• Title/Summary/Keyword: drying method

Search Result 1,452, Processing Time 0.033 seconds

A Study on the Development of Flat-Ring Type Restrained Test Method and Performance Evaluation for Evaluating Shrinkage Cracking Properties of Concrete in Early Age (콘크리트 초기 수축균열특성 평가를 위한 판상-링형 구속시험방법의 성능평가에 관한 연구)

  • Kim, Gyu-Yong;Choi, Hyeong-Gil;Lee, Eui-Bae;Nam, Jeong-Soo;Han, Min-Ki
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • v.13 no.3 s.55
    • /
    • pp.188-196
    • /
    • 2009
  • In Concrete, shrinkages occur like plastic shrinkage and drying shrinkage in the early age because of evaporation and transfer of moisture. Within the country, the crack test standardized by KS is used to test the drying shrinkage of the concrete by using the restricted drying shrinkage of Dumbbell type mold, but this test is for the cracking-point and the restricted shrinkage stress. Thus it is difficult to valuate the crack quantitative test. In this study, it is intended to develop the Flat-ring type restrained test method for the shrinkage deformation movement of the concrete and to provide the quantitative data for evaluating the cracks in concrete. And it suggest the proper specimen diameter and quantitative test method about shrinkage crack properties on Flat-ring type restrained test method. And Verified the suitability.

Development of SS-AG20-loaded Polymeric Microparticles by Oil-in-Water (o/w) Emulsion Solvent Evaporation and Spray Drying Methods for Sustained Drug Delivery

  • Choi, Eun-Jung;Bai, Cheng-Zhe;Hong, A-Reum;Park, Jong-Sang
    • Bulletin of the Korean Chemical Society
    • /
    • v.33 no.10
    • /
    • pp.3208-3212
    • /
    • 2012
  • Controlled drug delivery systems employing microparticles offer lots of advantages over conventional drug dosage formulations. Microencapsulation technique have been conducted with biodegradable polymers such as poly(lactic-co-glycolic acid) (PLGA) and poly(lactic acid) (PLA) for its adjustable biodegradability and biocompatibility. In this study, we evaluated two techniques, oil-in-water (o/w) emulsion solvent evaporation and spray drying, for preparation of polymeric microparticles encapsulating a newly synthesized drug, SS-AG20, for the long-term drug delivery of this low-molecular-weight drug with a very short half-life. Drug-loaded microparticles prepared by the solvent evaporation method showed a smoother morphology; however, relatively poor encapsulation efficiency and drastic initial burst were discovered as drawbacks. Spray-dried drug-loaded microparticles had an imperfect surface with pores and distorted portions so that its initial burst was critical (70.05-87.16%) when the preparation was carried out with a 5% polymeric solution. By increasing the concentration of the polymer, the morphology was refined and undesirable initial burst was circumvented (burst was reduced to 35.93-74.85%) while retaining high encapsulation efficiency. Moreover, by encapsulating the drug with various biodegradable polymers using the spray drying method, gradual and sustained drug release, for up to 2 weeks, was achieved.

Influence of Manufacturing Conditions on the Reflectance and Life Time of the Gold Protected IR Mirror (금 증착 적외선 반사판의 반사율 및 수명에 미치는 제조공정 변수의 영향)

  • Choi, Yong-Sun;Lee, Young-Ki;Lee, You-Kee
    • Korean Journal of Materials Research
    • /
    • v.28 no.4
    • /
    • pp.201-207
    • /
    • 2018
  • Infrared(IR) heating has many advantages, such as energy efficiency, reduced heating time, cleanliness, equipment compactness, high drying rate and easy automation. These features of IR heating provide widely industrial applications, such as surface heat treatment in semiconductor fabrication, thermoforming of polymers, drying and disinfection of food products, heating to metal forging, and drying of wet materials. In this study, the characteristics of a protected gold mirror were examined by spectrophotometer and the lifetime of the coating layers were evaluated by a cross-cutting method and salt spray test. The effects of manufacturing conditions on the protected gold mirror were seen and remedies for these effects were noted in order to improve the properties of the protected gold mirror in the drying process. The reflectance and lifetime of the protected gold mirror was influenced by manufacturing conditions, such as surface roughness and forming conditions of the anti-oxide layer, the adhesion layer, the reflecting layer and the protection layer. The results of this study showed that the protected gold mirror manufactured using a buffing method for pre-treatment resulted in the most effective reflectance. In addition, $Al_2O_3$ coating on an Al substrate as an anti-oxide layer was more effective than the anodizing process in the test of reflectance. Furthermore, the protected gold mirror manufactured by layers forming of various materials resulted in the most effective reflectance and lifetime when coated with $Al_2O_3$ as the anti-oxide layer, coated Cr as the adhesion layer, and coated $MgF_2$ as the protection layer.

Chloride Penetration into Concrete in Tidal Zone by Diffusion-Convection Analysis (확산과 이송을 고려한 콘크리트의 염소이온 침투해석)

  • Kim, Ki-Hyun;Cha, Soo-Won;Jung, Hyung-Mok
    • Journal of the Computational Structural Engineering Institute of Korea
    • /
    • v.22 no.6
    • /
    • pp.607-615
    • /
    • 2009
  • Analysis of chloride penetration into concrete is performed considering the repeated wetting and drying conditions of tidal zone, by means of the developed finite element program which enables the diffusion-convection analysis to be conducted. Heat conduction and moisture diffusion are also included in the finite element analysis program in order that their effects to chloride penetration may be considered. For the efficiency of calculation, the analyses of temperature, relative humidity and free chloride concentration are conducted successively in that order, by treating the convection of chloride due to moisture diffusion as an source or sink term. By comparing the analysis result from finite element analysis, where main variable is a wetting and drying period, with the chloride profiles from ACI Life-365 method, it is shown that the Life-365 method gives an accurate result for the submerged zone but does not consider the differences of wetting and drying period. To obtain an accurate chloride profile in the tidal zone, it is confirmed that the diffusion-convection finite element analysis should be applied.

Quality evaluation of Angelica gigas Nakai with different drying methods and different root parts (당귀(當歸)의 건조방법 및 뿌리 부위에 따른 품질 평가)

  • Seong, Gi Un;Beak, Mi Eun;Lee, Young Jong;Won, Jae Hee
    • The Korea Journal of Herbology
    • /
    • v.33 no.1
    • /
    • pp.85-91
    • /
    • 2018
  • Objectives : This study was carried out to evaluate the quality of different drying methods and different roots(primary root and lateral root) of Angelica gigas Nakai. Methods : The experimental method was performed according to the Korea Pharmacopoea Eleventh edition (KP11). Loss on drying, ash, acid insoluble ash, ethanol extract, nodakenin and total decursin contents were tested to evaluate the quality of root tissue of Angelica gigas Nakai. In addition, the treatment of different root parts were prepared in two groups of washing dry process and natural dry process. Results : In comparison of dry processing methods, total contents of nodakenin and total decursin in the primary root and lateral root through washing dry process were ranged from 3.55 to 4.09% and from 5.18 to 6.13%, respectively. And also, those of roots from the natural dry process were from 4.36 to 6.22% and from 6.28 to 8.34%, respectively. In the washing dry process and natural dry process methods, 47.9% and 22.3% higher amount of nodakenin and total decursin were measured in lateral root compared to primary root. In common, lateral roots accumulated higher contents of nodakenin and total decursin compared to primary roots, and samples drying processed with natural dry process compared to washing dry process method contained higher amount of compounds. Conclusions : We sincerely hope that this study will be contributed to the standardization and quality control of Angelica Gigas Root.

Changes of Microorganisms and Active Compounds in Glycyrrhizae Radix as Affected by Drying Method and Gamma Ray Treatments (건조 방법 및 감마선 조사에 따른 감초의 미생물 저감효과 및 유효성분 변화)

  • Kim, Joon-Hee;Kang, Byoung-Man;Kim, Jun Yong;Kim, Ryu-Dam;Hwang, Hyun Chul;Lee, Jae-Woong
    • Korean Journal of Plant Resources
    • /
    • v.35 no.4
    • /
    • pp.428-434
    • /
    • 2022
  • Glycyrrhizae Radix is an herbal medicine vulnerable to fungi. So there are regulations on mycotoxins. Therefore, in this study, the affect of various drying methods and additional gamma irradiation (10 kGy) was studied to suppress the microbial generation of Glycyrrhizae Radix. As a result of detecting and comparing microorganisms using the dry film method for samples prepared by each of natural, hot air, freezing, microwave drying and gamma irradiation, the affect of reducing microorganisms by microwave drying and gamma irradiation was confirmed. There was no statistically significant change in the content of the active compounds between the treatment groups.

Experimental Study on the Water Content Formula of Fresh Concrete by Microwave Oven Drying Test Method (고주파 가열건조 시험방법에 의한 굳지 않은 콘크리트의 단위수량 추정식에 관한 실험적 연구)

  • Park, Min-Yong;Han, Min-Cheol
    • Journal of the Korea Institute of Building Construction
    • /
    • v.23 no.2
    • /
    • pp.143-152
    • /
    • 2023
  • In this research, the microwave oven drying method was investigated as a potential accurate testing approach for determining the water content of fresh concrete. To do so, water content estimation formulas employed in three prominent oven drying test methods were selected, and the calculation principles for each equation, along with potential error factors arising during the actual testing process, were considered. Moreover, a concrete test was conducted to validate the possible error factors. Consequently, it was confirmed that estimation errors in the water content of fresh concrete can occur due to sample deviations arising during the wet screening process for creating mortar specimens or deviations in the coarse aggregate sampling quantity during the sample collection process.

A Method for Determining the Sandstone Porosity by Using a Microwave Oven (마이크로웨이브 오븐을 이용한 사암의 공극률 산출 방법)

  • Woo, Seulgi;Kim, Jinhoo
    • Journal of the Korean earth science society
    • /
    • v.38 no.2
    • /
    • pp.150-160
    • /
    • 2017
  • In order to determine the porosity of rock, the 'standard test method for porosity and density of rock' proposed by the Korean Society for Rock Mechanics is commonly used. However, the standard test method, which uses a drying oven, takes 8 to 24 hours to complete the test in taking samples out of the oven every four hours and measuring the weight of the specimen. To complement these disadvantages, we devised a method for measuring rock porosity by using a microwave oven. The devised method reduced the cause of errors and the inconvenience occurred in the process of weighing samples by constructing a weight monitoring system, which monitors the drying process. A suitable heating/pause time was set up to maintain the temperature of sample below $105{\pm}3^{\circ}C$ in drying process, and an alarm system was implemented in order to stop drying process when the weight change of the rock sample is within 0.1% of the initial weight. The porosity was determined from the dry weight of the sample, which was obtained by the curve fitting of weight monitoring data. Then, the porosities obtained by using the microwave oven were compared with those obtained by the standard test method. Test results using sandstone samples showed that the porosities obtained by a microwave oven was similar to those obtained by the standard method and the porosity difference between two methods was as large as 0.4%. In addition, repeated porosity measurement using the same specimen showed that the standard deviation of the porosity, which reflects the precision of the measurement was as good as 0.23%. Therefore, a microwave oven porosity measurement system can give the porosity of rock samples with high reliability.

Studies on Drying Method of the Powder to Utilize Deteriorated Sweet Persimmon (파찌감 이용을 위한 분말화의 건조방법에 관한 연구)

  • 김성규;이용재;권오창;박윤문;김태춘;조영수
    • Food Science and Preservation
    • /
    • v.7 no.4
    • /
    • pp.389-394
    • /
    • 2000
  • To utilize deteriorated sweet persimmon(Diospyros kaki T.) effectively, this study was investigated about the effective (Dying method of the powder. Chemical components, minerals, fatty acids and amino acids of hot-air dried and freeze dried conditions were determined Sample conditions used on analysis as follow; pretreatments of hot-air dry and freeze dry were soft, soft+peel, mixer, mixer+peel. The contents of crude protein, crude lipid, crude ash of hot-air dry were 0.9-1.1%,15.0-39.0% and 2.3-3.3%, respectively. And those of freeze dry were 1.3-2.2%, 27.-49.0% and 2.5%, respectively. Potassium, magnesium, phosphorus, calcium and sodium content in hot-air dry and freeze dry were high. Other minerals were less than 3.00ppm in all conditions. The major fatty acid contents were detected capric acid(C$\^$10:0/), lauric acid(C$\_$l2:0)/, tridecanoic acid(C$\_$13:00/), palmitic acid(C$\_$l6:00/), palmitoleic acid(C$\_$l6:1/), oleic acid(C$\_$18:1), linoleic acid(C$\_$18:2/), linolenic acid(C$\_$18:3/). The essential amino acids such as aspartic acid, threonine, serine, glutamic acid, glycine, alanine, valine, methirmine, isoleucine, leucine, tryosine, phenylalanine, histidine, lysine, arginine in freeze dry were contained richly. On the basis of chemical analysis, hot-air dry method will have to supply the additional different method, because simple hot-air dry method was shorten the dry time but had many problems. Therefore, the effective drying method considering changed color and nutrition was shown freeze dry method.

  • PDF

In-Bin Drying of Paddy with Ambient Air: Influence of Drying Parameters on Drying Time, Energy Requirements and Quality (상온통풍에 의한 벼의 In-Bin 건조 : 건조시간, 에너지 소요량 및 품질에 미치는 건조조건의 영향)

  • Cheigh, Hong-Sik;Muhlbauer, Werner;Rhim, Jong-Whan;Shin, Myung-Gon
    • Korean Journal of Food Science and Technology
    • /
    • v.17 no.1
    • /
    • pp.25-32
    • /
    • 1985
  • Low-temperature in-bin paddy drying has been examined to study the limitations of this drying method under Korean weather conditions, the initial moisture content of the paddy, the bulk depth and the airflow rate. The results are reported and discussed with regard to drying time, energy requirements and costs, uniformity in the moisture content of the dried kernels and, finally, the quality of the paddy. The tests carried out during the paddy-drying period in 1981 and 1982 have shown that under Korean weather conditions paddy can be dried to safe storage conditions by continuous aeration with ambient air. Depending upon the initial moisture content of the kernels(19.2%-25.5% w.b.), the bulk depth(1.1-3.5m) and the airflow $(3.0-6.9m^3\;air/m^3\;paddy/min)$ the paddy could be dried within 5 to 17 days. The energy requirements and energy costs are shown to be considerably lower than for conventional high-temperature drying. No significant changes in the quality in terms of milling yield, cracking ratio, acid value and germination were observed.

  • PDF