• Title/Summary/Keyword: dispersion method

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A Study on Cutting Performance of the BTA Drilling (BTA드릴가공의 절삭성능에 관한 연구)

  • 장성규;김순경;전언찬
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.10
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    • pp.65-72
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    • 1998
  • The BTA drilling chip is better for deep hole drilling than other self-piloting with pad drilling chips because the large length to diameter ratio allows a unique cutting force dispersion and better supplies the high pressure fluid. Therefore the BTA is useful for many tasks, such as coolant hole drilling of large scale dies, as well as tube seat drilling, which is essential for the heat exchanger, and variable component drilling for automobiles. Deep hole drilling has several significant problems, such as hole deviation, hole over-size, circularity, straightness, and surface roughness. The reasons for these problems, which often result in quality short comings, are an alignment of the BTA drilling system and the unbalance of cutting force by work piece and tool shape. This paper analyzes the properties through an experiment which com¬pared single-edge BTA drills with multiple-edge BTA drills, as well as the shapes of the tools to cause an unbalance of cutting force, and its effect on the precision of the worked hole. Conclusions are as follows. 1) In SMSSC drilling, 60m/min of BTA with single and multi-edged tools proved the best cutting condition and the lowest wear character. 2) The roundness got a little worse as cutting speed was increased, but surface roughness was hot affected. 3) It was proved that the burnishing torque of both drills approached 26%. which is almost the same as the 24% insisted on by Griffiths, and the dispersion characteristic of the multi-edged BTA drill proved better than the single-edge BTA drill.

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Fabrication of Nano-composites from the Radix of Angelica gigas Nakai by Hot Melt Extrusion Mediated Polymer Matrixs (중합체 매개 용융압출에 의한 참당귀 나노복합체의 제조)

  • Azad, Md Obyedul Kalam;Cho, Hyun Jong;Lim, Jung Dae;Park, Cheol Ho;Kang, Wie Soo
    • Korean Journal of Medicinal Crop Science
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    • v.26 no.5
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    • pp.417-429
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    • 2018
  • Background: The objective of this study was to make colloidal dispersions of the active compounds of radix of Angelica gigas Nakai that could be charaterized as nano-composites using hot melt extrusion (HME). Food grade hydrophilic polymer matrices were used to disperse these compound in aqueous media. Methods and Results: Extrudate solid formulations (ESFs) mediated by various HPMCs (hydroxypropyl methylcelluloses) and Na-Alg polymers made from ultrafine powder of the radix of Angelica gigas Nakai were developed through a physical crosslink method (HME) using an ionization agent (treatment with acetic acid) and different food grade polymers [HPMCs, such as HP55, CN40H, AN6 and sodium alignate (Na-Alg)]. X-ray powder diffraction (XRD) analysis confirmed the amorphization of crystal compounds in the HP55-mediated extrudate solid formulation (HP55-ESF). Differential scanning calorimetry (DSC) analysis indicated a lower enthalpy (${\Delta}H=10.62J/g$) of glass transition temperature (Tg) in the HP55-ESF than in the other formulations. Infrared fourier transform spectroscopy (FT-IR) revealed that new functional groups were produced in the HP55-ESF. The content of phenolic compounds, flavonoid (including decursin and decursinol angelate) content, and antioxidant activity increased by 5, 10, and 2 times in the HP55-ESF, respectively. The production of water soluble (61.5%) nano-sized (323 nm) particles was achieved in the HP55-ESF. Conclusions: Nano-composites were developed herein utilizing melt-extruded solid dispersion technology, including food grade polymer enhanced nano dispersion (< 500 nm) of active compounds from the radix of Angelica gigas Nakai with enhanced solubility and bioavailability. These nano-composites of the radix of Angelica gigas Nakai can be developed and marketed as products with high therapeutic performance.

Characterizations of Modified Silica Nanoparticles(II) ; Preparation and Application of Silica Nanoparticles as a Environmentally Filler

  • Min, Seong-Kee;Bae, Deok-Kwun;Park, Sang-Bo;Yoo, Seong-Il;Lee, Won-Ki;Park, Chan-Young;Seul, Soo-Duk
    • Korean Journal of Materials Research
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    • v.22 no.8
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    • pp.433-438
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    • 2012
  • A chemical process involves polymerization within microspheres, whereas a physical process involves the dispersion of polymer in a nonsolvent. Nano-sized monodisperse microspheres are usually prepared by chemical processes such as water-based emulsions, seed suspension polymerization, nonaqueous dispersion polymerization, and precipitation polymerizations. Polymerization was performed in a four-necked, separate-type flask equipped with a stirrer, a condenser, a nitrogen inlet, and a rubber stopper for adding the initiator with a syringe. Nitrogen was bubbled through the mixture of reagents for 1 hr. before elevating the temperature. Functional silane (3-mercaptopropyl)trimethoxysilane (MPTMS) was used for the modification of silica nanoparticles and the self-assembled monolayers obtained were characterized by X-ray photoelectron spectroscopy (XPS), laser scattering system (LSS), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), elemental analysis (EA), and thermogravimetric analysis (TGA). In addition, polymer microspheres were polymerized by radical polymerization of ${\gamma}$-mercaptopropyl modified silica nanoparticles (MPSN) and acrylamide monomer via precipitation polymerization; then, their characteristics were investigated. From the elemental analysis results, it can be concluded that the conversion rate of acrylamide monomer was 93% and that polyacrylamide grafted to MPSN nanospheres via the radical precipitation polymerization with AAm in ethanol solvent. The microspheres were successfully polymerized by the 'graft from' method.

Estimating the Economic Value of Recreation Sea Fishing in the Yellow Sea: An Application of Count Data Model (가산자료모형을 이용한 서해 태안군 유어객의 편익추정)

  • Choi, Jong Du
    • Environmental and Resource Economics Review
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    • v.23 no.2
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    • pp.331-347
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    • 2014
  • The purpose of this study is to estimate the economic value of the recreational sea fishing in the Yellow Sea using count data model. For estimating consumer surplus, we used several count data model of travel cost recreation demand such as a poisson model(PM), a negative binomial model(NBM), a truncated poisson model(TPM), and a truncated negative binomial model(TNBM). Model results show that there is no exist the over-dispersion problem and a NBM was statistically more suitable than the other models. All parameters estimated are statistically significant and theoretically valid. The NBM was applied to estimate the travel demand and consumer surplus. The consumer surplus pre trip was estimated to be 254,453won, total consumer surplus per person and per year 1,536,896won.

A study on the ordering of PIM family similarity measures without marginal probability (주변 확률을 고려하지 않는 확률적 흥미도 측도 계열 유사성 측도의 서열화)

  • Park, Hee Chang
    • Journal of the Korean Data and Information Science Society
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    • v.26 no.2
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    • pp.367-376
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    • 2015
  • Today, big data has become a hot keyword in that big data may be defined as collection of data sets so huge and complex that it becomes difficult to process by traditional methods. Clustering method is to identify the information in a big database by assigning a set of objects into the clusters so that the objects in the same cluster are more similar to each other clusters. The similarity measures being used in the cluster analysis may be classified into various types depending on the nature of the data. In this paper, we computed upper and lower limits for probability interestingness measure based similarity measures without marginal probability such as Yule I and II, Michael, Digby, Baulieu, and Dispersion measure. And we compared these measures by real data and simulated experiment. By Warrens (2008), Coefficients with the same quantities in the numerator and denominator, that are bounded, and are close to each other in the ordering, are likely to be more similar. Thus, results on bounds provide means of classifying various measures. Also, knowing which coefficients are similar provides insight into the stability of a given algorithm.

Synthesis and Microstructure of Porous Al2O3 with Nano-Sized Cu Dispersions (나노크기 Cu 분산입자를 갖는 Al2O3 다공체의 제조 및 미세조직 특성)

  • Yoo, Ho-Suk;Kim, An-Gi;Hyun, Chang-Yong
    • Korean Journal of Materials Research
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    • v.23 no.1
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    • pp.67-71
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    • 2013
  • Porous $Al_2O_3$ dispersed with nano-sized Cu was fabricated by freeze-drying process and solution chemistry method using Cu-nitrate. To prepare porous $Al_2O_3$, camphene was used as the sublimable vehicle. Camphene slurries with $Al_2O_3$ content of 10 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled to $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were subsequently generated by sublimation of the camphene during drying in air for 48 h. The green body was sintered in a furnace at $1400^{\circ}C$ for 1 h. Cu particles were dispersed in porous $Al_2O_3$ by calcination and hydrogen reduction of Cu-nitrate. The sintered samples showed large pores with sizes of about $150{\mu}m$; these pores were aligned parallel to the camphene growth direction. Also, the internal walls of the large pores had relatively small pores due to the traces of camphene left between the concentrated $Al_2O_3$ particles on the internal wall. EDS analysis revealed that the Cu particles were mainly dispersed on the surfaces of the large pores. These results strongly suggest that porous $Al_2O_3$ with Cu dispersion can be successfully fabricated by freeze-drying and solution chemistry routes.

Microstructure and Mechanical Properties of Al2O3/Fe-Ni Nanocomposite Prepared by Rapid Sintering (급속소결에 의해 제조된 Al2O3/Fe-Ni 나노복합재료의 미세조직 및 기계적 특성)

  • Lee, Young-In;Lee, Kun-Jae;Jang, Dae-Hwan;Yang, Jae-Kyo;Cho, Yong-Ho
    • Journal of Powder Materials
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    • v.17 no.3
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    • pp.203-208
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    • 2010
  • A new High Frequency Induction Heating (HFIH) process has been developed to fabricate dense $Al_2O_3$ reinforced with Fe-Ni magnetic metal dispersion particles. The process is based on the reduction of metal oxide particles immediately prior to sintering. The synthesized $Al_2O_3$/Fe-Ni nanocomposite powders were formed directly from the selective reduction of metal oxide powders, such as NiO and $Fe_2O_3$. Dense $Al_2O_3$/Fe-Ni nanocomposite was fabricated using the HFIH method with an extremely high heating rate of $2000^{\circ}C/min$. Phase identification and microstructure of nanocomposite powders and sintered specimens were determined by X-ray diffraction and SEM and TEM, respectively. Vickers hardness experiment were performed to investigate the mechanical properties of the $Al_2O_3$/Fe-Ni nanocomposite.

Dual-Band Unequal Power-Divider Miniaturized by Metamaterial CRLH Phase-Shift Lines (메타 재질 구조 CRLH 전송선 기반 소형 이중 대역 비균등 전력분배기)

  • Eom, Da-Jeong;Kahng, Sung-Tek
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.23 no.9
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    • pp.1048-1057
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    • 2012
  • In this paper, a new compact dual-band unequal power divider is suggested. Instead of the quarter wavelength transmission line(TX-line)s for the branches of the conventional Wilkinson's power divider, we use composite right- and left-handed(CRLH) phase-shift lines and can reduce the physical length. With the non-linear dispersion of the meta-meterial, each branch in the proposed divider is designed to have $+90^{\circ}$ and $-90^{\circ}$ at $f_1$ and $f_2$ respectively. To validate the proposed method, the performances of the circuit and full-wave simulation results are shown with the CRLH dispersion curve. The measurement results are compared with the simulation results. Also, the size reduction effect by the proposed scheme is addressed.

Effect of Ball Milling on Photosensitive Carbon Nanotube Pastes and Their Field Emission Properties (감광성 CNT paste에 대한 저에너지 Ball Milling 처리 효과)

  • Jang, Eun-Soo;Lee, Han-Sung;Lee, Nae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.154-154
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    • 2008
  • Although the screen printing technology using photosensitive carbon nanotube (CNT) paste has many advantages such as low cost, simple process, uniform emission, and capability of mass production, the CNT paste needs to be improved further in CNT dispersion, printability, adhesion, electrical conductivity, population of CNT emitters, etc. Ball milling has been frequently employed to prepare the CNT paste as ball milling can mix its ingredients very well and easily cut the long, entangled CNTs. This study carried out a parametric approach to fabricating the CNT paste in terms of low-energy ball milling and a paste composition. Field emission properties of the CNT paste was characterized with CNT dispersion and electrical conductivity which were measured by a UV-Vis spectrophotometer and a 4-point probe method, respectively. Main variables in formulating the CNT paste include a length of milling time, and amounts of CNTs and conductive inorganic fillers. In particular, we varied not only the contents of conductive fillers but also used two different sizes of filler particles of ${\mu}m$ and nm ranges. Among many variations of conductive fillers, the best field emission characteristics occurred at the 5 wt% fillers with the mixing ratio of 3:1 for ${\mu}m$-and nm-sizes. The amount and size of fillers has a great effect on the morphology, processing stability, and field emission characteristics of CNT emitter dots. The addition a small amount of nm-size fillers considerably improved the field emission characteristics of the photosensitive CNT paste.

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Ultrasonic guided wave approach incorporating SAFE for detecting wire breakage in bridge cable

  • Zhang, Pengfei;Tang, Zhifeng;Duan, Yuanfeng;Yun, Chung Bang;Lv, Fuzai
    • Smart Structures and Systems
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    • v.22 no.4
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    • pp.481-493
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    • 2018
  • Ultrasonic guided waves have attracted increasing attention for non-destructive testing (NDT) and structural health monitoring (SHM) of bridge cables. They offer advantages like single measurement, wide coverage of acoustical field, and long-range propagation capability. To design defect detection systems, it is essential to understand how guided waves propagate in cables and how to select the optimal excitation frequency and mode. However, certain cable characteristics such as multiple wires, anchorage, and polyethylene (PE) sheath increase the complexity in analyzing the guided wave propagation. In this study, guided wave modes for multi-wire bridge cables are identified by using a semi-analytical finite element (SAFE) technique to obtain relevant dispersion curves. Numerical results indicated that the number of guided wave modes increases, the length of the flat region with a low frequency of L(0,1) mode becomes shorter, and the cutoff frequency for high order longitudinal wave modes becomes lower, as the number of steel wires in a cable increases. These findings were used in design of transducers for defect detection and selection of the optimal wave mode and frequency for subsequent experiments. A magnetostrictive transducer system was used to excite and detect the guided waves. The applicability of the proposed approach for detecting and locating wire breakages was demonstrated for a cable with 37 wires. The present ultrasonic guided wave method has been found to be very responsive to the number of brokenwires and is thus capable of detecting defects with varying sizes.