1979
  • Eight derivatives of arylpropionic acid, arylcarbonylpropicnic acid, and arylhydroxybutyric acid were synthesized and their structures were elucidated on the basis of elemental analysis and spectral data. Also their antiinflammatory activities were evaluated by the method of the inhibitory effect on the carrageenin-induced rat paw edema and compared with phenylbutazone. Compound (I) exhibited 59% edema inhibition vs control when 100 mg/kg, was orally administered, whereas phenylbutazone showed 57.8% for 50mg/kg.

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Carbamate 화합물의 합성 및 보건학적 연구 (Synthesis and Biological Activities of Carbamate Derivative)

  • 민경진
    • 한국환경보건학회지
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    • 제17권1호
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    • pp.104-109
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    • 1991
  • Carbamates are generally used as insecticide, thus 8-hydroxy-5-chloroquinolinyl-N-ethylcarbamate was newly synthesized. Its physical properties were determined and chemical structure was identified by means of IR, nmr in addition to elemental analysis. The effect of the compound on rat's ileum, and antibacterial activity against Staphylococcus aureus, Salmonella typhi, E. coli, and Pseudomonas aeruginosa were examined. It was observed that the dosage over 100 $\mu$g/ml of the compound relaxed rat's ileum and the same dosage of the compound inhibited growth of the above strains of bacteria.

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High resolution spectroscopic study of the peculiar globular cluster M22 (NGC 6656)

  • Kim, Hyeong-Jun;Lee, Jae-Woo
    • 천문학회보
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    • 제42권2호
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    • pp.65.1-65.1
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    • 2017
  • We present the high-resolution spectroscopic study of the red-giant branch (RGB) stars in the peculiar globular cluster M22 (NGC 6656). We obtained high-resolution spectra of 55 RGB stars using the CTIO 4-m telescope and the HYDRA multi-object spectrograph. By employing an improved LTE analysis method, we measured accurate elemental abundances. In this talk, we will discuss the differences in the chemical composition between the two stellar populations in the context of the formation of M22.

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One Pot Synthesis of Bioactive Novel Cyanopyridones

  • Khokhani, Kamlesh;Khatri, Taslimahemad;Patel, Praful
    • 대한화학회지
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    • 제57권4호
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    • pp.476-482
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    • 2013
  • Cyanopyridone was prepared by the condensation of cyanoacetamide, substituted arylaldehydes and malononitrile in presence of pipyridine. The structure of the synthesized compound CP 1-20 was assigned on the basis of elemental analysis, IR, $^1H$-NMR and mass spectroscopy. These compounds were also screened for antimicrobial activity. The Minimum Inhibitory Concentration (MIC) of all the synthesized compounds was compared with standard drugs.

Synthesis of Some Palladium (II) Complexes of 1, 2-Diaminocyclohexane and Dicarboxylates as Cisplatin Analogues of Palladium Series

  • Kim, Jong-Yoon
    • Archives of Pharmacal Research
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    • 제15권4호
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    • pp.336-342
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    • 1992
  • Ten [$Pd^{II}$(dicarboxylato)(1, 2-diaminocyclohexane)] complexes were prepared after the antitumor-active Pt(II)1, 2-diaminocyclohexane complexes as the cisplatin analogues of palladium series. They were characterized by means of elemental analysis, IR and NMR spectroscopy. As a result, the dicarboxylate ligands were conformed to be chelated with Pd(II) within the scope studied. The stability differences beween the dicarboxylato complexes according to the chelate ring size could not be differentiated due to generally lower thermodynamic stability of the dicarboxylato Pd(II) complexes.

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강활 Angelica koreana $M_{AXIMOWICZ}$ 과실의 Coumarin 성분 (Coumarin Components in the Fruits of Angelica koreana $M_{AXIMOWICZ}$)

  • 육창수;류경수
    • 생약학회지
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    • 제1권2호
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    • pp.31-32
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    • 1970
  • Silica gel column chromatography on the ether extract from the fruits of Angelica koreana $M_{AXIMOWICZ}$ gave two kinds of crystalline products of coumarin. The following furocoumarins-imperatorin and bergapten has been identified by elemental analysis, IR, NMR spectra and physico-chemical tests.

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동양 체질론의 감성적 기질을 이용한 안전 직무설계 (Job Design for Safety by Sensibility Based on the Oriental Human Constitution)

  • 최성운;이영석
    • 대한안전경영과학회지
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    • 제1권1호
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    • pp.29-39
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    • 1999
  • Human sensibility ergonomics is the technique that qualities man's sensibility, measures and evaluates it Quantitatively and makes man's life comfortable, safe and delightful by applying it to products or environmental projects. This study consider the sensibility factor of Sasang constitutional medicine, five elemental properties, and Biorhythm in terms of human sensibility ergonomics. And this study measure reaction-time dependent on a temperament or a state and evaluate the differences of reaction-times objectively with the comparison and analysis using the ANOVA. We can harness it for job design.

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