• 제목/요약/키워드: distribution of particle size

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TEOS/O2 플라즈마 반응기에서 미립자 성장에 대한 실험적 분석 (Experimental Analysis on Particle Growth m TEOS/O2 Plasma Reactor)

  • 김동주;김교선
    • 산업기술연구
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    • 제21권B호
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    • pp.149-153
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    • 2001
  • A study on the particle growth in $TEOS/O_2$ plasma was performed, and particle size and its distribution was measured by the electrical aerosol analyzer (EAA), light scattering particle size analyzer and the particle size was also determined by SEM. The effects of process variables such as total gas flow rate, reactor pressure, supplied power and initial reactant concentration on the particle growth were investigated. From the EAA results, the particle size distribution is divided into three groups of the cluster size and the small and large size particles. The particle size distribution measured by the light scattering particle size analyzer becomes bimodal, because the cluster size particles smaller than 20 nm in diameter cannot be detected by the light scattering particle size analyzer. The size of particles measured by the light scattering particle size analyzer is in good agreements with those by the SEM. Also we could understand that the particle formation is very sensitive to the changes of reactor pressure and reactant concentration. As the total gas flow rate increases, the particle size decreases because of the shorter residence time. As the reactor pressure, or the reactant concentration increases, the particle concentration increases and the particles grow more quickly by the faster coagulation between particles.

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Mapping Particle Size Distributions into Predictions of Properties for Powder Metal Compacts

  • German, Randall M.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.704-705
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    • 2006
  • Discrete element analysis is used to map various log-normal particle size distributions into measures of the in-sphere pore size distribution. Combinations evaluated range from monosized spheres to include bimodal mixtures and various log-normal distributions. The latter proves most useful in providing a mapping of one distribution into the other (knowing the particle size distribution we want to predict the pore size distribution). Such metrics show predictions where the presence of large pores is anticipated that need to be avoided to ensure high sintered properties.

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내충격성 폴리스티렌의 형태구조 및 고무상 입도분포 해석 (Interpretation of Morphology and Rubber-Phase Particle Size Distribution of High Impact Polystyrene)

  • 정한균;정대원;안경현;이승종;이성재
    • 폴리머
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    • 제25권5호
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    • pp.744-753
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    • 2001
  • 내충격성 폴리스티렌 (HIPS)의 내충격성에 영향을 주는 중요한 요소 중의 하나는 분산된 고무상 입자의 크기 및 입도분포이다. 본 연구에서는 반응조건이 HIPS의 고무상 입자 크기 및 입도분포에 미치는 영향을 관찰하기 위하여 HIPS를 중합 제조한 다음 고무함량, 교반속도 및 전중합 시간에 따른 고무상 입도분포 및 형태구조를 고찰하였다. 입도분석기로 분석한 결과, 톨루엔을 분산용매로 사용한 경우 열처리 온도가 낮을수록, 열처리 시간이 짧을수록 팽윤의 영향으로 고무상의 평균 입자경이 커졌지만, MEK의 경우에는 열처리 과정이 없어도 보다 합당한 입도분포를 얻을 수 있었다. 고무함량이 증가함에 따라 고무상의 평균 입자경은 뚜렷하게 커졌지만 고무함량이 적은 경우에는 교반속도가 증가하여도 평균 입자경은 그다지 큰 변화를 나타내지 않았다. 하지만 교반속도가 커짐에 따라 고무상 내의 폴리스티렌 포획입자는 크기가 균일해짐을 확인하였다. 또한 전중합시간에 따른 입도분포의 변화를 고찰한 결과 전중합 시간이 길어질수록 보다 작은 입도분포를 얻을수 있었다.

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Model for simulating the effects of particle size distribution on the hydration process of cement

  • Chen, Changjiu;An, Xuehui
    • Computers and Concrete
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    • 제9권3호
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    • pp.179-193
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    • 2012
  • The hydration of cement contributes to the performance characteristics of concrete, such as strength and durability. In order to improve the utilization efficiency of cement and its early properties, the particle size distribution (PSD) of cement varies considerably, and the effects of the particle size distribution of cement on the hydration process should be considered. In order to evaluate effects of PSD separately, experiments testing the isothermal heat generated during the hydration of cements with different particle size distributions but the same chemical composition have been carried out. The measurable hydration depth for cement hydration was proposed and deduced based on the experimental results, and a PSD hydration model was developed in this paper for simulating the effects of particle size distribution on the hydration process of cement. First, a reference hydration rate was derived from the isothermal heat generated by the hydration of ordinary Portland cement. Then, the model was extended to take into account the effect of water-to-cement ratio, hereinafter which was referred to as PSD hydration model. Finally, the PSD hydration model was applied to simulate experiments measuring the isothermal heat generated by the hydration of cement with different particle size distributions at different water-to-cement ratios. This showed that the PSD hydration model had simulated the effects of particle size distribution and water-to-cement ratio on the hydration process of cement with satisfactory accuracy.

하상퇴적물의 입도분포에 따른 수질특성에 관한 연구 (A Study on the Characteristics of Water Quality According to Particle Size Distribution of Sediments)

  • 박성진;김환기
    • 상하수도학회지
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    • 제23권1호
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    • pp.97-105
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    • 2009
  • Analysis was done on the particle size distribution of sediments flown into Saemangeum from the Mankyung and Dongjin River. The organic pollutants and heavy metal existing in the sediments were analyzed, which was further used to study the properties of pollution in the sediments according to the particle size distribution. Conclusions shown below were made from these analyses. The particle size distribution showed a big difference between the upriver areas of Mankyung and Dongjin River. Particles under $75{\mu}m$ showed to be around 85% at Dongjin River, while it showed to be around 70% at Mankyung River. This kind of distribution in particle size concluded in greatly affecting the contamination density of the sediments. From the analysis done on the soil type of sediments, deposition in Mankyung River categorized into Silty loam and Sandy loam, where Silty loam covered most of area and deposition in Dongjin River categorized into Sand, Loamy sand, Silty loam, Sandy loam. Considering the weight ratio, the density of contamination of the sediments by particle size at Dongjin and Mankyung River has been analyzed to show that organic pollutants and heavy metals occupy more than 70% of the whole contamination in the range under the particle size of $75{\mu}m$.

고온정밀주조용 인산염계 매몰재에 관한 연구(I);매몰재의 특성에 미치는 규사의 입도와 입도분포의 영향 (Study on Phosphate Investment for High Temperature Precision Castings(I);The Effect of Particle size and Distribution of Silica Sand on the characteristics of the Investment)

  • 안지홍;이종남
    • 한국주조공학회지
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    • 제5권2호
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    • pp.85-96
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    • 1985
  • In order to investigate the effect of particle size and distribution of silica sand on the characteristics of investment, W/P ratio, setting time, temperature change during setting, setting expansion, thermal expansion and compressive strength of the investments were measured. In this experiment, magnesia clinker and mono ammonium phosphate were used as binder, and particle size and distribution of silica sand were classified for convinence into 10 categories. The main results obtained from this investigation were summerized as follows. 1. W/P ratio decreased with increase of particle size and evenness in distribution of sand grain. 2. Setting time decreased with increase of evenness in distribution of sand grain, and temperature during setting increased with evenness in distribution of sand grain. 3. Setting expansion decreased with increase of particle size, while it increased with evenness in distribution of sand grain. 4. Thermal expansion decreased with increase of particle size. 5. Compressive strength increased with increase of particle size and evenness in distribution of sand grain. From above results, G.F.N. 250 sand which contains 30% of 50-100 mesh could be recommended for investment casting.

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입도분포가 액상화 저항강도에 미치는 영향에 관한 실험적 연구 (Experimental Study on the Effect of Particle Size Distribution of Soil on the Liquefaction Resistance Strength)

  • 서경범;최문규;김수일;박인준
    • 한국지반공학회논문집
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    • 제21권7호
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    • pp.13-20
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    • 2005
  • 본 연구에서는 입도분포가 액상화 저항강도 및 동적물성치에 미치는 영향을 실험적으로 검증하였다. 우리나라 준설매립토의 입도분포 조사를 통해 준설매립토의 보편적인 평균입경 4가지와 균등계수 3가지를 선정하였고 평균입경과 균등계수를 각각 달리한 총 12종류의 대표적 준설매립토의 입도분포를 선정, 시료를 제작하였다. 제작된 시료를 이용하여 진동삼축시험을 수행하여 평균입경과 균등계수가 액상화 저항강도에 미치는 영향을 분석하였다. 또한 공진주시험을 수행하여 입도분포가 동적물성치에 미치는 영향도 분석하였다.

입자가 부유된 고온의 제트유동에서 응집과 부력을 고려한 이차원 입자크기 분포해석 (A two dimensional analysis of the evolution of the particle size distribution in particle laden high temperature jet flows including the effects of coagulation and buoyancy)

  • 이방원;최만수;황정호
    • 대한기계학회논문집B
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    • 제21권3호
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    • pp.380-391
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    • 1997
  • A numerical study has been done on the evolution of particle size distribution in particle laden high temperature jet flows undergoing convection, diffusion, thermophoresis and coagulation. The dynamic behavior of these particles have been modelled by approximating the particle size distribution by a lognormal function throughout the process and the moments of the particle size distribution have been used to solve the general dynamic equation. The size distributions of spherical particles in the radial and axial direction have been obtained including the effect of buoyancy. Of particular interests are the variations of geometric mean diameter, number concentration and polydispersity. Results show that buoyancy significantly alters the size distribution in both axial and radial direction. One dimensional analysis for non-spherical particles has also been done and the results have been compared with the existing experimental data.

실시간 입자분포 측정을 위한 Radial Exhaust Multi-port System의 개발 및 성능평가 (Development and Performance Evaluation of Radial Exhaust Multi-port System for Real-time Particle Size Distribution Measurement)

  • 이홍규;이양우;전기수;안강호
    • 한국입자에어로졸학회지
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    • 제9권3호
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    • pp.133-137
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    • 2013
  • Measuring particle size distribution is one of the primary concerns in aerosol studies. For a nano-particle size distribution measurement, many scientists use a combination of a differential mobility analyzer (DMA) and a condensation particle counter (CPC) system, which is a called scanning mobility particle sizer (SMPS). Although it has a very high particle size resolution, some issues still remain. These problems include residence time between a DMA and a CPC, discontinuity of a CPC, and disturbance due to long scanning time during the precise measurement of particles. In particular, long scanning time is not adequate for measuring particle size distribution since the particle concentration is changing during the measurement. In this study, we developed radial exhaust multi-port system (REM-system) with no scanning time and high resolution to measure real-time particle size distribution. As a result of the REM-system performed using mono-disperse particle, it is expected that this system will be suitable for measuring continuously changing aerosol. If the counting efficiency of multi-condensation particle counter (M-CPC) and data inversion matrix are completed, REM-system will be a very adequate system for unsteady aerosol, which changes for SMPS scanning time.

Particle Size and Shape Analysis : The Key to Success in Metal Powder Production

  • Pankewitz, Axel;Park, Yong-Jae
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.702-703
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    • 2006
  • The particle size distribution and shape are among the important parameters for characterisation of quality of metal powders. Specific material properties such as ability to flow, reactivity as well as compressibility and its hardening potentials hence the most important characteristics of sintered metals - are determined by the size distribution and shape. The correct particle size distribution and particle shape information are the key to best product quality in atomisation processes of aluminium, milling of pure metals and other processes. This paper presents state-of-the-art technology for characterization of particle size distribution and shape.

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