• 대한금속재료학회지
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• 제46권6호
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• pp.382-389
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• 2008

To manufacture Al MMCs, in-situ melt mixing process is used because it is free from contamination, and it makes reinforcements homogeneously dispersed. Large eddy simulation method is used to find the optimum melt mixing condition. At the Re 3000, the most suitable mixing is occurred between Al-Ti and Al- B melts. The in-situ formed $TiB_2$ particles has the size varying from 40 nm to 130 nm, due to the increase of cooling rate, and exhibits a homogeneous dispersion. And the interface between reinforcement and matrix is clean. Both hardness and Young's modulus of this composite are improved with increasing the cooling rate.

• 한국기계가공학회지
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• 제18권8호
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• pp.1-7
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• 2019

Materials that can be used for 3D printing have been developed in terms of phase and functionality. Materials should also be easily printed with high accuracy. In recent years, the concept of 4D printing has been extended to materials whose physical properties such as shape or volume can change depending on the environment. Typically, such high-performance 3D printing materials include bio-inks and inks for sensors. This study deals with the optimization of the manufacturing method to improve the functional properties of the pressure sensitive material, which can be used as a sensor based on change of the resistance according to the pressure. Specifically, the number of milling for dispersion, the ratio of hardener for controlling elasticity, and the content of MWCNTs were optimized. As a result, a method of manufacturing a highly sensitive pressure-sensitive ink capable of use in 3D printing was introduced.

• 대한화장품학회지
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• 제34권3호
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• pp.175-181
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• 2008

생체 친화성 에칠셀룰로오스 막제를 사용하여 자발적인 유화확산에 의하여 레티닐 팔미테이트를 봉입한 나노입자를 제조하였다. 분산매인 유화제로는 폴리소로베이트 20, 폴리소르베이트 60, 피피지 26-부테스-26/피이지-40 하이드로제네이티드캐스터오일를 이용하여 제조하였으며, 본 결과로서 나노크기 입자를 제조하기에 가장 적절하며 안정한 조건은 1w/v% 에칠셀룰로오스와 3w/v% 폴리소그베이트 60 수용액을 이용한 것이었으며, 레티닐 팔미테이트의 봉입률을 최대화하기 위한 조건은 2w/v% 에칠셀룰로오스와 1w/v% 폴리소르베이트 60 수용액을 이용한 제조 조건이었다. 또한 이 최적 조건에 다른 유효성분에도 적용 가능한 것을 확인하였다.

• Current Optics and Photonics
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• 제1권1호
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• pp.65-72
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• 2017

We propose a nearly lossless, compact, electrically modulated vertical directional coupler, which is based on the controllable evanescent coupling in a previously proposed graphene-assisted total internal reflection (GA-FTIR) scheme. In the proposed device, two single-mode waveguides are separate by graphene-$SiO_2$-graphene layers. By changing the chemical potential of the graphene layers with a gate voltage, the coupling strength between the waveguides, and hence the coupling length of the directional coupler, is controlled. Therefore, for a properly chosen, fixed device length, when an input wave is launched into one of the waveguides, the ratio of their output powers can be controlled electrically. The operation of the proposed device is analyzed, with the dispersion relations calculated using a model of a one-dimensional slab waveguide. The supermodes in the coupled waveguide are calculated using the finite-element method to estimate the coupling length, realistic devices are designed, and their performance was confirmed using the finite-difference time-domain method. The designed $3{\mu}m$ by $1{\mu}m$ device achieves an insertion loss of less than 0.11 dB, and a 24-dB extinction ratio between bar and cross states. The proposed low-loss device could enable integrated modulation of a strong optical signal, without thermal buildup.

• Elastomers and Composites
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• 제54권2호
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• pp.156-160
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• 2019

The changes in the dispersion of carbon black in liquid polyisoprene under shear flow with time have been investigated by time-resolved ultra small-angle X-ray scattering (USAXS) method. The analyses of USAXS profile immediately after the start of shear flow clarified that the aggregates of carbon black with a mean radius of gyration of 14 nm and surface fractal dimension of 2.5 form the fractal network structure with mass-fractal dimension of 2.9. After the application of the shear flow, the scattering intensity increases with time at the observed whole entire q region, and then the a shoulder appears at $q=0.005nm^{-1}$, indicating that the agglomerate is broken and becomes smaller by shear flow. The analysis by the Unified Guinier/Power-law approach yielded several characteristic parameters, such as the sizes of aggregate and agglomerate, mass-fractal dimension of agglomerate, and surface fractal dimension of the primary particle. While the mean radius of gyration of the agglomerate decreases with time, the mean radius of gyration of the aggregate, mass fractal dimension, and surface fractal dimension don't change with time, indicating that the aggregates peel off the surface of the agglomerate.

• Corrosion Science and Technology
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• 제20권3호
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• pp.105-111
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• 2021

In oxidizing nitric acid solutions, stainless steel undergoes intergranular corrosion accompanied by grain dropping and changes in the corrosion rate. For the safe operation of reprocessing plants, this mechanism should be understood. In this study, we constructed a three-dimensional computational model using a cellular automata method to simulate the intergranular corrosion propagation of stainless steel. The computational model was constructed of three types of cells: grain (bulk), grain boundary (GB), and solution cells. Model simulations verified the relationship between surface roughness during corrosion and dispersion of the dissolution rate of the GB. The relationship was investigated by simulation applying a constant dissolution rate and a distributed dissolution rate of the GB cells. The distribution of the dissolution rate of the GB cells was derived from the intergranular corrosion depth obtained by corrosion tests. The constant dissolution rate of the GB was derived from the average dissolution rate. Surface roughness calculated by the distributed dissolution rates of the GBs of the model was greater than the constant dissolution rates of the GBs. The cross-sectional images obtained were comparable to the corrosion test results. These results indicate that the surface roughness during corrosion is associated with the distribution of the corrosion rate.

• Advances in nano research
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• 제10권1호
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• pp.43-57
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• 2021

In this study, thermally induced bifurcation buckling of shallow composite cylindrical panels reinforced with aligned single-walled carbon nanotubes is investigated. Distribution of carbon nanotubes across the thickness of the cylindrical panel as reinforcements may be either uniform or functionally graded. Thermo-mechanical properties of the matrix and reinforcements are considered to be temperature dependent. Properties of the cylindrical panel are obtained using a refined micromechanical approach which introduces the auxiliary parameters into the rule of mixtures. The governing equations are obtained by using the static version of the Hamilton principle based on the first-order shear deformation theory and considering the linear strain-displacement relation. An energy-based Ritz method and an iterative process are used to obtain the critical buckling temperature of composite cylindrical panel with temperature dependent material properties. In addition, the effect of various parameters such as the boundary conditions, different geometrical conditions, distribution pattern of CNTs across the thickness and their volume fraction are studied on the critical buckling temperature and buckled pattern of cylindrical panels. It is shown that FG-X type of CNT dispersion is the most influential type in thermal stability.

• Nuclear Engineering and Technology
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• 제53권5호
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• pp.1593-1601
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• 2021

Oxide dispersion strengthening (ODS) tungsten alloys are highly desirable in irradiation applications. However, how to improve the properties of ODS-tungsten alloys efficiently has been worth studying for a long time. Here we report a nanostructuring approach that achieves W-La₂O₃ alloy with a high level of flexural strength and Vickers hardness at room temperature, which have the maximum value of 581 MPa and 703 Hv, respectively. This method named solution combustion synthesis (SCS) can generate 30 nm coating structures W-La₂O₃ composite powders by using Keggin-type structural polyoxometalates as raw materials in a fast and low-cost process. The composite powder can be fabricated to W-La₂O₃ alloy with an optimal microstructure of submicrometric W grains coexisting with nanometric oxide particles in the grain interior, and a stability interface structure of grain boundaries (GBs) by forming transition zones. The method can be used to prepare new ODS alloys with excellent properties in the future.

• International Journal of Naval Architecture and Ocean Engineering
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• 제13권1호
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• pp.833-847
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• 2021

The horizontal porous baffle and its effect as an anti-slosh device have been investigated intensively in a swaying and rolling rectangular tank. To accurately assess the level at which porous baffles reduce liquid sloshing, the Matched Eigenfunction Expansion Method (MEEM) has been utilized as an analytical tool. The velocity potentials in the horizontal baffle-covered fluid region are expressed by the sum of the homogeneous and particular solutions to avoid solving the complex dispersion equation. By applying an equivalent linearized quadratic loss model, the nonlinear algebraic equation is derived and solved by implementing the Newton-Raphson iterative scheme. To prove the validity of the present theoretical model, a series of experiments have been conducted with different centered horizontal porous baffles with varying porosities and submerged depths in a swaying and rolling rectangular tank. Reasonably good agreements are obtained regarding the analytical solutions and the experiment's findings. The influence of porosity, submerged depth, and length of a centered horizontal porous baffle on anti-slosh performance have been analyzed, especially at resonance modes. The developed predictive tool can potentially provide guidelines for optimal design of the horizontal porous baffle.

• 한국초전도ㆍ저온공학회논문지
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• 제10권1호
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• pp.1-5
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• 2008

The effect of $BaCeO_3$ doping on the critical current density of YBCO film by TFA-MOD method was studied. $BaCeO_3$ doping was made by two method; one is direct addition of $BaCeO_3$ nano-sized powder prepared by citrate process followed by grinding with planetary ball mill for 10 hours. Another is addition of Ba-Ce precursor solution prepared with Ba-acetate and Ce acetate dissolved in TFA to the YBCO-TFA precursor solution. The film was made by standard dip coating and heat treatment process with conversion temperature of $790^{\circ}C$ in 1000 ppm oxygen containing moisturized Ar gas atmosphere. The direct addition of $BaCeO_3$ powder resulted in YBCO film with good epitaxial growth and no evidence of second phase formation. The addition through precursor solution resulted in the increase of critical current density upto 30 at% doping and uniform dispersion of $BaCeO_3$ fine inclusion was confirmed by SEM-EDX.