• Title/Summary/Keyword: effective extraction

Search Result 1,655, Processing Time 0.025 seconds

Prediction of Optimal Microwave Extraction Conditions for Functional Compounds from Agrimonia pilosa Ledeb Using Response Surface Methodology (반응표면분석법을 이용한 용아초 기능성 성분의 마이크로웨이브 최적 추출조건 예측)

  • Park, Jong Jin;Lee, Won Young
    • Korean Journal of Medicinal Crop Science
    • /
    • v.24 no.4
    • /
    • pp.263-270
    • /
    • 2016
  • Background: In this study, microwave extraction was used, which is an effective method to extract useful bioactive substances as it requires low quantities of solvent and short time periods. The aim of this study was to determine the optimal extraction conditions for Agrimonia pilosa Ledeb. Methods and Results: The independent variables were ethanol concentration, microwave power, and extraction time, each of which had five levels. The dependent variables were total polyphenol and total flavonoid content, and DPPH radical scavenging activity. To determine the optimal extraction conditions for bioactive compounds, a response surface methodology was employed. Contour maps were generated from polynomial equations. The optimal conditions were then assumed by superimposing these contour maps. Based on the resulting graph, the optimal microwave extraction conditions for Agrimonia pilosa Ledeb were determined as 42 - 48% ethanol concentration, 240 - 280W microwave power, and 13 - 20 min of extraction time. Conclusions: Ethanol concentration had a significant effect on microwave extraction, in terms of total polyphenol and total flavonoid content, as well as DPPH radical scavenging activity. Microwave power and extraction time influenced the total polyphenol content, but not the total flavonoid content or the DPPH radical scavenging activity.

Fundamental Studies for the Removal and Recovery of Silver from Waste Photo-Developing Solution by Solvent Extraction (사진폐액으로부터 용매추출에 의한 은의 제거 및 회수에 대한 기초연구)

  • Lee, Sun-Hwa;Kim, Dong-Su;Lee, Hwa-Young
    • Journal of Korean Society on Water Environment
    • /
    • v.22 no.1
    • /
    • pp.122-127
    • /
    • 2006
  • Fundamental studies were carried out for an effective removal and recovery of silver from waste photo-developing solution by solvent extraction. The organic solvents examined for silver-extraction were ALIQUAT 336, D2EHPA, KELEX 100, and TBP. ALIQUAT 336, which is an anionic exchanger, was found to be efficient for the extraction of silver and the reason for this was considered to be due to the chloride ion contained in its structure. The extent of silver extraction was examined to increase with the concentration of ALIQUAT 336 until it reached 0.6 M and no more extraction was observed above this concentration. The extraction of silver by ALIQUAT 336 was found to reach its pseudo-equilibrium within a few minutes after the reaction started and additional slight increase in silver extraction was observed until 30 minutes of reaction time. The observed differences in silver extraction for artificial and actual waste solutions were considered to be based upon the different ionic form of silver-containing species in these solutions.

Hot-water Extraction Condition of Gastrodia elata Blume by Response Surface Methodology (반응표면분석법을 이용한 천마의 열수 추출조건 설정)

  • Kim Seong-Ho;Kim In-Ho;Kang Bok-Hee;Lee Sang-Han;Kim Jong-Hyun;Lee Jin-Man
    • Food Science and Preservation
    • /
    • v.13 no.2
    • /
    • pp.131-137
    • /
    • 2006
  • In order to reduce the damage of effective component during processing, we carried out hot-water extraction monitering in Gastrodia elata Blume by response surface methodology. The extraction con야tions for vanillyl alcohol, vanillin and coumarin were optimized at 91.07, 93.73 and $96.30^{\circ}C$, for 2.64, 2.58 and 3.84 hr, at the concentration of 15.16, 21.56 and 19.88 mL/g, respectively. The optimal condition for extraction of total phenolics was acheved at $98.14^{\circ}C$, 3.20 hr and 18.63 mL/g. This study elicited regression formula for each variable, and superimposed the total optimal conditions of extraction for effective compounds and optimal condition for antioxidant characteristics dividing processing factors. It is shown that the predicted result under the extraction condition as follows: extraction temperature for $90{\sim}100^{\circ}C$, extraction time for $3{\sim}4hr$, and solvent volume of $15{\sim}20mL/g$ of sample.

Effective Extraction of Phytoecdysteroids from Fronds of Matteuccia struthiopteris and Osmunda japonica (청나래고사리와 고비 지상부의 효율적인 phytoecdysteroids 추출조건)

  • Shin, So-Lim;Lee, Cheol-Hee
    • Korean Journal of Plant Resources
    • /
    • v.24 no.4
    • /
    • pp.351-357
    • /
    • 2011
  • This study was carried out to investigate the effective extraction condition for increase of phytoecdysteroids from fronds of Matteuccia struthiopteris (FMS) and Osmunda japonica (FOJ). Lyophilizated fronds were mixed with three different solvents (MeOH, 80% EtOH or water) and then extraction was carried out by using six different methods, such as, immersion (room temp.), heating (60$^{\circ}C$), stirring (200 rpm) for 6 h, or sonication in 42 kHz ultrasonic bath for 15, 30 and 45 minutes. Contents of 20-hydroxyecdysone (20E) and ponasterone A (PonA) were measured by using HPLC after purification of the extracts by $C_{18}$ cartridge. Altogether, our results indicate that the extraction using sonication with MeOH as a solvent (for 30 minutes) was the most effective condition for 20E and PonA from both MFS and FOJ. Resulting contents of 20E from FMS and FOJ were 66.76 and 104.48 ${\mu}g{\cdot}g^{-1}$ and PonA were 53.43 and 43.82 ${\mu}g{\cdot}g^{-1}$, respectively.

Optimization of Hot-water Extraction Conditions of Bioactive Compounds from Coffee Residue Extracts (커피박으로부터 생리활성물질 생산 증대를 위한 열수추출 공정 개발)

  • Jo, JaeMin;Kim, SeungKi;Min, Bora;Jung, HyunJin;Han, Yeojung;Kim, JinWoo
    • Korean Chemical Engineering Research
    • /
    • v.55 no.3
    • /
    • pp.358-362
    • /
    • 2017
  • In this study, the optimization of extraction parameters (solvent, temperature, time, solvent concentration) for the maximization of polyphenol extraction was performed to produce value-added food and cosmetic additives using a byproduct of coffee extraction process (coffee residue). All of the extraction parameters evaluated in this experiment had significant effects on polyphenol extraction and the results showed the effect of NaOH concentration on the polyphenol production was most significant among tested parameters. Especially, hot water extraction using acid or base was effective rather than hot-water extraction and the addition of 0.1 mol of NaOH increased 1.5 times extraction concentration compared with hot-water extraction using distilled water. It was found that hot-water extraction with NaOH was more effective than hot-water extraction, and 36.5 mg GAE/g DM was obtained under optimum condition of $100^{\circ}C$, 2 mol of NaOH and 30 min. This result was 2.9 times higher than that of 12.5 mg GAE/g DM obtained from the hot-water extraction before optimization. Thus, coffee residue could be used for food and cosmetic industry as a high-value additive such as antioxidant.

A Study on the Separation and Recovery of Magnesium from Waste Bittern (폐해수로부터 마그네슘의 분리.회수에 관한 연구)

  • Ju, Chang-Sik;Lee, Gyeong-Ok;Jeong, Seong-Uk;Park, Heung-Jae;Na, Seok-Eun;Jeong, Gap-Seon
    • Journal of Environmental Science International
    • /
    • v.10 no.5
    • /
    • pp.381-386
    • /
    • 2001
  • The characteristics of precipitation separation and solvent extraction separation of magnesium from the waste bittern were studied experimentally In the result of precipitation separation, the size of magnesium hydroxide precipitated was not affected on pH, but decreased with increasing the precipitation temperature. The purity of magnesium oxide precipitated was increased with pH beyond pH 11. From the solvent extraction separation, the equilibrium extraction ratio of magnesium was increased with pH and temperature of extraction phase, the concentration of stripping phase, and with decreasing pH of stripping phase. The extractant of Aliquat 336 and Acid 810 mixture was more effective than that of DCH18C6 and $D_2EHPA$ mixture in the extraction separation of magnesium.

  • PDF

Effect of Ethanol Concentration on Extraction of Vlolatile Components in Cinnamon (에탄올의 농도가 계피가 향기성분 용출에 미치는 영향)

  • 김나미;김영희
    • The Korean Journal of Food And Nutrition
    • /
    • v.13 no.1
    • /
    • pp.45-52
    • /
    • 2000
  • In order to select the optimum ethanol concentration for extraction of volatile components in cinnamon, the dried cinnamon was extracted with water and 30∼90% ethanol. The volatile components of cinnamon extracts were isolated by the simultaneous distillation extraction method using Likens and Nickerson's extraction apparatus, and analyzed by GC-MS. In cinnamon bark powder 45 components were detected and 21 components were identified. The major component of cinnamon bark powder was cinnamic aldehyde. In water extract of cinnamon, volatile components were not extracted sufficiently. The volatile components of cinnamon were increased with the increment of ethanol concentraction upto 70%. The volatile component of 70% ethanol extract showed similar pattern and amount to cinnamon bark powder. But in 90% ethanol extracts, the number and amount of volatile component were reduced. The above data suggested that 70% ethanol was the most effective solvent for volatile components extraction of cinnamon.

  • PDF

The Case of Nasal Polyp Extraction which was treated with Hemostat Forceps (지혈겸자 적출술을 이용한 비용종 환자의 치험 1례)

  • Kim, Dong-Hyun;Hong, Seung-Ug
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
    • /
    • v.28 no.2
    • /
    • pp.85-92
    • /
    • 2015
  • Object : To report the case of the improved patient after the extraction with hemostst forcept. Methods : We treated one patient who visited Gabsan Korean medical clinic.First two times, We used acupuncture, fumigation, exsanguination, external medincine. He had some agonistic response. But It was not satisfactory. So We operated extraction with hemostat forceps. Result and Conclusion : 1. We extracted nasal polyp, the length of polyp was 5.5 cm2. After extraction, the patient had not headache, nasal congestion and so on.3. On intranasal endoscopy, left nose did not have polyp any more.4. Hemostat forceps extraction is effective to nasal polyp.

Grammatical Structure Oriented Automated Approach for Surface Knowledge Extraction from Open Domain Unstructured Text

  • Tissera, Muditha;Weerasinghe, Ruvan
    • Journal of information and communication convergence engineering
    • /
    • v.20 no.2
    • /
    • pp.113-124
    • /
    • 2022
  • News in the form of web data generates increasingly large amounts of information as unstructured text. The capability of understanding the meaning of news is limited to humans; thus, it causes information overload. This hinders the effective use of embedded knowledge in such texts. Therefore, Automatic Knowledge Extraction (AKE) has now become an integral part of Semantic web and Natural Language Processing (NLP). Although recent literature shows that AKE has progressed, the results are still behind the expectations. This study proposes a method to auto-extract surface knowledge from English news into a machine-interpretable semantic format (triple). The proposed technique was designed using the grammatical structure of the sentence, and 11 original rules were discovered. The initial experiment extracted triples from the Sri Lankan news corpus, of which 83.5% were meaningful. The experiment was extended to the British Broadcasting Corporation (BBC) news dataset to prove its generic nature. This demonstrated a higher meaningful triple extraction rate of 92.6%. These results were validated using the inter-rater agreement method, which guaranteed the high reliability.

DATA MINING-BASED MULTIDIMENSIONAL EXTRACTION METHOD FOR INDICATORS OF SOCIAL SECURITY SYSTEM FOR PEOPLE WITH DISABILITIES

  • BATYHA, RADWAN M.
    • Journal of applied mathematics & informatics
    • /
    • v.40 no.1_2
    • /
    • pp.289-303
    • /
    • 2022
  • This article examines the multidimensional index extraction method of the disability social security system based on data mining. While creating the data warehouse of the social security system for the disabled, we need to know the elements of the social security indicators for the disabled. In this context, a clustering algorithm was used to extract the indicators of the social security system for the disabled by investigating the historical dimension of social security for the disabled. The simulation results show that the index extraction method has high coverage, sensitivity and reliability. In this paper, a multidimensional extraction method is introduced to extract the indicators of the social security system for the disabled based on data mining. The simulation experiments show that the method presented in this paper is more reliable, and the indicators of social security system for the disabled extracted are more effective in practical application.