• Title/Summary/Keyword: dislocations

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A High-Resolution Transmission Electron Microscopy Study of the Grain Growth of the Crystalline Silicon in Amorphous Silicon Thin Films (비정질 실리콘 박막에서 결정상 실리콘의 입자성장에 관한 고분해능 투과전자현미경에 의한 연구)

  • 김진혁;이정용;남기수
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.31A no.7
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    • pp.85-94
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    • 1994
  • A high-resolution transmission electron microscopy study of the solid phase crystallization of the amorphous silicon thin films, deposited on SiOS12T at 52$0^{\circ}C$ by low pressure chemical vapor deposition and annealed at 55$0^{\circ}C$ in a dry N$_{2}$ ambient was carried out so that the arrangement of atoms in the crystalline silicon and at the amorphous/crystalline interface of the growing grains could be understood on an atomic level. Results show that circular crystalline silicon nuclei have formed and then the grains grow to an elliptical or dendritic shape. In the interior of all the grains many twins whose{111} coherent boundaries are parallel to the long axes of the grains are observed. From this result, it is concluded that the twins enhance the preferential grain growth in the <112> direction along {111} twin planes. In addition to the twins. many defect such as intrinsic stacking faults, extrinsic stacking faults, and Shockley partial dislocations, which can be formed by the errors in the stacking sequence or by the dissociation of the perfect dislocation are found in the silicon grain. But neither frank partial dislocations which can be formed by the condensation of excess silicon atoms or vacancies and can form stacking fault nor perfect dislocations which can be formed by the plastic deformation are observed. So it is concluded that most defects in the silicon grain are formed by the errors in the stacking sequence during the crystallization process of the amorphous silicon thin films.

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Basal slip (0001)1/3<1120> dislocation in sapphire ($\alpha$-Al$_2$O$_3$) single crystals Part I : recombination motion (사파이어($\alpha$-Al$_2$O$_3$) 단결정에 있어 basal slip (0001)1/3<1120>전위 Part I : 재결합거동)

  • Yoon, Seog-Young
    • Korean Journal of Materials Research
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    • v.11 no.4
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    • pp.278-282
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    • 2001
  • The recombination motion of Partial dislocations on basal slip (0001) 1/3<1120> in sapphire ($\alpha$-Al$_2$$O_3$) single crystals was investigated using the four-point bending test with the prism plane (1120) samples. These bending experiments were carried but in the temperature range from $1200^{\circ}C$ to $1400^{\circ}C$ at various engineering stresses 90MPa, 120MPa, and 150MPa. During these tests it was shown that an incubation time was needed for basal slip to be activated. The activation energy for the incubation time was 5.6-6.0eV in the temperature range from $1200^{\circ}C$ to $1400^{\circ}C$. The incubation time is believed to be related to recombination of climb dissociated partial dislocations via self-climb. In addition, these activation energies are nearly same as those for oxygen self-diffusion in $Al_2$$O_3$ (approximately 6.3 eV). Thus, the recombination of the two partial dislocations would be possibly controlled by oxygen diffusion on the stacking fault between the partials.

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Effects of Growth Rate and III/V Ratio on Properties of AlN Films Grown on c-Plane Sapphire Substrates by Plasma-Assisted Molecular Beam Epitaxy

  • Lim, Se Hwan;Shin, Eun-Jung;Lee, Hyo Sung;Han, Seok Kyu;Le, Duc Duy;Hong, Soon-Ku
    • Korean Journal of Materials Research
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    • v.29 no.10
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    • pp.579-585
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    • 2019
  • In this study, we investigate the effect of Al/N source ratios and growth rates on the growth and structural properties of AlN films on c-plane sapphires by plasma-assisted molecular beam epitaxy. Both growth rates and Al/N ratios affect crystal qualities of AlN films. The full width at half maximum (FWHM) values of ($10{\bar{1}}5$) X-ray rocking curves (XRCs) change from 0.22 to $0.31^{\circ}$ with changing of the Al/N ratios, but the curves of (0002) XRCs change from 0.04 to $0.45^{\circ}$ with changing of the Al/N ratios. This means that structural deformation due to dislocations is slightly affected by the Al/N ratio in the ($10{\bar{1}}5$) XRCs but affected strongly for the (0002) XRCs. From the viewpoint of growth rate, the AlN films with high growth rate (HGR) show better crystal quality than the low growth rate (LGR) films overall, as shown by the FWHM values of the (0002) and ($10{\bar{1}}5$) XRCs. Based on cross-sectional transmission electron microscope observation, the HGR sample with an Al/N ratio of 3.1 shows more edge dislocations than there are screw and mixed dislocations in the LGR sample with Al/N ratio of 3.5.

Effect of Microstructure on the Strain Aging Properties of API X70 Pipeline Steels (API X70 라인파이프 강재의 변형 시효 특성에 미치는 미세조직의 영향)

  • Lee, Seung-Wan;Im, In-Hyuk;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.28 no.12
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    • pp.702-708
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    • 2018
  • This study deals with the effect of microstructure factors on the strain aging properties of API X70 pipeline steels with different microstructure fractions and grain sizes. The grain size and microstructure fraction of the API pipeline steels are analyzed by optical and scanning electron microscopy and electron backscatter diffraction analysis. Tensile tests before and after 1 % pre-strain and thermal aging treatment are conducted to simulate pipe forming and coating processes. All the steels are composed mostly of polygonal ferrite, acicular ferrite, granular bainite, and bainitic ferrite. After 1 % pre-strain and thermal aging treatment, the tensile test results reveal that yield strength, tensile strength and yield ratio increase, while uniform elongation decreases with an increasing thermal aging temperature. The increment of yield and tensile strengths are affected by the fraction of bainitic ferrite with high dislocation density because the mobility of dislocations is inhibited by interaction between interstitial atoms and dislocations in bainitic ferrite. On the other hand, the variation of yield ratio and uniform elongation is the smallest in the steel with the largest grain size because of the decrease in the grain boundary area for dislocation pile-ups and the presence of many dislocations inside large grains after 1 % pre-strain.

Total Elbow Arthroplasty after Failed Surgical Treatment for Elbow Fracture or Dislocation (주관절 골절 혹은 탈구의 실패한 수술적 치료 후 시행한 주관절 전 치환술의 결과)

  • Yi, Jin-Woong;Roh, Jun-Ha;Song, Jong-Hoon;Rhee, Yong-Girl
    • Clinics in Shoulder and Elbow
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    • v.10 no.2
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    • pp.190-198
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    • 2007
  • Purpose: The current study reports the clinical results of total elbow arthroplasties (TEA) which were Performed on patients with poor clinical and radiological results after initial surgeries for elbow fractures or dislocations. Materials and Methods: The clinical outcomes of twelve consecutive patients who underwent TEA after failed surgeries for elbow fractures or dislocations from january, 1995 to December, 2005 were evaluated. The initial diagnoses were distal humeral fractures in 8 cases and fracture-dislocations in 4 cases. The Mean period from the initial operations to the TEAs was 12 months. The mean folloow up period after TEA was 43 months. Results: The mean range of motion, in terms of active extension, activeflexion, supination, and pronation, improved from $14.2^{\circ}$, $96.7^{\circ}$, $50.8^{\circ}$ and $53.3^{\circ}$ to $5.4^{\circ}$, $122.1^{\circ}$, $63.3^{\circ}$ and $67.5^{\circ}$, respectively (p<0.05). RAdiolucent lines were found in 3 cases, which were 1 case of type 3, and 2 cases of type 4. All three loosening cases underwent revision TEAs. The mean postoperative Mayo elvow performance score was 79 point. There were 6 cases of excellent, 2 cases of good, and 4 cases in poor. Conclusion: Good clinical results were obtained after TEA performed in failed surgeries for elbow fractures of dislocations.

The Relationship between Mechanical Properties and Damping Capacity of Thermo-mechanical Treated 316L Stainless Steel (가공열처리한 316L 스테인리스강의 기계적 성질과 감쇠능의 상호관계)

  • Kim, J.S.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.30 no.6
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    • pp.271-278
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    • 2017
  • This study was carried out to investigate the relationship between the mechanical properties and damping capacity of thermo-mechanical treated 316L stainless steel. Dislocations, ${\varepsilon}$ and ${\alpha}^{\prime}$-martensites were formed by thermo-mechanical treatment, and the grain size was changed from micrometer to sub-micrometer by 5-cycled thermo-mechanical treatment. The volume fraction of dislocations, ${\varepsilon}$ and ${\alpha}^{\prime}$-martensites was increased, and grain size of austenite increased and lengthened by the with increasing cycle number of thermo-mechanical treatment. In 5-cycled specimens, the volume fraction of ${\alpha}^{\prime}$-martensite was more than 25% and the less than 5% of volume fraction of ${\varepsilon}$-martensite was attained. With increasing number of thermo-mechanical treatment, hardness, strength and damping capacity were increased, but elongation was decreased. Damping capacity was increased with increased hardness and strength, but decreased with increased elongation, and this result was the opposite tendency for general metal.

Stress intensity factors for periodic edge cracks in a semi-infinite medium with distributed eigenstrain

  • Afsar, A.M.;Ahmed, S.R.
    • Structural Engineering and Mechanics
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    • v.21 no.1
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    • pp.67-82
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    • 2005
  • This study analyzes stress intensity factors for a number of periodic edge cracks in a semiinfinite medium subjected to a far field uniform applied load along with a distribution of eigenstrain. The eigenstrain is considered to be distributed arbitrarily over a region of finite depth extending from the free surface. The cracks are represented by a continuous distribution of edge dislocations. Using the complex potential functions of the edge dislocations, a simple as well as effective method is developed to calculate the stress intensity factor for the edge cracks. The method is employed to obtain the numerical results of the stress intensity factor for different distributions of eigenstrain. Moreover, the effect of crack spacing and the intensity of the normalized eigenstress on the stress intensity factor are investigated in details. The results of the present study reveal that the stress intensity factor of the periodic edge cracks is significantly influenced by the magnitude as well as distribution of the eigenstrain within the finite depth. The eigenstrains that induce compressive stresses at and near the free surface of the semi-infinite medium reduce the stress intensity factor that, in turn, contributes to the toughening of the material.

Analysis of Workplace Accidents in Automotive Repair Workshops in Spain

  • Lopez-Arquillos, Antonio;Rubio-Romero, Juan Carlos
    • Safety and Health at Work
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    • v.7 no.3
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    • pp.231-236
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    • 2016
  • Background: To analyze the effects of the factors associated with different types of injury (superficial wounds, dislocations and sprains, bone fractures, concussion and internal injuries, burns scalding and freezing) caused by occupational accidents in automotive repair workshops. Methods: Study of a sample consisting of 89,954 industry accidents reported from 2003 to 2008. Odds ratios were calculated with a 95% confidence interval. Results: Belonging to a small company is a risk factor for suffering three of the five types of injury studied. Women are less likely to suffer burns and superficial wounds, and more likely to suffer dislocations or sprains. Foreign workers are more likely to suffer concussion and internal injuries. Conclusion: Health and safety strategies and accident prevention measures should be individualized and adapted to the type of worker most likely to be injured in each type of accident. Occupational health and safety training courses designed according to worker profile, and improving the participation of the workers in small firms creating regional or roving safety representatives would improve working conditions.