• Title/Summary/Keyword: distillation

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A study on development of a reduced-order distillation model and identification using nonlinear filtering techniques (증류공정의 차수감소모델 개발 및 비선형휠터기법을 이용한 모델인식에 관한 연구)

  • 김홍식;이광순
    • 제어로봇시스템학회:학술대회논문집
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    • 1989.10a
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    • pp.367-371
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    • 1989
  • A linear form of reduced-order distillation model is proposed, which contains the physical properties of distillation process and can be used in real time applications. The proposed model is linear in terms of liquid mole fraction and contains some tuning parameters. To verify the applicability of the proposed model, the model identification using nonlinear filtering techniques was applied. As a result, it was found that this model represented the simulated distillation process very closely as the parameters were converged.

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A Study on Optimal Reflux Ratio for Batch Distillation (회분식 증류공정의 환류비 최적에 관한 연구)

  • 이영상;이의수
    • Journal of Institute of Control, Robotics and Systems
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    • v.8 no.10
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    • pp.833-841
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    • 2002
  • We develope a model that can manipulate the reflux ratio of a batch distillation process in real time for optimal operations. Firstly, reflux ratio decision model for batch distillation unit was developed using the simple short-cut method. Secondly, more detailed rigorous method was applied to improve the accuracy of the model. Based on these models, operational strategies for the optimal reflux ratio was proposed. The results are illustrated with suitable examples and compared with the results using commercial simulator.

Development of 3th Effects Evaporative desalination system for Solar Desalination System (태양에너지 해수담수화를 위한 3중 효용 증발식 담수기 개발)

  • Hwang, In-Seon;Joo, Hong-Jin;Yun, Eung-Sang;Kwak, Hee-Youl
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.201-201
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    • 2010
  • The evaporative desalination system with solar energy would be the efficient and attractive method to get fresh water. This study was described the development of Multi Effect Distillation(MED) with solar energy desalination system. The system was designed and manufactured Multi effect distillation on the capacity of $3m^3$/day. The experimental apparatus consists mainly of ejector pump, Hot water pump, flow meter, demister, cooler, evaporator and condenser. Evaporator and condenser were made Shell&Tube Heat Exchanger type with corrugated tube. The experimental variables were chosen $75^{\circ}C$ for hot water inlet temperature, 40, 60 and $80{\ell}$/min for hot water inlet volume flow rate, 6.0 and $8.0{\ell}$/min for evaporator feed seawater flow rate, $18^{\circ}C$ for sea water inlet temperature to cover the average sea water temperature and the salinity of sea water is measured about 33,000 PPM (parts per million). for a year in Korea. This study was analyzed the results of thermal performance of Multi Effect Distillation. The results are as follows, The experimental Multi effect distillation is required about 40 kW heat source for production of $3m^3$/day fresh water. Various operating flow rate was confirm in the experiments to get the optimum design data and the results showed that the optimum total flow was $8.0{\ell}$/min. Comparison of Single Effect Distillation with Multi Effect Distillation showed MED is at least more than double of SED.

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Effect of the Crucible Cover on the Distillation of Cadmium

  • Kwon, S.W.;Jung, J.H.;Lee, S.J.
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2019.05a
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    • pp.69-69
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    • 2019
  • The distillation of liquid cathode is necessary to separate cadmium from the actinide elements in the pyroprocessing since the actinide deposits are dissolved or precipitated in a liquid cathode. It is very important to avoid a splattering of cadmium during evaporation due to the high vapor pressure. Several methods have been proposed to lower the splattering of cadmium during distillation. One of the important methods is an installation of crucible cover on the distillation crucible. A multi-layer porous round cover was proposed to avoid a cadmium splattering in our previous study. In this study, the effect of crucible cover on the cadmium distillation was examined to develop a splatter shield. Various surrogates were used for the actinides in the cadmium. The surrogates such as bismuth, zirconia, and tungsten don't evaporate at the operational temperature of the Cd distiller due to their low vapor pressures. The distillation experiments were carried out in a crucible equipped with cover and in a crucible without cover. About 40 grams of Cd was distilled at a reduced pressure for two hours at various temperatures. The mixture of the cadmium and the surrogate was heated at $470{\sim}620^{\circ}C$. Most of the bismuth remained in the crucible equipped with cover after distillation under $580^{\circ}C$ for two hours, whereas small amount of bismuth decreased in the crucible without cover above $580^{\circ}C$. The liquid bismuth escaped with liquid cadmium drop from the crucible without cover. It seems that the crucible cover played a role to prevent the splash of the liquid cadmium drop. The effect of the cover was not clear for the tungsten or zirconia surrogate since the surrogates remained as a solid powder at the experimental temperature. From the results of this work, it can be concluded that the crucible cover can be used to minimize the deposit loss by prevention of escape of liquid drop from the crucible during distillation of liquid cathode.

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Analysis of Effect on Freshwater Production of Vacuum Membrane Distillation Module according to Housing Leak (중공사막 진공 막증류 모듈의 하우징 누수가 담수 생산에 미치는 영향 분석)

  • Joo, Hongjin;Kwak, Heeyoul
    • Journal of Korean Society of Water and Wastewater
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    • v.30 no.3
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    • pp.313-319
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    • 2016
  • In this study, the performance experiment was conducted to compare the permeate flux of hollow fiber Vacuum Membrane Distillation module according to leak problem between module housing and membrane bundle. For the permeate flux performance experiment of the two Vacuum Membrane Distillation modules, the Lab-scale experimental equipment was built in the capacity of $1m^3/day$. The performance test of the two Vacuum Membrane Distillation modules were analyzed according to the feed water conditions. As a result, it was analyzed that the leak VMD module decreased about 14% of permeate flux than normal VMD module.

Extraction Method of Antioxidants in Soybean Oil (Sweep Co-Distillation 법에 의한 산화방지제의 추출법)

  • 황혜정
    • The Korean Journal of Food And Nutrition
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    • v.12 no.4
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    • pp.358-363
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    • 1999
  • This study was conducted to evaluate the extraction methods for the determination of antioxidants in soybean oil. Recovery rates of various antioxidants in soybean oil showed similar rates as 80.4~102.1% by solvent/solvent extraction method and 89.9~106.4% by sweep co-distillation method except 46.6~61.2% of PG at corresponding spiked concentractions. The maximun recovery rates of antioxidnts were obtained when extraction time and extraction temperature used in UNITREX were 20min and 21$0^{\circ}C$ respectively. In the recovery rates with the activation of florisil when 2% ofwater was added to florisil the highest recovery rates for TBHQ, BHA, BHT were obtained by sweep co-distillation met-hod. Therefore sweep co-distillation method showed less solvent simple operation and high recovery rate compared with solvent/solvent extraction method.

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Knowledge Distillation Based Continual Learning for PCB Part Detection (PCB 부품 검출을 위한 Knowledge Distillation 기반 Continual Learning)

  • Gang, Su Myung;Chung, Daewon;Lee, Joon Jae
    • Journal of Korea Multimedia Society
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    • v.24 no.7
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    • pp.868-879
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    • 2021
  • PCB (Printed Circuit Board) inspection using a deep learning model requires a large amount of data and storage. When the amount of stored data increases, problems such as learning time and insufficient storage space occur. In this study, the existing object detection model is changed to a continual learning model to enable the recognition and classification of PCB components that are constantly increasing. By changing the structure of the object detection model to a knowledge distillation model, we propose a method that allows knowledge distillation of information on existing classified parts while simultaneously learning information on new components. In classification scenario, the transfer learning model result is 75.9%, and the continual learning model proposed in this study shows 90.7%.

Numerical study of direct contact membrane distillation process: Effects of operating parameters on TPC and thermal efficiency

  • Zamaniasl, Mohammadmehdi
    • Membrane and Water Treatment
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    • v.10 no.5
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    • pp.387-394
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    • 2019
  • Membrane distillation (MD) is one of the water treatment processes which involves the momentum, heat and mass transfer through channels and membrane. In this study, CFD modeling has been used to simulate the heat and mass transfer in the direct contact membrane distillation (DCMD). Also, the effect of operating parameters on the water flux is investigated. The result shows a good agreement with the experimental result. Results indicated that, while feed temperature is increasing in the feed side, water flux improves in the permeate side. Since higher velocity leads to the higher mixing and turbulence in the feed channel, water flux rises due to this increase in the feed velocity. Moreover, results revealed that temperature polarization coefficient is rising as flow rate (velocity) increases and it is decreasing while the feed temperature increases. Lastly, the thermal efficiency of direct contact membrane distillation is defined, and results confirm that thermal efficiency improves while feed temperature increases. Also, flow rate increment results in enhancement of thermal efficiency.

A Computer Simulation Study on the Separation Process for Electronic Grade, Highly Pure Carbon Dioxide through a Cryogenic Distillation (심냉 증류를 통한 전자급 고순도 이산화탄소의 분리 공정에 대한 전산 모사 연구)

  • ILSU PARK;HUNGMAN MOON;JUNGHO CHO
    • Transactions of the Korean hydrogen and new energy society
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    • v.34 no.1
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    • pp.83-89
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    • 2023
  • In this study, a computer simulation work has been performed for the separation of electronic grade highly pure carbon dioxide more than 7 N purity through a cryogenic distillation process. For the cold utility as a cooling medium for a condenser of the cryogenic distillation column, propylene was utilized as a refrigerant in the vapor-recompression refrigeration cycle. Through this work, it was concluded that the cryogenic distillation column with two stage compression and refrigeration cycle were essential to obtain a highly-pure liquefied CO2.

The Validation Study of Auto Anlysis Method Combined with Aqua Regia Digestion for Fluorine of Soil (왕수분해와 결합한 자동분석법의 토양 중 불소시험 유효성 연구)

  • Na, Kyung-Ho;Yun, In-Chul;Lee, Jung-Bok
    • Journal of Soil and Groundwater Environment
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    • v.15 no.5
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    • pp.8-15
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    • 2010
  • The purpose of this research is to check the validation of an auto-analysis method combined with aqua regia digestion apparatus for improvement of water distillation method used as a fluorine test of soil. Fluorine contents of CaO used in the pretreatment course of water distillation method were 120 mg/kg ~ 5,064 mg/kg at the blank test, which was exceeded up to maximum 12.5 times of the soil standard, so it was estimated due to a effect of fluorine existing as impurities of CaO. The recovery test of the same samples indicated that water distillation method and auto-analysis method were 134.5mg/kg and 161.7mg/kg respectively, the recovery ratio of the latter was 16.8% higher than the formal. The validation test of two methods satisfied the standard, but auto analysis method was excellent more than distillation method. Also, auto analysis method could save a analysis time up to maximum 4.7 times by comparison with water distillation method.